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Author |
Rouchon, V.; Pellizzi, E.; Duranton, M.; Vanmeert, F.; Janssens, K. |
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Title |
Combining XANES, ICP-AES, and SEM/EDS for the study of phytate chelating treatments used on iron gall ink damaged manuscripts |
Type |
A1 Journal article |
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Year |
2011 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
J Anal Atom Spectrom |
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Volume |
26 |
Issue |
12 |
Pages |
2434-2441 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Many historical documents written with iron gall inks are endangered by the corrosive effects of these inks. In this work, a combination of complementary analytical methods was used for the first time in order to study the phytate process which is used in conservation studios to stabilize damaged manuscripts. This process consists of an antioxidant treatment performed by means of a calcium phytate (CP) solution, followed by a deacidification treatment performed with a calcium carbonate (CC) solution. The antioxidant treatment capitalizes on the properties of myo-inositol hexaphosphoric acid (phytic acid) that inhibits iron through chelation. In order to use relatively low acidic solutions, the pH of the CP solution is increased up to values between 5 and 6, which is in the range of the CP precipitation threshold. This study was performed on laboratory samples made of paper impregnated with iron gall ink and artificially aged in climatic chambers. It aims to investigate how the CP precipitate impacts the efficiency of the treatment. Side effects, such as elemental losses and deposits, were measured by means of several analytical techniques (FeK Edge XANES, SEM/EDS, and ICP-AES). These measurements were crosschecked with a ready to use colour spot test made of bathophenanthroline impregnated paper. It appeared that the CP treatment should necessarily be followed by the deacidification treatment in order to achieve long term stability. The precipitation of CP in the treating solution does finally not impact the efficiency of the treatment despite the fact that it should theoretically lower the availability of phytate to chelate iron. A scenario is proposed to explain this point. |
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Wos |
000297030400008 |
Publication Date |
2011-10-06 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0267-9477 |
ISBN |
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Additional Links  |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.379 |
Times cited |
10 |
Open Access |
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Notes |
; This research was funded by SOLEIL (proposals 20060396 and 20080761) and was supported by the Interuniversity Attraction Poles Programme-Belgian Science Policy (IUAP VI/16). The text also presents results of GOA “XANES meets ELNES” (Research Fund University of Antwerp, Belgium) and from FWO (Brussels, Belgium) projects no. G.0704.08 and G.01769.09. We are thankful to the paper conservator students of the Institut National du Patrimoine who were involved in some of the sample preparations, and to Dr Dominique Thiaudiere and Dr Solenn Reguer for their assistance and help during the experiments performed at SOLEIL beamline “DIFFABS”. ; |
Approved |
Most recent IF: 3.379; 2011 IF: 3.220 |
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Call Number |
UA @ admin @ c:irua:93845 |
Serial |
5527 |
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Author |
Cagno, S.; Nuyts, G.; Bugani, S.; De Vis, K.; Schalm, O.; Caen, J.; Helfen, L.; Cotte, M.; Reischig, P.; Janssens, K. |
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Title |
Evaluation of manganese-bodies removal in historical stained glass windows via SR-\mu-XANES/XRF and SR-\mu-CT |
Type |
A1 Journal article |
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Year |
2011 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
J Anal Atom Spectrom |
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Volume |
26 |
Issue |
12 |
Pages |
2442-2451 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The speed and effectiveness of a conservation treatment used for stained glass windows have been investigated. Dark-coloured Mn-rich stains can be found in the alteration layer of ancient glass artefacts and cause the surface to turn brown/black: this phenomenon is known as Mn-browning or Mn-staining. While in glass manganese is present in the +II or +III oxidation states, in the Mn-rich bodies, manganese is in a higher oxidation state (+IV). In restoration practice, mildly reducing solutions are employed to eliminate the dark colour and restore the clear appearance of the glass. In this paper the effectiveness and side effects of the use of hydroxylamine hydrochloride for this purpose are assessed. Archaeological fragments of stained glass windows, dated to the 14th century and originating from Sidney Sussex College, Cambridge (UK), were examined by means of synchrotron radiation (SR) based microscopic X-ray Absorption Near-Edge Spectroscopy (μ-XANES) and microscopic X-Ray Fluorescence (μ-XRF) and with high resolution computed absorption tomography (μ-CT) before, during and after the treatment. The monitoring of the glass fragments during the treatment allows us to better understand the manner in which the process unfolds and its kinetics. The results obtained reveal that the hydroxylamine hydrochloride treatment is effective, but also that it has a number of unwanted side effects. These findings are useful for optimizing the time and other modalities of the Mn-reducing treatment as well as minimizing its unwanted results. |
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Wos |
000297030400009 |
Publication Date |
2011-10-11 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0267-9477 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.379 |
Times cited |
17 |
Open Access |
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Notes |
; This research was supported by the Interuniversity Attraction Poles Programme-Belgian Science Policy (IUAP VI/16). The text also presents results of GOA “XANES meets ELNES” (Research Fund University of Antwerp, Belgium) and from FWO (Brussels, Belgium) projects no. G.0704.08 and G.01769.09. Special thanks to Ms Leonie Seliger, head of the stained-glass conservation studio (The Cathedral Studios-The Chapter of Canterbury Cathedral) for the supply of the archaeological samples. The authors gratefully acknowledge ESRF for granting beamtime (proposal EC-602). ; |
Approved |
Most recent IF: 3.379; 2011 IF: 3.220 |
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Call Number |
UA @ admin @ c:irua:93848 |
Serial |
5613 |
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Author |
Horemans, B. |
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Title |
Chemical characterization of particulate air pollutants : case studies on indoor air quality, cultural heritage and the marine environment |
Type |
