Records |
Author |
Storms, H.M.; Janssens, K.H.; Török, S.B.; Van Grieken, R.E. |
Title |
Evaluation of the ArmstrongBuseck correction for automated electron probe X-ray microanalysis of particles |
Type |
A1 Journal article |
Year |
1989 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
18 |
Issue |
2 |
Pages |
45-52 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The ArmstrongBuseck correction for absorption effects in electron probe x-ray microanalysis of particles considers seven specific particle shapes, and for these geometries exact correction equations are used. This procedure implies that the analyst has to associate the particle to be analysed with a certain particle type; an arbitrary relative thickness is sometimes assumed. A theoretical study was made of this absorption correction as a function of the particle composition, type and thickness for micrometre-sized particles. It appears that a correct choice of the particle type is critical. However, when the analytical results are normalized to 100%, the differences between the models are much less pronounced, and it is justified to assume a spherical model in all cases. |
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Wos |
A1989U261400001 |
Publication Date |
2005-05-28 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0049-8246 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116489 |
Serial |
5616 |
Permanent link to this record |
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Author |
Vincze, L.; Janssens, K.; Adams, F. |
Title |
A general Monte-Carlo simulation of energy-dispersive X-ray fluorescence spectrometers : 1 : unpolarized radiation, homogenious samples |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
|
Volume |
48 |
Issue |
4 |
Pages |
553-573 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
A general Monte Carlo program for the simulation of X-ray fluorescence (XRF) spectrometers is presented. The global layout of the program is discussed and the way in which variance reduction techniques have been employed to improve the efficiency of the code is described. For the case of polychromatic excitation in a direct excitation energy-dispersive (ED) XRF instrument, experimentally collected ED-XRF spectra are compared with simulated spectral distributions. Applications of the software in the field of quantitative analysis and thickness estimation of samples of intermediate thickness illustrate the potential of the method. |
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Wos |
A1993KY21500006 |
Publication Date |
2002-07-25 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0584-8547; 0038-6987 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:6118 |
Serial |
5632 |
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Author |
Janssens, K.; van Espen, P. |
Title |
Implementation of an expert system for the qualitative interpretation of x-ray-fluorescence spectra |
Type |
A1 Journal article |
Year |
1986 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
|
Volume |
184 |
Issue |
|
Pages |
117-132 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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Wos |
A1986D964700010 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2670 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:149782 |
Serial |
5655 |
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Author |
Janssens, K.; Vanborm, W.; van Espen, P. |
Title |
Increased accuracy in the automated interpretation of large epma data sets by the use of an expert system |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Journal of research of the National Bureau of Standards (1934) |
Abbreviated Journal |
|
Volume |
93 |
Issue |
3 |
Pages |
260-264 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
Abstract |
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Wos |
A1988P035100026 |
Publication Date |
2012-07-30 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0091-0635 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:149777 |
Serial |
5660 |
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Author |
Janssens, K.; Vekemans, B.; Rindby, A.; Vincze, L.; Adams, F. |
Title |
A laboratory mu-XRF spectrometer employing capillary optics |
Type |
P1 Proceeding |
Year |
1995 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
159-160 |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
A1995BE26U00071 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1-56081-919-7 |
ISBN |
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UA library record; WoS full record |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:104453 |
Serial |
5687 |
Permanent link to this record |
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Author |
Janssens, K.; Vekemans, B.; Vincze, L.; Adams, F.; Rindby, A. |
Title |
A micro XRF spectrometer based on rotating anode generator and capillary optics |
Type |
A1 Journal article |
Year |
1996 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
|
Volume |
51 |
Issue |
13 |
Pages |
