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Author | Schryvers, D.; Cao, S.; Tirry, W.; Idrissi, H.; Van Aert, S. | ||||
Title | Advanced three-dimensional electron microscopy techniques in the quest for better structural and functional materials | Type | A1 Journal article | ||
Year | 2013 | Publication | Science and technology of advanced materials | Abbreviated Journal | Sci Technol Adv Mat |
Volume | 14 | Issue | 1 | Pages | 014206-14213 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | After a short review of electron tomography techniques for materials science, this overview will cover some recent results on different shape memory and nanostructured metallic systems obtained by various three-dimensional (3D) electron imaging techniques. In binary NiTi, the 3D morphology and distribution of Ni4Ti3 precipitates are investigated by using FIB/SEM slice-and-view yielding 3D data stacks. Different quantification techniques will be presented including the principal ellipsoid for a given precipitate, shape classification following a Zingg scheme, particle distribution function, distance transform and water penetration. The latter is a novel approach to quantifying the expected matrix transformation in between the precipitates. The different samples investigated include a single crystal annealed with and without compression yielding layered and autocatalytic precipitation, respectively, and a polycrystal revealing different densities and sizes of the precipitates resulting in a multistage transformation process. Electron tomography was used to understand the interaction between focused ion beam-induced Frank loops and long dislocation structures in nanobeams of Al exhibiting special mechanical behaviour measured by on-chip deposition. Atomic resolution electron tomography is demonstrated on Ag nanoparticles in an Al matrix. | ||||
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Publisher | Place of Publication | Sendai | Editor | ||
Language | Wos | 000316463800008 | Publication Date | 2013-03-13 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1468-6996;1878-5514; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.798 | Times cited | 6 | Open Access | |
Notes | Fwo; Iap; Esteem | Approved | Most recent IF: 3.798; 2013 IF: 2.613 | ||
Call Number | UA @ lucian @ c:irua:107343 | Serial | 77 | ||
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Author | Lu, J.; Martinez, G.T.; Van Aert, S.; Schryvers, D. | ||||
Title | Lattice deformations in quasi-dynamic strain glass visualised and quantified by aberration corrected electron microscopy | Type | A1 Journal article | ||
Year | 2014 | Publication | Physica status solidi: B: basic research | Abbreviated Journal | Phys Status Solidi B |
Volume | 251 | Issue | 10 | Pages | 2034-2040 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | Advanced transmission electron microscopy and statistical parameter estimated quantification procedures were applied to study the room temperature quasi-dynamical strain glass state in NiTi alloys. Nanosized strain pockets are visualised and the displacements of the atom columns are quantified. A comparison is made with conventional high-resolution transmission electron microscopy images of point defect induced strains in NiAl alloys. | ||||
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Corporate Author | Thesis | ||||
Publisher | Place of Publication | Berlin | Editor | ||
Language | Wos | 000344360000009 | Publication Date | 2014-03-31 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0370-1972; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 1.674 | Times cited | 2 | Open Access | |
Notes | Fwo | Approved | Most recent IF: 1.674; 2014 IF: 1.489 | ||
Call Number | UA @ lucian @ c:irua:120471 | Serial | 1801 | ||
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Author | Wang, X.; Amin-Ahmadi, B.; Schryvers, D.; Verlinden, B.; Van Humbeeck, J. | ||||
Title | Effect of annealing on the transformation behavior and mechanical properties of two nanostructured Ti-50.8at.%Ni thin wires produced by different methods | Type | A1 Journal article | ||
Year | 2013 | Publication | Materials science forum | Abbreviated Journal | |
Volume | 738/739 | Issue | Pages | 306-310 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A Ti-50.8at.%Ni wire produced using a co-drawing method and a commercial Ti-50.8at.%Ni wire were annealed at different temperatures between 450°C and 700°C. Grains with diameter less than 100nm were revealed by transmission electron microscopy for both wires before annealing treatment. However, the microstructural heterogeneity of the co-drawn wire is more obvious than that of the commercial wire. Multi-stage martensitic transformation was observed in the co-drawn wire, compared with the one-stage A↔M transformation in the commercial wire after annealing at 600°C for 30min. The differences of total elongation, plateau strain and pseudoelastic recoverable strain between the commercial wire and the co-drawn wire were also observed. The differences of the transformation behavior and mechanical properties between the commercial wire and the co-drawn wire are attributed to the microstructural difference between these two wires. | ||||
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Corporate Author | Thesis | ||||
Publisher | Place of Publication | Lausanne | Editor | ||
Language | Wos | 000316089000055 | Publication Date | 2013-03-11 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1662-9752; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | Times cited | 5 | Open Access | ||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:104691 | Serial | 798 | ||