Doctoral thesis |
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Year |
2012 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
229 p. |
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Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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no |
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Call Number |
UA @ admin @ c:irua:94360 |
Serial |
7649 |
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Author |
Krupińska, B.; Worobiec, A.; Rotondo, G.G.; Novaković, V.; Kontozova, V.; Ro, C.-U.; Van Grieken, R.; De Wael, K. |
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Title |
Assessment of the air quality (NO2, SO2, O3 and particulate matter) in the Plantin-Moretus Museum/Print Room in Antwerp, Belgium, in different seasons of the year |
Type |
A1 Journal article |
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Year |
2012 |
Publication |
Microchemical journal |
Abbreviated Journal |
Microchem J |
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Volume |
102 |
Issue |
1 |
Pages |
49-53 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Abstract |
The Plantin-Moretus Museum/Print Room in Antwerp, Belgium, gathers one of the most precious collections of typographical material and old printed books in the world. Rich decorations of this former printing-house and the history of the building itself underline its uniqueness. The cultural heritage (CH) objects collected in the museum, in particular books and manuscripts are vulnerable to the atmospheric pollution and can be irreversibly damaged. To assess the air quality inside the museum, four consecutive sampling campaigns were performed in each season of the year. The gas monitoring of nitrogen dioxide (NO2), sulphur dioxide (SO2) and ozone (O3) was carried out outside the building, in galleries and in showcases by means of using diffusive samplers. The particulate matter (PM) was collected in bulk form and as single particles and then analysed with use of energy dispersive X-ray fluorescence (EDXRF) and electron probe micro-analyser (EPMA), respectively. The museum complex turned out to show good protection against gaseous pollutants, especially SO2 and O3. The concentrations of these pollutants were significantly reduced inside the building in comparison to the outdoor ones. Similar protective character of the museum complex was established in case of the coarse fraction of PM; however with some limitations. Single particle analysis showed that the relative abundance of carbon-rich particles inside the museum was greater than outside. Moreover, these particles contributed more to the fine fraction of PM than to the coarse fraction. Therefore, for better preservation of cultural heritage, special attention should be paid to the small particles and their distribution within the museum. |
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Wos |
000301559100007 |
Publication Date |
2011-11-22 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0026-265x; 0026-265x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.034 |
Times cited |
25 |
Open Access |
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Notes |
; The presented work was realised in the frame of the project Preventive conservation/preservation in the museum Plantin-Moretus/Prentenkabinet, Antwerp, financed by the Flemish Government. Special thanks are due to Mrs Hanne Moris and Mrs Elke van Herck and all the staff of the Museum Plantin-Moretus/Print Room in Antwerp for their sincere interest in this work and their eager assistance during all the sampling campaigns. Barbara Krupinska is supported as PhD student by the Flemish Fund for Scientific Research (FWO, Belgium). ; |
Approved |
Most recent IF: 3.034; 2012 IF: 2.879 |
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Call Number |
UA @ admin @ c:irua:94466 |
Serial |
5483 |
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Author |
Bugani, S.; Modugno, F.; Lucejko, J.J.; Giachi, G.; Cagno, S.; Cloetens, P.; Janssens, K.; Morselli, L. |
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Title |
Study on the impregnation of archaeological waterlogged wood with consolidation treatments using synchrotron radiation microtomography |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Analytical and bioanalytical chemistry |
Abbreviated Journal |
Anal Bioanal Chem |
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Volume |
395 |
Issue |
7 |
Pages |
1977-1985 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
In favourable conditions of low temperature and low oxygen concentration, archaeological waterlogged wooden artefacts, such as shipwrecks, can survive with a good state of preservation. Nevertheless, anaerobic bacteria can considerably degrade waterlogged wooden objects with a significant loss in polysaccharidic components. Due to these decay processes, wood porosity and water content increase under ageing. In such conditions, the conservation treatments of archaeological wooden artefacts often involve the replacement of water with substances which fill the cavities and help to prevent collapse and stress during drying. The treatments are very often expensive and technically difficult, and their effectiveness very much depends on the chemical and physical characteristics of the substances used for impregnation. Also important are the degree of cavity-filling, penetration depth and distribution in the structure of the wood. In this study, the distribution in wood cavities of some mixtures based on polyethylene glycols and colophony, used for the conservation of waterlogged archaeological wood, was investigated using synchrotron radiation X-ray computed microtomography (SR-A mu CT). This non-destructive imaging technique was useful for the study of the degraded waterlogged wood and enabled us to visualise the morphology of the wood and the distribution of the materials used in the wood treatments. The study has shown how deposition is strictly related to the dimension of the wooden cavities. The work is currently proceeding with the comparison of synchrotron observations with the data of the solutions viscosity and with those of the properties imparted to the wood by the treatments. |
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Wos |
000272017000005 |
Publication Date |
2009-09-16 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1618-2642 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.431 |
Times cited |
30 |
Open Access |
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Notes |
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Approved |
Most recent IF: 3.431; 2009 IF: 3.480 |
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Call Number |
UA @ admin @ c:irua:94493 |
Serial |
5853 |
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Author |
van der Linden, V.; Cosyns, P.; Schalm, O.; Cagno, S.; Nys, K.; Janssens, K.; Nowak, A.; Wagner, B.; Bulska, E. |
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Title |