1661-1678 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Publisher |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0584-8547; 0038-6987 |
ISBN |
|
Additional Links |
UA library record |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:14256 |
Serial |
5720 |
Permanent link to this record |
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Author |
Janssens, K.; Vincze, L.; Aerts, A.; Vekemans, B.; Adams, F.; Jones, K.; Knöchel, A. |
Title |
Microscopic synchroton radiation induced X-ray fluorescence analysis |
Type |
A3 Journal article |
Year |
1996 |
Publication |
Mikrochimica acta: supplementum |
Abbreviated Journal |
|
Volume |
|
Issue |
13 |
Pages |
87-115 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0076-8642 |
ISBN |
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UA library record |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:14252 |
Serial |
5724 |
Permanent link to this record |
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|
Author |
Janssens, K.; Vincze, L.; Rubio, J.; Bernasconi, G.; Adams, F. |
Title |
Microscopic X-ray fluorescence analysis |
Type |
A1 Journal article |
Year |
1994 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
|
Volume |
9 |
Issue |
|
Pages |
151-157 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Wos |
A1994NK96200009 |
Publication Date |
2004-04-20 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0267-9477 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:8917 |
Serial |
5726 |
Permanent link to this record |
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|
|
Author |
Janssens, K.; Vincze, L.; van Espen, P.; Adams, F. |
Title |
Monte Carlo simulation of conventional and synchrotron energy-dispersive X-ray spectrometers |
Type |
A1 Journal article |
Year |
1993 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
22 |
Issue |
|
Pages |
234-243 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1993LQ04200011 |
Publication Date |
2005-05-28 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0049-8246 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:6117 |
Serial |
5736 |
Permanent link to this record |
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|
|
Author |
Vincze, L.; Janssens, K.; Adams, F. |
Title |
Optics for X-ray microfluorescence to be used at the European synchrotron radiation facility |
Type |
A1 Journal article |
Year |
1994 |
Publication |
Advances in X-ray analysis |
Abbreviated Journal |
|
Volume |
37 |
Issue |
|
Pages |
553-563 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1994BB55S00067 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0376-0308 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:8930 |
Serial |
5757 |
Permanent link to this record |
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|
|
Author |
Vincze, L.; Janssens, K.; Adams, F.; Larsson, S.; Rindby, A.; Engstrom, P. |
Title |
Parameters influencing focussing capabilities of capillary optics |
Type |
P1 Proceeding |
Year |
1995 |
Publication |
Microbeam Analysis 1995: Proceedings Of The 29th Annual Conference Of The Microbeam Analysis Society |
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
161-162 |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1995BE26U00072 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1-56081-919-7 |
ISBN |
|
Additional Links |
UA library record; WoS full record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:104454 |
Serial |
5767 |
Permanent link to this record |
|
|
|
Author |
Janssens, K.; Nobels, J.; van Espen, P. |
Title |
PC-MCA : a software package for the acquisition and processing of spectral data |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Chemometrics and intelligent laboratory systems |
Abbreviated Journal |
|
Volume |
3 |
Issue |
4 |
Pages |
335-341 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1988P260100012 |
Publication Date |
2002-07-25 |
Series Editor |
|
Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0169-7439 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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|
Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:149776 |
Serial |
5768 |
Permanent link to this record |
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|
|
Author |
van Langevelde, F.; Janssens, K.H.; Adams, F.C.; Vis, R.D. |
Title |
Prediction of the optical characteristics and analytical qualities of an X-ray fluorescence microprobe at the European Synchrotron Radiation Facility (Grenoble) |
Type |
A1 Journal article |
Year |
1992 |
Publication |
Nuclear instruments and methods in physics research : A: accelerators, spectrometers, detectors and associated equipment |
Abbreviated Journal |
|
Volume |
317 |
Issue |
|
Pages |
383-393 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1992JF39700044 |
Publication Date |
2002-11-12 |
Series Editor |
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Series Title |
|
Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0168-9002 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:2810 |
Serial |
5783 |
Permanent link to this record |
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|
|