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Author | Heidari, H.; Rivero, G.; Idrissi, H.; Ramachandran, D.; Cakir, S.; Egoavil, R.; Kurttepeli, M.; Crabbé, A.C.; Hauffman, T.; Terryn, H.; Du Prez, F.; Schryvers, D. | ||||
Title | Melamine–Formaldehyde Microcapsules: Micro- and Nanostructural Characterization with Electron Microscopy | Type | A1 Journal article | ||
Year | 2016 | Publication | Microscopy and microanalysis | Abbreviated Journal | Microsc Microanal |
Volume | 22 | Issue | 22 | Pages | 1222-1232 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A systematic study has been carried out to compare the surface morphology, shell thickness, mechanical properties, and binding behavior of melamine–formaldehyde microcapsules of 5–30 μm diameter size with various amounts of core content by using scanning and transmission electron microscopy including electron tomography, in situ nanomechanical tensile testing, and electron energy-loss spectroscopy. It is found that porosities are present on the outside surface of the capsule shell, but not on the inner surface of the shell. Nanomechanical tensile tests on the capsule shells reveal that Young’s modulus of the shell material is higher than that of bulk melamine–formaldehyde and that the shells exhibit a larger fracture strain compared with the bulk. Core-loss elemental analysis of microcapsules embedded in epoxy indicates that during the curing process, the microcapsule-matrix interface remains uniform and the epoxy matrix penetrates into the surface micro-porosities of the capsule shells. | ||||
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Publisher | Place of Publication | Editor | |||
Language | Wos | 000393853100011 | Publication Date | 2016-12-21 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1431-9276 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 1.891 | Times cited | 2 | Open Access | |
Notes | This work was supported by SIM vzw, Technologiepark 935, BE-9052 Zwijnaarde, Belgium, within the InterPoCo project of the H-INT-S horizontal program. The authors are also thankful to Stijn Van den Broeck and Dr. Frederic Leroux for help in sample preparation and to S. Bals and J. Verbeeck for valuable discussions. H.I. acknowledges the IAP program of the Belgian State Federal Office for Scientific, Technical and Cultural Affairs, under Contract No. P7/21. | Approved | Most recent IF: 1.891 | ||
Call Number | EMAT @ emat @ c:irua:138980 | Serial | 4333 | ||
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Author | Idrissi, H.; Schryvers, D.; Salje, E.K.H.; Zhang, H.; Carpenter, M.A.; Moya, X. | ||||
Title | Pinning of the martensitic microstructures by dislocations in Cu74.08Al23.13Be2.79 | Type | P1 Proceeding | ||
Year | 2009 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | 02029,1-02029,5 | ||
Keywords | P1 Proceeding; Electron microscopy for materials research (EMAT) | ||||
Abstract | A single crystal of Cu74.08Al23.13Be2.79 undergoes a martensitic phase transition at 246K and 232K under heating and cooling, respectively. Surprisingly, the martensite phase is elastically much harder than the austenite phase showing that interfaces between various crystallographic variants are strongly pinned and can not be moved by external stress while the phase boundary between the austenite and martensite regions in the sample remains mobile. This unusual behavior was revealed by Dynamical Mechanical Analysis and Resonant Ultrasound Spectroscopy. Transmission Electron Microscopy shows that the pinning is generated by dislocations, which are inherited from the austenite phase. Such dislocations can hinder the movement of stacking faults in the 18R martensite structure or twin boundaries between martensite variants. | ||||
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Publisher | Edp | Place of Publication | Coutaboeuf | Editor | |
Language | Wos | 000274582300033 | Publication Date | 2009-08-31 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | ||
Impact Factor | Times cited | 2 | Open Access | ||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:81952 | Serial | 2626 | ||
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Author | Salje, E.K.H.; Zhang, H.; Idrissi, H.; Schryvers, D.; Carpenter, M.A.; Moya, X.; Planes, A. | ||||
Title | Mechanical resonance of the austenite/martensite interface and the pinning of the martensitic microstructures by dislocations in Cu74.08Al23.13Be2.79 | Type | A1 Journal article | ||
Year | 2009 | Publication | Physical review: B: condensed matter and materials physics | Abbreviated Journal | Phys Rev B |
Volume | 80 | Issue | 13 | Pages | 134114,1-1134114,8 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A single crystal of Cu74.08Al23.13Be2.79 undergoes a martensitic phase transition at 246 and 232 K under heating and cooling, respectively. The phase fronts between the austenite and martensite regions of the sample are weakly mobile with a power-law resonance under external stress fields. Surprisingly, the martensite phase is elastically much harder than the austenite phase showing that interfaces between various crystallographic variants are strongly pinned and cannot be moved by external stress while the phase boundary between the austenite and martensite regions in the sample remains mobile. This unusual behavior was studied by dynamical mechanical analysis (DMA) and resonant ultrasound spectroscopy. The remnant strain, storage modulus, and internal friction were recorded simultaneously for different applied forces in DMA. With increasing forces, the remnant strain increases monotonously while the internal friction peak height shows a minimum at 300 mN. Transmission electron microscopy shows that the pinning is generated by dislocations which are inherited from the austenite phase. | ||||