Deeply coloured and black glass in the Northern provinces of the Roman Empire : differences and similarities in chemical composition before and after AD 150 |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Archaeometry |
Abbreviated Journal |
Archaeometry |
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Volume |
51 |
Issue |
5 |
Pages |
822-844 |
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Keywords |
A1 Journal article; History; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
In this work we attempt to elucidate the chronological and geographical origin of deeply coloured and black glass dating between 100 bc and ad 300 on the basis of their major and trace element compositions. Samples from the western and eastern parts of the Roman Empire were analysed. Analytical data were obtained by means of a scanning electron microscope – energy-dispersive system (SEM-EDS, 63 samples analysed) and laser ablation – inductively coupled plasma – mass spectrometry (LA-ICP-MS, 41 samples analysed). Among the glass fragments analysed, dark brown, dark purple and dark green hues could be distinguished. Only among the dark green fragments could a clear compositional distinction be observed between fragments dated to the periods before and after ad 150. In the early samples (first century bc to first century ad), iron, responsible for the green hue, was introduced by using impure sand containing relatively high amounts of Ti. In contrast, a Ti-poor source of iron was employed, containing Sb, Co and Pb in trace quantities, in order to obtain the dark green colour in the later glass samples. The analytical results obtained by combining SEM-EDS and LA-ICP-MS are therefore consistent with a differentiation of glassmaking recipes, detectable in glass composition, occurring in the period around ad 150. |
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Wos |
000269728600009 |
Publication Date |
2008-11-27 |
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Abbreviated Series Title |
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Edition |
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ISSN |
0003-813x; 1475-4754 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
1.47 |
Times cited |
39 |
Open Access |
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Notes |
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Approved |
Most recent IF: 1.47; 2009 IF: 1.355 |
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Call Number |
UA @ admin @ c:irua:94510 |
Serial |
5568 |
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Author |
Karabidak, S.M.; Čevik, U.; Kaya, S. |
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Title |
A new method to compensate for counting losses due to system dead time |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Nuclear instruments and methods in physics research : A: accelerators, spectrometers, detectors and associated equipment |
Abbreviated Journal |
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Volume |
603 |
Issue |
3 |
Pages |
361-364 |
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Keywords |
A1 Journal article; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Determination of count losses and pile-up pulse effects in quantitative and qualitative analysis became a vital step in various analyses. Therefore, compensating for counting losses is of importance. These counting losses are due to the pulse pile-up, paralyzable and non-paralyzable system dead time or a combination of these mechanisms. In this work, a new method is suggested for the correction of dead time losses resulting from the above mechanisms. For this purpose, a source code was developed. It was found that the peaking time was an important parameter over system dead time. The method suggested seems to be more effective even at high count rate. (C) 2009 Elsevier B.V. All rights reserved. |
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Wos |
000266829400021 |
Publication Date |
2009-02-14 |
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Abbreviated Series Title |
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Edition |
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ISSN |
0168-9002 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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no |
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Call Number |
UA @ admin @ c:irua:94550 |
Serial |
8304 |
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Author |
Celik, N.; Čevik, U.; Celik, A.; Koz, B. |
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Title |
Natural and artificial radioactivity measurements in Eastern Black Sea region of Turkey |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Journal of hazardous materials |
Abbreviated Journal |
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Volume |
162 |
Issue |
1 |
Pages |
146-153 |
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Keywords |
A1 Journal article; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
In the present work, naturally occurring radionuclides of (226)Ra, (232)Th and (40)K were measured in soil samples collected from the Eastern Black Sea region of Turkey. It was found that the activity concentrations ranged from 12 to 120 Bq kg(-1) for (226)Ra, from 13 to 121 Bq kg(-1) for (232)Th and from 204 to 1295 Bq kg(-1) for (40)K. Besides naturally occurring radionuclides, (137)Cs activity concentration was measured in soil, lichen and moss samples and it was found that (137)Cs activity concentration ranged from 27 to 775 Bq kg(-1) with for soil, from 29 to 879 Bq kg(-1) for lichen and from 67 to 1396 Bq kg(-1) for moss samples. Annual effective doses due to the naturally occurring radionuclides and (137)CS were estimated. Ecological half-lives of (137)CS in lichen and moss species were estimated. The decrease of the activity concentrations in the present measurements (2007) relative to those in 1993 indicated ecological half-lives between 1.36 and 2.96 years for lichen and between 1.35 and 2.85 years for moss species. (C) 2008 Elsevier B.V. All rights reserved. |
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Wos |
000263149400019 |
Publication Date |
2008-05-10 |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
0304-3894 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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no |
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Call Number |
UA @ admin @ c:irua:94562 |
Serial |
8296 |
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Author |
Baltas, H.; Čevik, U. |
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Title |
Variation of K X-ray fluorescence cross-sections of Cu, Y and Ba in YBa2Cu3O7-\delta superconductor |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Solid state communications |
Abbreviated Journal |
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Volume |
149 |
Issue |
5/6 |
Pages |
231-235 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