Author |
Aerts, A.; Janssens, K.; Vincze, L.; Vekemans, B.; Adams, F.; Haller, M.; Radtke, M.; Knöchel, A. |
Title |
Provenance analysis of Roman glass from the 1st-6th century A.D |
Type |
A3 Journal article |
Year |
1996 |
Publication |
HASYLAB Jahresbericht |
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
918-919 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
Impact Factor |
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Times cited |
|
Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:21744 |
Serial |
5790 |
Permanent link to this record |
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|
|
Author |
Haller, M.; Radtke, M.; Knöchel, A.; Clöck, W.; Sutton, S.; Janssens, K.; Vincze, L. |
Title |
Quantification of SY-XRF measurements at the X-ray microprobe |
Type |
A3 Journal article |
Year |
1996 |
Publication |
HASYLAB Jahresbericht |
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
956-957 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Place of Publication |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:21745 |
Serial |
5792 |
Permanent link to this record |
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|
|
Author |
Vincze, L.; Janssens, K.; Adams, F.; Jones, K. |
Title |
Quantitative mu-XRF analysis of heterogeneous samples |
Type |
P1 Proceeding |
Year |
1995 |
Publication |
Microbeam Analysis 1995: Proceedings Of The 29th Annual Conference Of The Microbeam Analysis Society |
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
175-176 |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Place of Publication |
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Wos |
A1995BE26U00079 |
Publication Date |
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Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1-56081-919-7 |
ISBN |
|
Additional Links |
UA library record; WoS full record |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:104455 |
Serial |
5795 |
Permanent link to this record |
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|
|
Author |
Janssens, K. |
Title |
Special issue on Microscopic and ultratrace x-ray fluorescence analysis: 2 |
Type |
A1 Journal article |
Year |
1996 |
Publication |
Journal of trace and microprobe techniques |
Abbreviated Journal |
|
Volume |
14 |
Issue |
3 |
Pages |
461-604 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Corporate Author |
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Place of Publication |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0733-4680 |
ISBN |
|
Additional Links |
UA library record |
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Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:16250 |
Serial |
5839 |
Permanent link to this record |
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|
|
Author |
van Espen, P.; Janssens, K. |
Title |
Spectrum evaluation |
Type |
H3 Book chapter |
Year |
1992 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
|
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
chapter 4 |
Series Issue |
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Edition |
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ISSN |
|
ISBN |
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Additional Links |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:2809 |
Serial |
5842 |
Permanent link to this record |
|
|
|
Author |
Adams, F.; Adriaens, A.; Berghmans, P.; Janssens, K. |
Title |
Surface microanalysis |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
|
Volume |
283 |
Issue |
|
Pages |
19-34 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
|
Editor |
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Language |
|
Wos |
A1993MK02800003 |
Publication Date |
2002-07-25 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0003-2670 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:6106 |
Serial |
5856 |
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Author |
Janssens, K.; Vincze, L.; Adams, F.; Jones, K.W. |
Title |
Synchrotron radiation-induced X-ray microanalysis |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
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Volume |
283 |
Issue |
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Pages |
98-119 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1993MK02800009 |
Publication Date |
2002-07-25 |
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Series Issue |
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Edition |
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ISSN |
0003-2670 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:6107 |
Serial |
5865 |
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Author |
Janssens, K.; Vincze, L.; Vekemans, B.; Aerts, A.; Adams, F.; Jones, K.W.; Knöchel, A. |
Title |
Synchrotron radiation induced X-ray microfluorescence analysis |
Type |
A1 Journal article |
Year |
1996 |
Publication |
Microchimica acta
T2 – 4th Workshop of the European-Microanalysis-Society on Modern, Developments and Applications in Microbeam Analysis, MAY, 1995, ST MALO, FRANCE |
Abbreviated Journal |