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Publisher | Place of Publication | Lancaster, Pa | Editor | ||
Language | Wos | 000271351300033 | Publication Date | 2009-10-22 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1098-0121;1550-235X; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.836 | Times cited | 38 | Open Access | |
Notes | Multimat | Approved | Most recent IF: 3.836; 2009 IF: 3.475 | ||
Call Number | UA @ lucian @ c:irua:78542 | Serial | 1975 | ||
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Author | Delville, R.; Schryvers, D.; Zhang, Z.; James, R.D. | ||||
Title | Transmission electron microscopy investigation of microstructures in low-hysteresis alloys with special lattice parameters | Type | A1 Journal article | ||
Year | 2009 | Publication | Scripta materialia | Abbreviated Journal | Scripta Mater |
Volume | 60 | Issue | 5 | Pages | 293-296 |
Keywords | A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT) | ||||
Abstract | A sharp drop in hysteresis is observed for shape memory alloys satisfying the compatibility condition between austenite and martensite, i.e. ë2 = 1, where ë2 is the middle eigenvalue of the transformation strain matrix. The present work investigates the evolution of microstructure by transmission electron microscopy as the composition of the Ti50Ni50−xPdx system is systemically tuned to achieve the condition ë2 = 1. Changes in morphology, twinning density and twinning modes are reported along with twinless martensite and exact austenitemartensite interfaces. | ||||
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Publisher | Place of Publication | Oxford | Editor | ||
Language | Wos | 000262553300007 | Publication Date | 2008-11-08 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1359-6462; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.747 | Times cited | 56 | Open Access | |
Notes | Multimat | Approved | Most recent IF: 3.747; 2009 IF: 2.949 | ||
Call Number | UA @ lucian @ c:irua:76017 | Serial | 3710 | ||
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Author | Kuriplach, J.; van Petegem, S.; Hou, M.; Van Tendeloo, G.; Schryvers, D.; et al. | ||||
Title | Positron annihilation study of nanocrystalline Ni3Al : simulations and measurements | Type | A1 Journal article | ||
Year | 2001 | Publication | Materials science forum T2 – 12th International Conference on Positron Annihilation (ICPA-12), AUG 06-12, 2000, UNIV BUNDERSWEHR MUNCHEN, NEUBIBERG, GERMANY | Abbreviated Journal | |
Volume | 363-3 | Issue | Pages | 94-96 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A positron lifetime experiment is performed on samples produced by the compaction of nanocrystalline Ni3Al powder synthesized by the inert-gas condensation technique. In the lifetime spectrum we observe two components corresponding to defects. Computer (virtual) samples of n-Ni3Al are obtained using molecular dynamics combined with the Metropolis Monte Carlo technique. Positron lifetime calculations are then performed on selected regions of simulated samples. For this purpose, a new computational technique based on a generalization of the atomic superposition method for non-periodic systems was developed. Lifetimes calculated in this way are compared to experiment. | ||||
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Publisher | Place of Publication | Lausanne | Editor | ||
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0-87849-875-3 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:102865 | Serial | 2681 | ||
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Author | Ji, G.; Tan, Z.; Shabadi, R.; Li, Z.; Grünewald, W.; Addad, A.; Schryvers, D.; Zhang, D. | ||||
Title | Triple ion beam cutting of diamond/Al composites for interface characterization | Type | A1 Journal article | ||
Year | 2014 | Publication | Materials characterization | Abbreviated Journal | Mater Charact |
Volume | 89 | Issue | Pages | 132-137 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A novel triple ion beam cutting technique was employed to prepare high-quality surfaces of diamond/Al composites for interfacial characterization, which has been unachievable so far. Near-perfect and artifact-free surfaces were obtained without mechanical pre-polishing. Hence, the as-prepared surfaces are readily available for further study and also, ready to be employed in a focus ion beam system for preferential selection of transmission electron microscopy samples. Dramatically different diamond/Al interface configurations – sub-micrometer Al2O3 particles and clean interfaces were unambiguously revealed. | ||||
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Publisher | Place of Publication | New York | Editor | ||
Language | Wos | 000333513400015 | Publication Date | 2014-01-18 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1044-5803; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.714 | Times cited | 9 | Open Access | |
Notes | Fwo | Approved | Most recent IF: 2.714; 2014 IF: 1.845 | ||
Call Number | UA @ lucian @ c:irua:113394 | Serial | 3735 | ||