K X-ray fluorescence cross-sections of Cu, Y and Ba elements were measured in CuO, Y(2)O(3), BaCO(3) Compounds and YBa(2)Cu(3)O(7-delta) superconductor samples (nonreacted agent, calcined and sintered states). A superconductor sample of YBa(2)Cu(3)O(7-delta) was prepared by using a solid-state reaction technique. The samples were excited by gamma rays of energy 59.5 keV from a (241)Am radioisotope source. The Cu, Y and Ba K X-ray intensities counted with a Si(Li) detector were measured in different solid-state conditions. The obtained values of K X-ray fluorescence cross-section were compared with the theoretical values of pure Cu, Y and Ba elements. We found that the K X-ray fluorescence cross-section of Cu, Y and Ba in YBa(2)Cu(3)O(7-delta) sample is changed in different solid-state conditions, depending on the mixture (nonreacted agent), calcined and sintered states. (c) 2008 Elsevier Ltd. All rights reserved. |
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Place of Publication |
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Wos |
000262795900013 |
Publication Date |
2008-11-21 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0038-1098 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:94568 |
Serial |
8735 |
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Author |
Kabsch-Korbutowicz, M.; Kozak, A.; Krupińska, B. |
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Title |
Ion exchange-ultrafiltration integrated process as a useful method in removing natural organic matter from water |
Type |
A1 Journal article |
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Year |
2008 |
Publication |
Environment protection engineering |
Abbreviated Journal |
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Volume |
34 |
Issue |
2 |
Pages |
79-93 |
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Keywords |
A1 Journal article; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The experiments conducted are focused on natural organic substances, removal from water in ion-exchange process, ultrafiltration process and ion exchange-ultrafiltration integrated process. The water from the Odra River and model solution were investigated. In treatment processes, various doses of 5 anion-exchange resins as well as polyethersulphone membranes with different cut-offs were used. The efficiency of process was determined by measuring a decrease both in the colour intensity and the UV 254 nm absorbance. The results show that separation efficiency in integrated process depends on resin dose added to water before ultrafiltration and on the membrane cut-off as well. Among the resins tested the most efficient was MIEX (R) resin. The ion-exchange process carried out prior to the ultrafiltration increased, especially for high cut-off membranes, NOM retention and resulted in the decrease of membrane fouling intensity. |
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Place of Publication |
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Wos |
000257186600008 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0324-8828 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:94633 |
Serial |
8131 |
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| Permanent link to this record |
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| |
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Author |
Ajtony, Z.; Szoboszlai, N.; Bella, Z.; Bolla, S.; Szakál, P.; Bencs, L. |
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| |
Title |
Determination of total selenium content in cereals and bakery products by flow injection hydride generation graphite furnace atomic absorption spectrometry applying in-situ trapping on iridium-treated graphite platforms |
Type |
A1 Journal article |
| |
Year |
2005 |
Publication |
Microchimica acta |
Abbreviated Journal |
|
|
| |
Volume |
150 |
Issue |
1 |
Pages |
1-8 |
|
| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
A flow injection hydride generation graphite furnace atomic absorption spectrometric (FI-HG-GFAAS) method was applied to the determination of Se in Se-doped and undoped cereals and bakery products. For the purpose of doping, the soils used for the cultivation of the cereals were dosed with Se- doped foliar fertilizers. The samples were dissolved in a mixture of HNO(3) and H(2)O(2) solutions using micro-waveassisted digestion. The decomposition of H(2)Se generated from the sample solutions and the trapping of elemental Se were performed at a temperature of 300 degrees C on an Ir-pretreated integrated graphite platform of a transversally heated graphite atomizer(THGA). For release of the trapped Se within a fairly short atomization time (5s), an atomization temperature of 2200 degrees C was observed to be optimal. The overall efficiency of hydride generation, transport and trapping was similar to 86%. The upper limit of the linear dynamic range of calibration was 10 mu gL(-1), which corresponds to 0.5 mu g g(-1) for solid samples. Recovery of the samples spiked with Se(VI) solutions was found to be 93 +/- 6% on average. The relative standard deviation of the determinations was less than 8%. The limit of detection was found to be 0.06 mu gL(-1), corresponding to 3 ng g(-1) for solid samples. The accuracy of the method was verified with the use of IAEA-155 ( whey powder) certified reference material. End-capped THGA tubes resulted in an extension of the linear calibration range compared to that of standard THGAs. The Se content in bakery products made of undoped cereals ranged from 7.7 to 68 ng g(-1) ( wet weight) in 18 samples, whereas the Se content of the corresponding cereals was found to be below 100 ng g(-1) ( wet weight). The Se level of cereals grown on soils treated with Se- doped fertilizers ranged from 128 to 1046 ng g(-1) ( wet weight), and it depended linearly on the Se concentration of the corresponding foliar fertilizer. |
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Wos |
000229219900001 |
Publication Date |
2005-03-28 |
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| |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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| |
Series Volume |
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Series Issue |
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Edition |
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| |
ISSN |
0026-3672; 1436-5073 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:94727 |
Serial |
7791 |
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| Permanent link to this record |
| |
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| |
|
Author |
Vincze, L.; Vekemans, B.; Szaloki, I.; Brenker, F.E.; Falkenberg, G.; Rickers, K.; Aerts, K.; Van Grieken, R.; Adams, F. |
|
| |
Title |
X-ray fluorescence microtomography and polycapillary based confocal imaging using synchrotron radiation |
Type |
P1 Proceeding |
| |
Year |
2004 |
Publication |
|
Abbreviated Journal |
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| |
Volume |
|
Issue |
|
Pages |
220-231
T2 - 4th Conference on Developments in X-R |
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| |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