4th Workshop of the European-Microanalysis-Society on Modern, Developments and Applications in Micro |
Volume |
|
Issue |
s:[13] |
Pages |
87-115 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
mu-XRF is the microscopic equivalent of the well-established multielement analytical technique. In this paper, after comparing the interaction of X-ray photons, electrons and protons with matter and an introduction to synchrotron rings and microfocussing of X-rays, the instrumentation for mu-XRF is discussed, both for laboratory source and synchrotron based setups and the analytical characteristics of mu-XRF are contrasted to that of other microanalytical techniques, Also, this issue of quantification of mu-XRF data is addressed; the applicability of the method in archeological and geological analysis is illustrated. |
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A1996VT82300006 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:104410 |
Serial |
5866 |
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Author |
Janssens, K.; Dorrine, W.; van Espen, P. |
Title |
The development process of an expert system for the automated interpretation of large epma data sets |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Chemometrics and intelligent laboratory systems |
Abbreviated Journal |
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Volume |
4 |
Issue |
2 |
Pages |
147-161 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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Wos |
A1988Q148500007 |
Publication Date |
2002-07-25 |
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Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0169-7439 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:149775 |
Serial |
5872 |
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Author |
Adams, F.; Janssens, K. |
Title |
X-ray microanalysis: a new tool for environmental analysis |
Type |
H3 Book chapter |
Year |
1996 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
183-199 |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:14257 |
Serial |
5916 |
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Author |
Vincze, L.; Janssens, K.; Adams, F. |
Title |
X-ray optics for synchrotron-radiation-induced X-ray micro fluorescence at the european synchrotron-radiation facility, Grenoble |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Institute of physics conference series |
Abbreviated Journal |
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Volume |
|
Issue |
130 |
Pages |
613-616 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Different optical designs for generating synchrotron x-ray micro beams suitable for use in an X-ray fluorescence microscope using an ESRF bending magnet X-ray source are compared. Attention is devoted to the spatial and energy distribution of the photons in the micro beam and to the minimum detection limits that are achievable with each alternative optical system. |
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Wos |
A1993LW34000126 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0305-2346 |
ISBN |
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UA library record; WoS full record |
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no |
Call Number |
UA @ admin @ c:irua:104541 |
Serial |
5917 |
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Author |
Pouyet, E.; Cotte, M.; Fayard, B.; Salome, M.; Meirer, F.; Mehta, A.; Uffelman, E.S.; Hull, A.; Vanmeert, F.; Kieffer, J.; Burghammer, M.; Janssens, K.; Sette, F.; Mass, J. |
Title |
2D X-ray and FTIR micro-analysis of the degradation of cadmium yellow pigment in paintings of Henri Matisse |
Type |
A1 Journal article |
Year |
2015 |
Publication |
Applied physics A : materials science & processing |
Abbreviated Journal |
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Volume |
121 |
Issue |
3 |
Pages |
967-980 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The chemical and physical alterations of cadmium yellow (CdS) paints in Henri Matisse's The Joy of Life (1905-1906, The Barnes Foundation) have been recognized since 2006, when a survey by portable X-ray fluorescence identified this pigment in all altered regions of the monumental painting. This alteration is visible as fading, discoloration, chalking, flaking, and spalling of several regions of light to medium yellow paint. Since that time, synchrotron radiation-based techniques including elemental and spectroscopic imaging, as well as X-ray scattering have been employed to locate and identify the alteration products observed in this and related works by Henri Matisse. This information is necessary to formulate one or multiple mechanisms for degradation of Matisse's paints from this period, and thus ensure proper environmental conditions for the storage and the display of his works. This paper focuses on 2D full-field X-ray Near Edge Structure imaging, 2D micro-X-ray Diffraction, X-ray Fluorescence, and Fourier Transform Infra-red imaging of the altered paint layers to address one of the long-standing questions about cadmium yellow