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Author | Ghidelli, M.; Orekhov, A.; Bassi, A.L.; Terraneo, G.; Djemia, P.; Abadias, G.; Nord, M.; Béché, A.; Gauquelin, N.; Verbeeck, J.; Raskin, J.-p.; Schryvers, D.; Pardoen, T.; Idrissi, H. | ||||
Title | Novel class of nanostructured metallic glass films with superior and tunable mechanical properties | Type | A1 Journal article | ||
Year | 2021 | Publication | Acta Materialia | Abbreviated Journal | Acta Mater |
Volume | Issue | Pages | 116955 | ||
Keywords | A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT) | ||||
Abstract | A novel class of nanostructured Zr50Cu50 (%at.) metallic glass films with superior and tunable mechanical properties is produced by pulsed laser deposition. The process can be controlled to synthetize a wide range of film microstructures including dense fully amorphous, amorphous embedded with nanocrystals and amorphous nano-granular. A unique dense self-assembled nano-laminated atomic arrangement characterized by alternating Cu-rich and Zr/O-rich nanolayers with different local chemical enrichment and amorphous or amorphous-crystalline composite nanostructure has been discovered, while significant in-plane clustering is reported for films synthetized at high deposition pressures. This unique nanoarchitecture is at the basis of superior mechanical properties including large hardness and elastic modulus up to 10 and 140 GPa, respectively and outstanding total elongation to failure (>9%), leading to excellent strength/ductility balance, which can be tuned by playing with the film architecture. These results pave the way to the synthesis of novel class of engineered nanostructured metallic glass films with high structural performances attractive for a number of applications in microelectronics and coating industry. |
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Publisher | Place of Publication | Editor | |||
Language | Wos | 000670077800004 | Publication Date | 2021-05-12 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1359-6454 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 5.301 | Times cited | 27 | Open Access | OpenAccess |
Notes | H.I. is mandated by the Belgian National Fund for Scientific Research (FSR-FNRS). This work was supported by the Fonds de la Recherche Scientifique – FNRS under Grant T.0178.19 and Grant CDR– J011320F. We acknowledge funding for the direct electron detector used in the 4D stem studies from the Hercules fund 'Direct electron detector for soft matter TEM' from the Flemish Government J.V acknowledges funding from the European Union's Horizon 2020 research and innovation program under grant agreement No 823717 – ESTEEM3. A.O. has received partial funding from the GOA project “Solarpaint” of the University of Antwerp. A.B. and J.V. acknowledge funding through FWO project G093417N ('Compressed sensing enabling low dose imaging in transmission electron microscopy') from the Flanders Research Fund. M.G. and A.L.B acknowledge Chantelle Ekanem for support in PLD depositions. | Approved | Most recent IF: 5.301 | ||
Call Number | EMAT @ emat @c:irua:178142 | Serial | 6761 | ||
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Author | Yao, X.; Li, Y.; Cao, S.; Ma, X.; Zhang, X.-ping; Schryvers, D. | ||||
Title | Optimization of Automated Crystal Orientation and Phase Mapping in TEM Applied to Ni-Ti All Round Shape Memory Alloy | Type | P1 Proceeding | ||
Year | 2015 | Publication | MATEC web of conferences T2 – Proceedings of ESOMAT 2015 10th European Symposium on Martensitic Transformations, September 14-18, 2015, Antwerp, Belgium | Abbreviated Journal | |
Volume | 33 | Issue | 33 | Pages | 03022 |
Keywords | P1 Proceeding; Electron microscopy for materials research (EMAT) | ||||
Abstract | A new application which focuses on an artificial sphincter fabricated by Ni-Ti SMAs for human implantation is under investigation by applying the all-round shape memory effect with precise control of the phase transformation temperatures. In this study, a Ni51at.%-Ti alloy was fabricated by arc melting with fast solidification, followed by a proper strained aging which induces the two way shape memory effect needed for this particular application. Differential scanning calorimetry was used to investigate the thermal behavior and transmission electron microscopy was used for studying the microstructure of the alloys. With the latter the novel technique of automated crystal orientation microscopy is used and optimized to obtain phase and orientation mapping of the various structures. | ||||
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Publisher | Place of Publication | Editor | |||
Language | Wos | 000372402800037 | Publication Date | 2015-12-15 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 2261-236X | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | Times cited | 1 | Open Access | ||
Notes | The author gratefully acknowledges the Chinese Scholarship Council (CSC) for providing a scholarship. | Approved | Most recent IF: NA | ||
Call Number | c:irua:129977 | Serial | 3988 | ||
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Author | Pardoen, T.; Colla, M.-S.; Idrissi, H.; Amin-Ahmadi, B.; Wang, B.; Schryvers, D.; Bhaskar, U.K.; Raskin, J.-P. | ||||
Title | A versatile lab-on-chip test platform to characterize elementary deformation mechanisms and electromechanical couplings in nanoscopic objects | Type | A1 Journal article | ||
Year | 2016 | Publication | Comptes rendus : physique | Abbreviated Journal | Cr Phys |