Ibis work illustrates the development of X-ray fluorescence tomography and polycapillary based confocal imaging towards a three-dimensional (313), quantitative analytical method with lateral resolution levels down to the 2-20 mum scale. Detailed analytical characterization is given for polycapillary based confocal XRF imaging, which is a new variant of the 3D micro-XRF technique. Applications for 2D/3D micro-XR-F are illustrated for the analysis of biological (zooplankton) and geological samples (microscopic inclusions in natural diamonds and fluid inclusions in quartz). Based on confocal imaging, fully three-dimensional distributions of trace elements could be obtained, representing a significant generalization of the regular 2D scanning technique for micro-XRF spectroscopy. The experimental work described in this paper has been carried out at the ESRF ID18F microfluorescence end-station and at HASYLAB Beam Line L. |
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Corporate Author |
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Wos |
000225665000023 |
Publication Date |
2004-11-02 |
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| |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
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| |
ISSN |
0-8194-5473-7 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:94812 |
Serial |
8767 |
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| Permanent link to this record |
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| |
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Author |
Kindratenko, V.V.; van Espen, P.J.M.; Treiger, B.A.; Van Grieken, R.E. |
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| |
Title |
Fractal dimensional classification of aerosol particles by computer-controlled scanning electron microscopy |
Type |
A1 Journal article |
| |
Year |
1994 |
Publication |
Environmental science and technology |
Abbreviated Journal |
|
|
| |
Volume |
28 |
Issue |
|
Pages |
2197-2202 |
|
| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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| |
Abstract |
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| |
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Language |
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Wos |
A1994PP82900033 |
Publication Date |
2007-05-30 |
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| |
Series Editor |
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Series Title |
|
Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
|
| |
ISSN |
0013-936x; 1520-5851 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
|
|
| |
Notes |
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Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:9497 |
Serial |
7983 |
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| Permanent link to this record |
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| |
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Author |
Treiger, B.; Injuk, J.; Bondarenko, I.; van Espen, P.; Van Grieken, R.; Breitenbach, L.; Wätjen, U. |
|
| |
Title |
Non-linear mapping of microbeam proton-induced X-ray emission data for source identification of North Sea aerosols |
Type |
A1 Journal article |
| |
Year |
1994 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
|
|
| |
Volume |
49 |
Issue |
4 |
Pages |
345-353 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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| |
Abstract |
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| |
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1994NM41200004 |
Publication Date |
2003-04-25 |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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|
| |
Series Volume |
|
Series Issue |
|
Edition |
|
|
| |
ISSN |
0584-8547; 1873-3565 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
|
Open Access |
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|
| |
Notes |
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Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:9500 |
Serial |
8314 |
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| Permanent link to this record |
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| |
|
Author |
van Put, A.; Vertes, A.; Wegrzynek, D.; Treiger, B.; Van Grieken, R. |
|
| |
Title |
Quantitative characterization of individual particle surfaces by fractal analysis of scanning electron microscope images |
Type |
A1 Journal article |
| |
Year |
1994 |
Publication |
Fresenius' journal of analytical chemistry |
Abbreviated Journal |
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|
| |
Volume |
350 |
Issue |
|
Pages |
440-447 |
|
| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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| |
Abstract |
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| |
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1994PR64400005 |
Publication Date |
2004-10-19 |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
|
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| |
ISSN |
0937-0633; 1432-1130 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
|
Open Access |
|
|
| |
Notes |
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Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:9505 |
Serial |
8442 |
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| Permanent link to this record |
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| |
|
Author |
Van Grieken, R.; de Bruin, M. |
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| |
Title |
Nomenclature for radioanalytical chemistry (IUPAC Recommendations 1994) |
Type |
A1 Journal article |
| |
Year |
1994 |
Publication |
Pure and applied chemistry |
Abbreviated Journal |
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| |
Volume |
66 |
Issue |
12 |
Pages |
2513-2526 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
Nearly 200 terms commonly used in radioanalytical chemistry are unambiguously defined. The list is partially based on an earlier IUPAC-glossary (Pure Appl. Chem. 54 (1982) 1533-1554), but some modifications have been made, terms related to nuclear physics and technology have not been reconsidered and numerous new entries from the realm of radiometric analysis, radioimmunoassay and related techniques have been included. |
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Corporate Author |
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Place of Publication |
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Language |
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Wos |
A1994PZ23000010 |
Publication Date |
2007-10-23 |
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| |
Series Editor |
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Series Title |
|
Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
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ISSN |
0033-4545 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
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Times cited |
|
Open Access |
|
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9506 |
Serial |
8312 |
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| Permanent link to this record |