alteration-the roles of cadmium carbonates and cadmium sulphates found in the altered paint layers. These compounds have often been assumed to be photo-oxidation products, but could also be residual starting reagents from an indirect wet process synthesis of CdS. The data presented here allow identifying and mapping the location of cadmium carbonates, cadmium chlorides, cadmium oxalates, cadmium sulphates, and cadmium sulphides in thin sections of altered cadmium yellow paints from The Joy of Life and Matisse's Flower Piece (1906, The Barnes Foundation). Distribution of various cadmium compounds confirms that cadmium carbonates and sulphates are photo-degradation products in The Joy of Life, whereas in Flower Piece, cadmium carbonates appear to have been a [(partially) unreacted] starting reagent for the yellow paint, a role previously suggested in other altered yellow paints. |
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Wos |
000364914100017 |
Publication Date |
2015-06-03 |
Series Editor |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0947-8396; 1432-0630 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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no |
Call Number |
UA @ admin @ c:irua:130290 |
Serial |
7382 |
Permanent link to this record |
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Author |
Lenaerts, S.; Roggen, J.; Maes, G. |
Title |
FT-IR characterization of tin dioxide gas sensor materials under working conditions |
Type |
A1 Journal article |
Year |
1995 |
Publication |
Spectrochimica acta: part A: molecular and biomolecular spectroscopy |
Abbreviated Journal |
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Volume |
51 |
Issue |
5 |
Pages |
883-894 |
Keywords |
A1 Journal article |
Abstract |
In this work self-supporting tin dioxide disks are characterized using FT-IR spectroscopy in the presence of a reducing gas in air, and in different O2/N2 mixtures at temperatures varying from room temperature up to 450°C. Every factor inducing a change in the oxygen content of the gas atmosphere above the tin dioxide, as for instance a temperature change, a surface reaction or adsorption of another species, induces a broad, intense IR absorption band with discrete weak bands superimposed on it. This broad absorption is assigned to the electronic transition from a native donor level, the oxygen vacancy in the bulk of the domain, to the conduction band of the tin dioxide material. For the interpretation of the narrow, superimposed absorptions, two hypotheses remain. The results demonstrate that FT-IR spectroscopy is an extremely suitable technique for the characterization of semiconducting metal oxide sensors, since it allows to follow in situ the processes in the bulk, at the surface and in the surrounding gas atmosphere of the sensor material at working temperature as well as in the presence of reducing gases in air. |
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Wos |
A1995RJ99900014 |
Publication Date |
2003-04-05 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1386-1425 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:82015 |
Serial |
5954 |
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Author |
Lenaerts, S.; Honoré, M.; Huyberechts, G.; Roggen, J.; Maes, G. |
Title |
In situ infrared and electrical characterization of tin dioxide gas sensors in nitrogen/oxygen mixtures at temperatures up to 720 K |
Type |
A1 Journal article |
Year |
1994 |
Publication |
Sensors and actuators : B : chemical |
Abbreviated Journal |
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Volume |
19 |
Issue |
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Pages |
478-482 |
Keywords |
A1 Journal article |
Abstract |
FT-IR spectroscopy and impedance measurements of tin dioxide sensor materials at working temperatures up to 450 °C in atmospheres with varying O2/N2 ratio are used as an in situ probe to study the interactions at the surface of the semiconducting oxide. Every diminution in the oxygen content above the sample induces a broad IR absorption band (X-band) between 2300700 cm−1 with a few small peaks in the 1400850 cm−1 region of the spectrum superimposed on it. The X-band results from the enchanced electron concentration in the bulk of the tin dioxide domain. The fine structure is due to the absorption of several kinds of surface oxygen species associated vibration modes. The porous tin dioxide consists of domains were the outward shell is depleted of electrons by the formation of adsorbed O− species on oxygen surface sites, SO(O− species. In our proposed model for the impedance data this gives rise to a parallel RpCp circuit for the domain boundary characteristics and to an Rs parameter for the intradomain resistance. The evolution of these IR and impedance spectroscopic effects with temperature and oxygen content is used to set up, to confirm and refine a physicochemical operation model of tin dioxide gas sensor. This model consists of a sensitizing reaction sequence in the presence of oxygen and a gas-detection reaction sequence when a reducing gas is present. Based on this model, the principal disadvantages of this type of gas sensor become clear. Every factor that influences the concentration of SO(O−) species, causes a conductance modification. If we can control and direct the nature, the number and the arrangement of the tin dioxide domains, a directed development and improvement of the sensor characteristics is possible. |