Volume | 17 | Issue | 17 | Pages | 485-495 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A nanomechanical on-chip test platform has recently been developed to deform under a variety of loading conditions freestanding thin films, ribbons and nanowires involving submicron dimensions. The lab-on-chip involves thousands of elementary test structures from which the elastic modulus, strength, strain hardening, fracture, creep properties can be extracted. The technique is amenable to in situ transmission electron microscopy (TEM) investigations to unravel the fundamental underlying deformation and fracture mechanisms that often lead to size-dependent effects in small-scale samples. The method allows addressing electrical and magnetic couplings as well in order to evaluate the impact of large mechanical stress levels on different solid-state physics phenomena. We had the chance to present this technique in details to Jacques Friedel in 2012 who, unsurprisingly, made a series of critical and very relevant suggestions. In the spirit of his legacy, the paper will address both mechanics of materials related phenomena and couplings with solids state physics issues. | ||||
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Publisher | Place of Publication | Editor | |||
Language | Wos | 000373524300020 | Publication Date | 2015-12-01 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1631-0705 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.048 | Times cited | 7 | Open Access | |
Notes | This research has been performed with the financial support of the “Politique scientifique fédérale” under the framework of the interuniversity attraction poles program, IAP7/21, as well as with the support of the “Communauté française de Belgique” under the program “Actions de recherche concertées” ARC 05/10-330 and ARC Convention No. 11/16-037. The support of the “Fonds belge pour la recherche dans l'industrie et l'agriculture (FRIA)” for M.-S. Colla is also gratefully acknowledged as are the FWO research projects G012012N “Understanding nanocrystalline mechanical behavior from structural investigations” for B. Amin-Ahmadi. | Approved | Most recent IF: 2.048 | ||
Call Number | c:irua:129995 | Serial | 4014 | ||
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Author | Verleysen, E.; Bender, H.; Richard, O.; Schryvers, D.; Vandervorst, W. | ||||
Title | Compositional characterization of nickel silicides by HAADF-STEM imaging | Type | A1 Journal article | ||
Year | 2011 | Publication | Journal of materials science | Abbreviated Journal | J Mater Sci |
Volume | 46 | Issue | 7 | Pages | 2001-2008 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A methodology for the quantitative compositional characterization of nickel silicides by high angle annular dark field scanning transmission electron microscopy (HAADF-STEM) imaging is presented. HAADF-STEM images of a set of nickel silicide reference samples Ni3Si, Ni31Si12, Ni2Si, NiSi and NiSi2 are taken at identical experimental conditions. The correlation between sample thickness and HAADF-STEM intensity is discussed. In order to quantify the relationship between the experimental Z-contrast intensities and the composition of the analysed layers, the ratio of the HAADF-STEM intensity to the sample thickness or to the intensity of the silicon substrate is determined for each nickel silicide reference sample. Diffraction contrast is still detected on the HAADF-STEM images, even though the detector is set at the largest possible detection angle. The influence on the quantification results of intensity fluctuations caused by diffraction contrast and channelling is examined. The methodology is applied to FUSI gate devices and to horizontal TFET devices with different nickel silicides formed on source, gate and drain. It is shown that, if the elements which are present are known, this methodology allows a fast quantitative 2-dimensional compositional analysis. | ||||
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Publisher | Place of Publication | London | Editor | ||
Language | Wos | 000286633000002 | Publication Date | 2011-01-06 | |
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Series Volume | Series Issue | Edition | |||
ISSN | 0022-2461;1573-4803; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.599 | Times cited | 1 | Open Access | |
Notes | Approved | Most recent IF: 2.599; 2011 IF: 2.015 | |||
Call Number | UA @ lucian @ c:irua:88950 | Serial | 446 | ||
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Author | Pourbabak, S.; Orekhov, A.; Schryvers, D. | ||||
Title | Twin-jet electropolishing for damage-free transmission electron microscopy specimen preparation of metallic microwires | Type | A1 Journal article | ||
Year | 2020 | Publication | Microscopy Research And Technique | Abbreviated Journal | Microsc Res Techniq |
Volume | Issue | Pages | 1-7 | ||
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A method to prepare TEM specimens from metallic microwires and based on conventional twin-jet electropolishing is introduced. The wire is embedded in an opaque epoxy resin medium and the hardened resin is mechanically polished to reveal the wire on both sides. The resin containing wire is then cut into discs of the appropriate size. The obtained embedded wire is electropolished in a conventional twin-jet electropolishing machine until electron transparency in large areas without radiation damage is achieved. | ||||
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Publisher | Place of Publication | Editor | |||