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| |
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Author |
Wonders, J.H.A.M.; Houweling, S.; de Bont, F.A.J.; van Leeuwen, H.P.; Eeckhaoudt, S.M.; Van Grieken, R. |
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| |
Title |
Characterization of aerosol-associated lead by DPASV and LAMMA |
Type |
A1 Journal article |
| |
Year |
1994 |
Publication |
International journal of environmental analytical chemistry |
Abbreviated Journal |
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| |
Volume |
56 |
Issue |
|
Pages |
193-205 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1994PF99800002 |
Publication Date |
2007-07-07 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
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Edition |
|
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ISSN |
0306-7319 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
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Times cited |
|
Open Access |
|
|
| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9514 |
Serial |
7611 |
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| Permanent link to this record |
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| |
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Author |
van Malderen, H.; Van Grieken, R.; Khodzher, T.V.; Bufetov, N.S.; Koutsenogii, K.P. |
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| |
Title |
Analysis of individual aerosol particles in Siberian region: provisional results |
Type |
A3 Journal article |
| |
Year |
1994 |
Publication |
Atmospheric and oceanic optics |
Abbreviated Journal |
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| |
Volume |
7 |
Issue |
|
Pages |
622-627 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9515 |
Serial |
7445 |
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| Permanent link to this record |
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| |
|
Author |
Cholewa, M.; Legge, G.J.F.; Eeckhaoudt, S.; Van Grieken, R. |
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| |
Title |
A study of aluminium-exposed fish using a scanning proton microprobe |
Type |
P3 Proceeding |
| |
Year |
1994 |
Publication |
Proceedings of the Australian Conference on Nuclear Techniques of Analysis |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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| |
Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9517 |
Serial |
8594 |
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| Permanent link to this record |
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| |
|
Author |
Struyf, H.; van Roy, W.; Van Vaeck, L.; Van Grieken, R.; Caravatti, P. |
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| |
Title |
The feasibility of Fourier transform laser microprobe mass spectrometry for applications of local and surface analysis |
Type |
P3 Proceeding |
| |
Year |
1994 |
Publication |
Proceedings of the European FTMS Workshop |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Wos |
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Publication Date |
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Series Editor |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
|
Open Access |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9520 |
Serial |
7961 |
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| Permanent link to this record |
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| |
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Author |
Van Grieken, R.; de Bock, L.; Injuk, J.; van Malderen, H. |
|
| |
Title |
Atmospheric deposition of heavy metals in the North Sea as studied by micro- and trace analysis |
Type |
H3 Book chapter |
| |
Year |
1994 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
|
Pages |
284-286
T2 - Environmental contamination / Varnava |
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| |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Wos |
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Publication Date |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9521 |
Serial |
7525 |
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| Permanent link to this record |
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Author |
Wegrzynek, D.; Van Grieken, R.; Eisma, D. |
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| |
Title |
Particle analysis of sediments from the Gulf of Lions, suspended matter from the Rhone river, and Sahara dust |
Type |
H3 Book chapter |
| |
Year |
1994 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
51-60
T2 - Particles and particle-water interactio |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Wos |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9525 |
Serial |
8358 |
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| Permanent link to this record |
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Author |
van Malderen, H.; Van Grieken, R.; Khodzher, T.V.; Grachev, M.; Bufetov, N.S.; Koutsenogii, K.P. |
|
| |
Title |
Single particle analysis of aerosols from Siberia |
Type |
P3 Proceeding |
| |
Year |
1994 |
Publication |
Proceedings of the Russian-Ukrainian-Austrian-German Analytical Symposium |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Wos |
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Series Editor |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
|
ISBN |
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Additional Links |
UA library record |
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| |
Impact Factor |
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Times cited |
|
Open Access |
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|
| |
Notes |
|
Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:9527 |
Serial |
8530 |
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| Permanent link to this record |
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| |
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Author |
Vazquez, C.; Martin Palacios, O.; Darchuk, L.; Marco Parra, L.-M. |
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| |
Title |
Compositional study of prehistoric pigments (Carriqueo rock shelter, Argentina) by synchrotron radiation X-ray diffraction |
Type |
A1 Journal article |
| |
Year |
2010 |
Publication |
Powder diffraction |
Abbreviated Journal |
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| |
Volume |
25 |
Issue |
3 |
Pages |
264-269 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
In this work synchrotron radiation X-ray diffraction technique was successfully applied for the analysis of pigments found in excavation at Carriqueo rock shelter, Neuquen, Argentina. The pigment samples of orange, red, and brown shades were collected from different levels of this archaeological site and compared with a suspected source of provenance (La Oficina creek). X-ray diffraction patterns of several yellowish, reddish, and red pigments showed the presence of haematite, goethite, kaolinite, and quartz. The majority of Carriqueo collected samples belonged to the same group of the suspected source, having haematite and quartz as main crystalline phases. The results indicate that the raw material from La Oficina is the source of most of the pigments found at Carriqueo. The present work helps us to understand the strategy of supplying raw materials by human groups in the North Patagonia region. (C) 2010 International Centre for Diffraction Data. [DOI: 10.1154/1.3478884] |