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Wos |
A1994NN90000040 |
Publication Date |
2002-07-25 |
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Abbreviated Series Title |
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Series Volume |
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Edition |
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ISSN |
0925-4005 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:82014 |
Serial |
5962 |
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Author |
Honoré, M.; Lenaerts, S.; Desmet, J.; Huyberechts, G.; Roggen, J. |
Title |
Synthesis and characterization of tin dioxide powders for the realization of thick-film gas sensors |
Type |
A1 Journal article |
Year |
1994 |
Publication |
Sensors and actuators : B : chemical |
Abbreviated Journal |
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Volume |
19 |
Issue |
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Pages |
621-624 |
Keywords |
A1 Journal article |
Abstract |
Semiconductor gas sensors produced with screen-printing techniques and based on home-made tin dioxide inks are presented. The ink consists of home-made tin dioxide powder added to a polymer solution to make it screen printable on 96% alumina substrates. The major work is performed on the preparation and the characterization of pure undoped tin dioxide powder produced by two different synthetic pathways. Inks prepared with powders from each method are consecutively handled in an identical way to obtain gas sensors. The sensor response towards different gases is measured and compared for both types of starting materials. |
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Wos |
A1994NN90000073 |
Publication Date |
2002-07-25 |
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Edition |
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ISSN |
0925-4005 |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:82013 |
Serial |
5996 |
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Author |
Guzzinati, G.; Ghielens, W.; Mahr, C.; Béché, A.; Rosenauer, A.; Calders, T.; Verbeeck, J. |
Title |
Electron Bessel beam diffraction patterns, line scan of Si/SiGe multilayer |
Type |
Dataset |
Year |
2019 |
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Keywords |
Dataset; ADReM Data Lab (ADReM); Electron microscopy for materials research (EMAT) |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:169114 |
Serial |
6865 |
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Author |
Marteleur, M.; Idrissi, H.; Amin-Ahmadi, B.; Prima, F.; Schryvers, D.; Jacques, P.J. |
Title |
On the nucleation mechanism of {112} < 111 > mechanical twins in as-quenched beta metastable Ti-12 wt.% Mo alloy |
Type |
A1 Journal article |
Year |
2019 |
Publication |
Materialia |
Abbreviated Journal |
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Volume |
7 |
Issue |
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Pages |
Unsp 100418 |
Keywords |
A1 Journal article; Electron microscopy for materials research (EMAT) |
Abstract |
Recently developed beta-metastable Ti grades take advantage of the simultaneous activation of TRIP and TWIP effects for enhancing their work hardening rate. However, the role of each plasticity mechanism on the macroscopic mechanical response is still unclear. In this work, the nucleation mechanism of the first activated plasticity mechanism, namely {112} < 111 > twinning, was investigated. Firstly, post-mortem TEM analysis showed that twins nucleate on pre-existing microstructural defects such as thermal jogs with the zonal dislocation mechanism. The precipitation of the omega phase on twin boundaries has been observed, as well as the emission of numerous dislocations from super-jogs present in these twin boundaries. It is also shown that {112} < 111 > twins act as effective dislocation sources for the subsequent plasticity mechanisms such as beta -> alpha '' martensitic transformation and {332} < 111 > twinning. Secondly, in situ TEM tensile testing of the investigated Ti grade highlighted the primary role of the initial defect configuration present in the microstructure. It is shown that twins cannot nucleate without the presence of specific defects allowing the triggering of the dislocation decomposition needed for the twinning mechanism highlighted in investigated bulk samples. |
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Wos |
000537131000052 |
Publication Date |
2019-07-31 |
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Edition |
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ISSN |
2589-1529 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:170326 |
Serial |
6875 |
Permanent link to this record |