Language | Wos | 000567944200001 | Publication Date | 2020-09-28 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1059-910x | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.5 | Times cited | Open Access | OpenAccess | |
Notes | ; Fonds Wetenschappelijk Onderzoek, Grant/Award Number: G.0366.15N ; | Approved | Most recent IF: 2.5; 2020 IF: 1.147 | ||
Call Number | UA @ admin @ c:irua:171969 | Serial | 6642 | ||
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Author | Van Tendeloo, G.; De Meulenaere, P.; Schryvers, D. | ||||
Title | Landscape roughness at an atomic scale | Type | A1 Journal article | ||
Year | 1997 | Publication | Physica: D : nonlinear phenomena | Abbreviated Journal | Physica D |
Volume | 107 | Issue | Pages | 401-410 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A large number of materials have a highly degenerate ground state and therefore a complex microstructure. Because of this degenerate state, phase transitions between the different phases play an important role. High resolution techniques in electron microscopy and nano-scale chemical analysis allow to study not only the microstructure but also the interfaces down to an atomic scale. We focus particularly on the ambiguity of alloys oil approaching the phase transition. The short range order (SRO) in ''1 1/20'' type alloys and the microstructure of ''tweed'' and needle formation in martensite like alloys with composition Ni5Al3 are considered in more detail. | ||||
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Publisher | Place of Publication | Amsterdam | Editor | ||
Language | Wos | A1997YC73400034 | Publication Date | 2003-05-13 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0167-2789; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 1.514 | Times cited | 2 | Open Access | |
Notes | Approved | Most recent IF: 1.514; 1997 IF: 1.508 | |||
Call Number | UA @ lucian @ c:irua:21347 | Serial | 1775 | ||
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Author | Tian, H.; Schryvers, D.; Mohanchandra, K.P.; Carman, G.P.; van Humbeeck, J. | ||||
Title | Fabrication and characterization of functionally graded Ni-Ti multilayer thin films | Type | A1 Journal article | ||
Year | 2009 | Publication | Functional materials letters | Abbreviated Journal | Funct Mater Lett |
Volume | 2 | Issue | 2 | Pages | 61-66 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | A functionally graded multilayer NiTi thin film was deposited on a SiO2/Si substrate by d.c. sputtering using a ramped heated NiTi alloy target. The stand-alone films were crystallized at 500°C in vacuum better than 10-7 Torr. Transmission electron microscopy micrographs taken along the film cross section show two distinct regions, thin and thick, with weak R and B2 phases, respectively. The film compositions along the thickness were measured and quantified using the standard-less EELSMODEL method. The film deposited during the initial thermal ramp (thin regions) displays an average of 54 at.% Ni while the film deposited at a more elevated target temperature (thick regions) shows about 51 at.% Ni. | ||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Editor | |||
Language | Wos | 000271077000003 | Publication Date | 2009-07-22 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1793-6047;1793-7213; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 1.234 | Times cited | 9 | Open Access | |
Notes | Fwo | Approved | Most recent IF: 1.234; 2009 IF: 2.561 | ||
Call Number | UA @ lucian @ c:irua:77655 | Serial | 1165 | ||
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Author | Boyat, X.; Ballat-Durand, D.; Marteau, J.; Bouvier, S.; Favergeon, J.; Orekhov, A.; Schryvers, D. | ||||
Title | Interfacial characteristics and cohesion mechanisms of linear friction welded dissimilar titanium alloys: Ti–5Al–2Sn–2Zr–4Mo–4Cr (Ti17) and Ti–6Al–2Sn–4Zr–2Mo (Ti6242) | Type | A1 Journal article | ||
Year | 2019 | Publication | Materials characterization | Abbreviated Journal | Mater Charact |
Volume | 158 | Issue | Pages | 109942 | |
Keywords | A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT) | ||||
Abstract | A detailed microstructural examination endeavoring to understand the interfacial phenomena yielding to cohesion in solid-state assembling processes was performed. This study focuses on the transition zone of a dissimilar titanium alloy joint obtained by Linear Friction Welding (LFW) the β-metastable Ti17 to the near-α Ti6242. The transition zone delimitating both alloys is characterized by a sharp microstructure change from acicular HCP (Hexagonal Close-Packed) α′ martensitic laths in the Ti6242 to equiaxed BCC β (Body-Centered Cubic) subgrains in the Ti17; these α′ plates were shown to precipitate within prior-β subgrains remarkably more rotated than the ones formed in the Ti17. Both α′ and β microstructures were found to be intermingled within transitional subgrains demarcating a limited gradient from one chemical composition to the other. These peculiar interfacial grains revealed that the cohesive mechanisms between the rubbing surfaces occurred in the single-phase β domain under severe strain and high-temperature conditions. During the hot deformation process, the mutual migration of the crystalline interfaces from one material to another assisted by a continuous dynamic recrystallization process was identified as the main adhesive mechanism at the junction zone. The latter led to successful cohesion between the rubbing surfaces. Once the reciprocating motion stopped, fast cooling caused both materials to experience either a βlean→α′ or βlean→βmetastable transformation in the interfacial zone depending on their local chemical composition. The limited process time and the subsequent hindered chemical homogenization at the transition zone led to retaining the so-called intermingled α’/βm subgrains constituting the border between both Ti-alloys. |