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Wos |
000282386500009 |
Publication Date |
2010-09-15 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0885-7156 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:95582 |
Serial |
7717 |
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Author |
Van Grieken, R.; Jaenicke, R.; Koutsenogii, K.P.; Khodzher, T.V.; Kulipanov, G.N. |
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Title |
Atmospheric aerosols in the Asian part of the former Soviet Union |
Type |
P1 Proceeding |
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Year |
2000 |
Publication |
AIP conference proceedings
T2 – 15th International Conference on Nucleation and Atmospheric Aerosols, (ICNAA), August 06-11, 2000, Univ. Missouri Rolla, Rolla, MO |
Abbreviated Journal |
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Volume |
534 |
Issue |
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Pages |
740-743 |
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Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The paper presents the results of the study of atmospheric aerosols in the Siberian region. This research was focused on studying the chemical and biological characteristics of both natural and pollution aerosols in this vast territory of the Asian part of the former Soviet Union (FSU). The data received within the frame of this project formed the basis for the evaluation of the impact of these aerosols on the Arctic region and the global climate. The Asian part of FSU is of scientific interest in the context of environmental chemistry, air pollution and study of atmospheric aerosols, The specific relevance of aerosol research in Siberia is as follows. There are areas that are very remote from industrial or densely populated centres, In these circumstances, aerosol characterization contributes to the definition of global continental “background”) or “baseline” aerosol, i.e, the aerosol which should occur in natural circumstances and on which all pollution is superimposed. Recently, in the context of global and long-term climatic changes, baseline aerosols and long-range transport of particulate air pollutants have become a topic of much debate, This is because it has been thought that aerosols might compensate for the well-known greenhouse effect to a significant. In this context, more and more attention is being paid to long-range effects of continental aerosols on the polar regions. Research in Norway and Alaska showed that Western or Central Siberia may be a very important source of pollutants affecting the air composition in the Arctic region. Cities and regions in south Siberia are enormously polluted by heavy metals, the level of pollution being many times higher than in the Western world, thus the health of local population is seriously affected. In most cases, gigantic point sources are in the area, which is simple from the viewpoint of environmental chemistry and unambiguous results should be obtained easily. Atmospheric deposition is a possible cause of the existence of heavy metals in the southern part of Lake Baikal. in the northern part of the lake, the environment is unpolluted. However in the southern part of the lake is considerably threatened by pollution from Baikalsk wood-pulp mill and industrial enterprises of Irkutsk, Angarsk, |
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Wos |
000089526000168 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1-56396-958-0 |
ISBN |
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Additional Links |
UA library record; WoS full record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:95766 |
Serial |
7516 |
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Author |
Callebaut, D.K.; Makarovska, Y.; Tlatov |
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Title |
Gravitational energy of solar oscillations and climatic changes |
Type |
P1 Proceeding |
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Year |
2000 |
Publication |
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Abbreviated Journal |
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Volume |
463 |
Issue |
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Pages |
297-300
T2 - 1st Solar and Space Weather Euroconfe |
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Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The gravitational energy associated with variations in the radius of the Sun is huge: with a relative change of 1/2000 (the estimated difference between maximum and minimum solar activity) and taking only the convection zone to expand, corresponds to about 2 10(34)J, which is 1/10 of the total rotational energy of the Sun. Non-radial oscillations with a tiny nonlinearity can still yield energies comparable to or larger than the total magnetic energy of a full sunspot cycle or three or four orders more than the luminosity of the Sun, but that is not sufficient to account for the changes of the temperature on Earth. The expansion of the upper layers of the convection zone, however, may directly or indirectly affect the climate and the biological aspects on the Earth. Moreover this suits a qualitative explanation why the Sun expands during a minimum of the magnetic activity. |
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Language |
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Wos |
000168300800040 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
92-9092-693-7 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:95767 |
Serial |
8006 |
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Author |
Callebaut, D.K.; Makarovska, Y. |
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Title |
On the relationship between current and magnetic field in ring-filaments |
Type |
P1 Proceeding |
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Year |
1998 |
Publication |
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Abbreviated Journal |
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Volume |
150 |
Issue |
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Pages |
111-114
T2 - IAU Colloquium 167 on New Perspective |
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Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
