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Records |
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Author |
Godoi, A.F.L.; Van Vaeck, L.; Van Grieken, R. |
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Title |
Use of solid-phase microextraction for the detection of acetic acid by ion-trap gas chromatography-mass spectrometry and application to indoor levels in museums |
Type |
A1 Journal article |
| |
Year |
2005 |
Publication |
Journal of chromatography: A: bibliography section |
Abbreviated Journal |
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Volume |
1067 |
Issue |
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Pages |
331-336 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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000227925800032 |
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2005-01-26 |
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no |
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Call Number |
UA @ admin @ c:irua:51590 |
Serial |
8723 |
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Author |
Amiri-Aref, M. |
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Title |
Utilization of magnetic nanoparticles and carbon nanotubes to fabrication electrochemical sensors for determination of some important biological and pharmaceutical compounds |
Type |
Doctoral thesis |
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Year |
2015 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
137 p. |
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Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:128299 |
Serial |
8727 |
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Author |
Vanmeert, F.; Van der Snickt, G.; Legrand, S.; Janssens, K. |
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Title |
Velázquez? A portrait of Pope Innocent X : an X-ray imaging investigation (II) |
Type |
H3 Book chapter |
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Year |
2019 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
132-141
T2 - Velázquez : Anregungen, Vorschläge, L |
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Keywords |
H3 Book chapter; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Encompassing a broad spectrum of methodological approaches and aims, the scholars contributing to this volume offer renewed perspectives on the multifaceted oeuvre of Diego Velázquez. The seventeenth-century artist’s exceptional religious works as well as his numerous portraits are examined within the social and historical context of Velázquez’s milieu which included both the Spanish court as well as circles comprising important intellectual figures of his time. Following a close investigation of his works, which also includes the results of recent technological examinations on his paintings, the contributors to this volume offer new, exciting findings and discussions on the inspirations, sources and possible intentions of Velázquez. |
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ISBN |
978-3-99020-155-8 |
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no |
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Call Number |
UA @ admin @ c:irua:190783 |
Serial |
8736 |
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Author |
Deutsch, F.; Stranger, M.; Kaplinskii, A.E.; Samek, L.; Joos, P.; Van Grieken, R. |
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| |
Title |
O vlijanii kolitsjestva osadkov na kontsentratsioe elementov i ionov v tsjastitsach gorodskogo aerozolja |
Type |
A3 Journal article |
| |
Year |
2003 |
Publication |
Optika atmospheri i okeana |
Abbreviated Journal |
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| |
Volume |
16 |
Issue |
10 |
Pages |
927-932 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:43705 |
Serial |
8738 |
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Author |
Delalieux, F.; Sweevers, H.; Van Grieken, R. |
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| |
Title |
Weathering mechanism of Pentelic marble under ambient atmospheric conditions derived from runoff studies |
Type |
P3 Proceeding |
| |
Year |
1997 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:18791 |
Serial |
8751 |
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| Permanent link to this record |
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Author |
Vleugels, G.; Van Grieken, R. |
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| |
Title |
Weathering of bare and treated limestones under ambient conditions using runoff water analysis and microanalysis |
Type |
P3 Proceeding |
| |
Year |
1992 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:2865 |
Serial |
8752 |
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| Permanent link to this record |
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| |
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Author |
Vleugels, G.J.; Van Grieken, R.E. |
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| |
Title |
Weathering of treated and untreated limestones in atmospheric exposures |
Type |
A3 Journal article |
| |
Year |
1991 |
Publication |
Journal of preservation technology |
Abbreviated Journal |
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| |
Volume |
23 |
Issue |
|
Pages |
48-51 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:4320 |
Serial |
8755 |
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Author |
Roekens, E.; Van Raemdonck, C.; Leysen, L.; Chakravorty, R.; Van Grieken, R. |
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| |
Title |
Weathering products and surface recession rates for sandy limestones exposed to air pollution |
Type |
H3 Book chapter |
| |
Year |
1987 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
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Pages |
707-714
T2 - Acid rain : scientific and technical |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Additional Links |
UA library record |
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| |
Notes |
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Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:117536 |
Serial |
8756 |
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| Permanent link to this record |
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Author |
Van Grieken, R. |
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| |