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Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Editor | |||
Language | Wos | 000503314000018 | Publication Date | 2019-10-16 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1044-5803 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.714 | Times cited | Open Access | ||
Notes | The authors gratefully acknowledge the financial support of the French National Research Agency (ANR) through the OPTIMUM ANR- 14-CE27-0017 project. The authors would also like to thank the Hautsde- France Region and the European Regional Development Fund (ERDF) 2014/2020 for the co-funding of this work. The authors would also like to thank ACB for providing LFW samples as well as Airbus for their technical support. | Approved | Most recent IF: 2.714 | ||
Call Number | EMAT @ emat @c:irua:165084 | Serial | 5441 | ||
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Author | Wang, X.; Li, K.; Schryvers, D.; Verlinden, B.; Van Humbeeck, J. | ||||
Title | R-phase transition and related mechanical properties controlled by low-temperature aging treatment in a Ti50.8 at.% Ni thin wire | Type | A1 Journal article | ||
Year | 2014 | Publication | Scripta materialia | Abbreviated Journal | Scripta Mater |
Volume | 72-73 | Issue | Pages | 21-24 | |
Keywords | A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT) | ||||
Abstract | A cold-drawn Ti50.8 at.% Ni wire was annealed at 600 °C for 30 min, followed by aging at 250 °C for different times. A microstructure with small grains and nanoscaled precipitates was obtained. The thermally induced martensite transformation is suppressed in the samples aged for 4 h or longer, leaving a one-stage R-phase transition between −150 and +150 °C. The transformation behavior, work output and recovery stress associated with the R-phase transition are presented. | ||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Oxford | Editor | ||
Language | Wos | 000329148500006 | Publication Date | 2013-10-17 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1359-6462; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.747 | Times cited | 27 | Open Access | |
Notes | Fwo | Approved | Most recent IF: 3.747; 2014 IF: 3.224 | ||
Call Number | UA @ lucian @ c:irua:111847 | Serial | 2806 | ||
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Author | Oleshko, V.; Schryvers, D.; Gijbels, R.; Jacob, W. | ||||
Title | Investigation of Ag, Ag2S and Ag(Br,I) small particles by HREM and AEM | Type | H3 Book chapter | ||
Year | 1998 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | 293-294 | ||
Keywords | H3 Book chapter; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | s.l. | Editor | ||
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:20553 | Serial | 1729 | ||
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Author | Potapov, P.L.; Kulkova, S.E.; Schryvers, D.; Verbeeck, J. | ||||
Title | Structural and chemical effects on EELS L3,2 ionization edges in Ni-based intermetallic compounds | Type | A1 Journal article | ||
Year | 2001 | Publication | Physical review : B : condensed matter and materials physics | Abbreviated Journal | Phys Rev B |
Volume | 64 | Issue | Pages | 184110,1-9 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Lancaster, Pa | Editor | ||
Language | Wos | 000172239400038 | Publication Date | 2002-07-27 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1098-0121;1550-235X; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.836 | Times cited | 44 | Open Access | |
Notes | Approved | Most recent IF: 3.836; 2001 IF: NA | |||
Call Number | UA @ lucian @ c:irua:48393 | Serial | 3192 | ||
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Author | Cautaerts, N.; Delville, R.; Schryvers, D. | ||||
Title | ALPHABETA: a dedicated open-source tool for calculating TEM stage tilt angles | Type | A1 Journal article | ||
Year | 2019 | Publication | Journal of microscopy | Abbreviated Journal | J Microsc-Oxford |
Volume | 273 | Issue | 3 | Pages | 189-198 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Editor | |||
Language | Wos | 000458426100004 | Publication Date | 2018-12-24 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0022-2720 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 1.692 | Times cited | 2 | Open Access | Not_Open_Access |
Notes | ENGIE Ph.D. sponsorship, 2015-AC-007 – BSUEZ6900 ; | Approved | Most recent IF: 1.692 | ||
Call Number | EMAT @ emat @UA @ admin @ c:irua:157474 | Serial | 5163 | ||
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Author | Cao, S.; Tirry, W.; Schryvers, D. | ||||
Title | 3D reconstruction of a Ni51Ti49 alloy with precipitates by FIB-SEM alice-and-view | Type | A3 Journal article | ||
Year | 2007 | Publication | Materia Japan | Abbreviated Journal | |
Volume | 46 | Issue | Pages | 803-804 | |
Keywords | A3 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Editor | |||
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:67711 | Serial | 15 | ||
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Author | Schryvers, D. | ||||
Title | Advanced TEM studies of martensite and related phase transformations | Type | H1 Book chapter | ||
Year | 1999 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | 947-956 | ||