There is a type of filament that forms dosed contours encircling regions of one polarity of magnetic field, while the surrounding region has the opposite polarity One distribution of ring-filaments has sizes 2R = 40,000 to 160,000 km with the maximum around 100,000 km; the other distribution (with filaments and filament channels) has bigger sizes, with a maximum around 300,000 km. At low and mid latitudes the radial component B-rs (radial for the Sun) in the region outlined by filaments varies from 50 to 100 gauss, while the longitudinal component B-phi varies from 10 to 30 gauss. The total current inside the filament is 10(10) – 10(11) A, the ratio R/a approximate to 5 to 10, the magnetic flux crossing the surface is approximate to 10(21) – 10(22) MX; th, magnetic energy is approximate to 10(29) – 10(31) erg. Polar ring-filaments at latitudes 60 degrees-80 degrees are related to the polar magnetic field reversal and the quasi-flare processes at the poles during the field reversal. Correlation between B-rs and B-phi for the polar filament bands cannot be satisfactorily explained. A theoretical model using the conservation laws is used to study the relations between the various fields, currents, etc, of shrinking polar ring-filaments and their evolution. According to this theory ring-filaments should rise higher above the photosphere when shrinking. However, observations show that the height lowers. Presumably the discrepancy is due to the lack of dissipation in the model. |
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Wos |
000076565100020 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1-886733-70-8 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:95844 |
Serial |
8333 |
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Author |
Janssens, K.; Vekemans, B.; Adams, F.; van Espen, P.; Mutsaers, P. |
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Title |
Accurate evaluation of \mu-PIXE and \mu-XRF spectral data through iterative least squares fitting |
Type |
A1 Journal article |
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Year |
1996 |
Publication |
Nuclear instruments and methods in physics research: B: beam interactions with materials and atoms
T2 – 7th International Conference on Particle Induced X-ray Emission and Its Analytical Applications, MAY 26-30, 1995, Abano Terme, Italy |
Abbreviated Journal |
7th International Conference on Particle Induced X-ray Emission and Its Analytical Applications, MAY |
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Volume |
109 |
Issue |
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Pages |
179-185 |
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Keywords |
A1 Journal article; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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Abstract |
The integration of the nonlinear least squares X-ray spectrum evaluation progam AXIL. into a mu-PIXE and a mu-XRF setup is discussed. The use of the software when procesing data sets derived from biological and geological samples is described. |
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Wos |
A1996UV44400035 |
Publication Date |
2002-07-25 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0168-583x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:95887 |
Serial |
5457 |
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Author |
Cabal Rodríguez, A.E.; Leyva Pernia, D.; Schalm, O.; van Espen, P.J.M. |
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Title |
Possibilities of energy-resolved X-ray radiography for the investigation of paintings |
Type |
A1 Journal article |
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Year |
2012 |
Publication |
Analytical and bioanalytical chemistry |
Abbreviated Journal |
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Volume |
402 |
Issue |
4 |
Pages |
1471-1480 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
X-ray radiographic images of paintings often show little or no contrast. In order to increase the contrast in radiographic images we measured the X-ray spectrum of a low power X-ray tube, after passing through the painting, with a high energy-resolution SDD detector. To obtain images, the detector is collimated with a 400 mu m diameter pinhole and the painting was moved through the beam in the x and y-direction using a dwell time of a few seconds per pixel. The data obtained consists of a data cube of, typically, 200 x 200 pixels and a 512-channel X-ray spectrum for each pixel, spanning the energy range from 0 to 40 keV. Having the absorbance spectrum available for each pixel, we are able, a posteriori, to produce images by edge subtraction for any given element. In this way high contrast, element-specific, images can be obtained. Because of the high energy-resolution a much simpler edge subtraction algorithm can be applied. We also used principal-component imaging to obtain, in a more automated way, images with high contrast. Some of these images can easily be attributed to specific elements. It turns out that preprocessing of the spectral data is crucial for the success of the multivariate image processing. |
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Wos |
000299842000008 |
Publication Date |
2011-07-14 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1618-2642; 1618-2650 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:96200 |
Serial |
8394 |
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Author |
De Keersmaecker, M.; De Wael, K.; Adriaens, A. |
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Title |
The use of lead dodecanoate as an environmentally friendly coating to inhibit the corrosion of lead objects : comparison of three different deposition methods |
Type |
A1 Journal article |
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Year |
2012 |
Publication |
Progress in organic coatings |
Abbreviated Journal |
Prog Org Coat |
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Volume |
74 |
Issue |
1 |
Pages |
1-7 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
An aqueous sodium dodecanoate solution has been used for the formation of a protective coating for lead. Three deposition methods have been compared: immobilization using cyclic voltammetry, immersion and amperometry. Apart from this, we tested a reduction pretreatment of the lead surface (−1.5 V during 600 s) in order to obtain a more reproducible coating, resulting in a better corrosion protection behavior. The corrosion inhibition properties were examined using potentiodynamic polarization curves and electrochemical impedance measurements in a standard corrosive environment. |
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Wos |
000302585300001 |
Publication Date |
2012-02-16 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0300-9440; 0033-0655 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
2.858 |
Times cited |
8 |
Open Access |
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Notes |
; The Research Foundation – Flanders (FWO) and Ghent University are acknowledged for funding this work. The authors would like to thank Pieter Van Hoe for the production of the embedded lead electrodes. They also acknowledge Pieter Arickx and Jonas Van Damme for their contribution. ; |
Approved |
Most recent IF: 2.858; 2012 IF: 1.848 |
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Call Number |
UA @ admin @ c:irua:96354 |
Serial |
5894 |
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| Permanent link to this record |