Keywords | H1 Book chapter; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | s.l. | Editor | ||
Language | Wos | 000086479100208 | Publication Date | 0000-00-00 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record; WoS full record; | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:48373 | Serial | 76 | ||
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Author | Yang, Z.; Tirry, W.; Schryvers, D. | ||||
Title | Analytical TEM investigations on concentration gradients surrounding Ni4Ti3 precipitates in Ni-Ti shape memory material | Type | A1 Journal article | ||
Year | 2005 | Publication | Scripta materialia | Abbreviated Journal | Scripta Mater |
Volume | 52 | Issue | 11 | Pages | 1129-1134 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Oxford | Editor | ||
Language | Wos | 000228190200010 | Publication Date | 2005-03-16 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 1359-6462; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.747 | Times cited | 49 | Open Access | |
Notes | GOA project; MCRTN-FP6-505226 Multimat | Approved | Most recent IF: 3.747; 2005 IF: 2.228 | ||
Call Number | UA @ lucian @ c:irua:55687 | Serial | 110 | ||
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Author | Fredrickx, P.; Wouters, J.; Schryvers, D. | ||||
Title | The application of transmission electron microscopy (TEM) in the research of inorganic colorants in stained glass windows and parchment illustrations | Type | H3 Book chapter | ||
Year | 2003 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | 137-143 | ||
Keywords | H3 Book chapter; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Archetype | Place of Publication | London | Editor | |
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:48779 | Serial | 144 | ||
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Author | Schryvers, D.; Potapov, P.; Santamarta, R.; Tirry, W. | ||||
Title | Applications of advanced transmission electron microscopic techniques to Ni-Ti based shape memory materials | Type | A1 Journal article | ||
Year | 2004 | Publication | Materials science and engineering: part A: structural materials: properties, microstructure and processing | Abbreviated Journal | Mat Sci Eng A-Struct |
Volume | 378 | Issue | 1/2 | Pages | 11-15 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Lausanne | Editor | ||
Language | Wos | 000223329900003 | Publication Date | 2004-03-23 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0921-5093; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.094 | Times cited | 6 | Open Access | |
Notes | Approved | Most recent IF: 3.094; 2004 IF: 1.445 | |||
Call Number | UA @ lucian @ c:irua:48783 | Serial | 145 | ||
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Author | Pauwels, B.; Yandouzi, M.; Schryvers, D.; Van Tendeloo, G.; Verschoren, G.; Lievens, P.; Hou, M.; van Swygenhoven, H. | ||||
Title | Atomic scale characterization of supported and assembled nanoparticles | Type | P3 Proceeding | ||
Year | 2001 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | B8.3,1-6 | ||
Keywords | P3 Proceeding; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | s.l. | Editor | ||
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:48390 | Serial | 181 | ||
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Author | Zhurkin, E.; Hou, M.; van Swygenhoven, H.; Pauwels, B.; Yandouzi, M.; Schryvers, D.; Van Tendeloo, G.; Lievens, P.; Verschoren, G.; Kuriplach, J.; van Peteghem, S.; Segers, D.; Dauwe, C. | ||||
Title | Atomic scale modeling of supported and assembled nanoparticles | Type | P3 Proceeding | ||
Year | 2001 | Publication | Abbreviated Journal | ||
Volume | Issue | Pages | B8.2,1-6 | ||
Keywords | P3 Proceeding; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | s.l. | Editor | ||
Language | Wos | Publication Date | 0000-00-00 | ||
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:48391 | Serial | 186 | ||
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Author | Van Tendeloo, G.; Schryvers, D. | ||||
Title | Atomic structure of alloys close to phase transitions | Type | A1 Journal article | ||
Year | 2000 | Publication | Nucleation and growth processes in materials | Abbreviated Journal | |
Volume | 580 | Issue | Pages | 283-292 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Editor | |||
Language | Wos | 000165506200043 | Publication Date | 0000-00-00 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | ISBN | Additional Links | UA library record; WoS full record; | ||
Impact Factor | Times cited | Open Access | |||
Notes | Approved | Most recent IF: NA | |||
Call Number | UA @ lucian @ c:irua:48377 | Serial | 197 | ||
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Author | Schryvers, D.; Holland-Moritz, D. | ||||
Title | Austenite and martensite microstructures in splat-cooled Ni-Al | Type | A1 Journal article | ||
Year | 1998 | Publication | Intermetallics | Abbreviated Journal | Intermetallics |
Volume | 6 | Issue | Pages | 427-436 | |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT) | ||||
Abstract | |||||
Address | |||||
Corporate Author | Thesis | ||||
Publisher | Place of Publication | Chicago, Ill. | Editor | ||
Language | Wos | 000074235500010 | Publication Date | 2002-07-25 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0966-9795; | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 3.14 | Times cited | 13 | Open Access | |
Notes | Approved | Most recent IF: 3.14; 1998 IF: 1.785 | |||
Call Number | UA @ lucian @ c:irua:48365 | Serial | 209 | ||
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