Title |
Working close to the detection limits: XRF |
Type |
Minutes and reports |
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Year |
1998 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:20973 |
Serial |
8761 |
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Author |
Samek, L.; Worobiec, A.; Van Grieken, R.; van Meel, K.; Kontozova, V.; Karaszkiewicz, P.; Wiłkojć, E. |
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| |
Title |
Wpływ zwiedzajacych na zanieczyszczenia wnetrz muzealnych |
Type |
H3 Book chapter |
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Year |
2007 |
Publication |
|
Abbreviated Journal |
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| |
Volume |
|
Issue |
|
Pages |
209-218
T2 - Konserwacja zapobiegawcza w muzeach |
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| |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:67628 |
Serial |
8762 |
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Author |
Injuk, J.; Van Grieken, R.E. |
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Title |
X-ray fluorescence |
Type |
H3 Book chapter |
| |
Year |
2001 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
151-178
T2 - Non-destructive elemental analysis / |
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| |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:34107 |
Serial |
8764 |
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Author |
Margu'i', E.; Queralt, I.; Van Grieken, R. |
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| |
Title |
X-ray fluorescence analysis, sample preparation for |
Type |
H1 Book chapter |
| |
Year |
2009 |
Publication |
|
Abbreviated Journal |
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| |
Volume |
|
Issue |
|
Pages |
1-20
T2 - Sncyclopedia of analytical chemistry / M |
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| |
Keywords |
H1 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Series Issue |
|
Edition |
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| |
ISSN |
|
ISBN |
978-0-471-97670-7 |
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UA library record |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:81641 |
Serial |
8765 |
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| |
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Author |
Van Grieken, R.; Potgieter-Vermaak, S.; Darchuk, L.; Worobiec, A. |
|
| |
Title |
X ray fluorescence in member states: Belgium: integration of analysis techniques of different scales using X ray induced and electron induced X ray spectrometry for applications in preventive conservation and environmental monitoring |
Type |
A3 Journal article |
| |
Year |
2009 |
Publication |
XRF newsletter |
Abbreviated Journal |
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|
| |
Volume |
|
Issue |
18 |
Pages |
9-13 |
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| |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:81898 |
Serial |
8766 |
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| Permanent link to this record |
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| |
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Author |
Marguí, E.; Van Grieken, R. |
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| |
Title |
X-ray fluorescence spectrometry and related techniques : an introduction |
Type |
MA3 Book as author |
| |
Year |
2013 |
Publication |
|
Abbreviated Journal |
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| |
Volume |
|
Issue |
|
Pages |
148 p. |
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| |
Keywords |
MA3 Book as author; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
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Edition |
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| |
ISSN |
|
ISBN |
978-1-60650-391-1 |
Additional Links |
UA library record |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:106179 |
Serial |
8768 |
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| Permanent link to this record |
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| |
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Author |
Van Grieken, R.E. |
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| |
Title |
X-ray spectrometry |
Type |
H3 Book chapter |
| |
Year |
2000 |
Publication |
|
Abbreviated Journal |
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| |
Volume |
15 |
Issue |
|
Pages |
13269-13443
T2 - Encyclopedia of analytical chemis |
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| |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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| |
Notes |
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Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:31650 |
Serial |
8775 |
|
| Permanent link to this record |
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| |
|
Author |
Van Grieken, R.; Delalieux, F. |
|
| |
Title |
X-ray spectrometry for air pollution and cultural heritage research |
Type |
P3 Proceeding |
| |
Year |
2004 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
|
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| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:51259 |
Serial |
8783 |
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| Permanent link to this record |
| |
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| |
|
Author |
Van Grieken, R.; Makarovska, Y.; van Meel, K.; Worobiec, A. |
|
| |
Title |
X-ray spectrometry for analysis of atmospheric particulate matter: detection limits versus legal levels |
Type |
H3 Book chapter |
| |
Year |
2007 |
Publication |
|
Abbreviated Journal |
|
|
| |
Volume |
|
Issue |
|
Pages |
153-161
T2 - Topics in X-ray spectrometry / Vázque |
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| |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Abstract |
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Address |
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Corporate Author |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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| |
Series Volume |
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Series Issue |
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Edition |
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| |
ISSN |
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ISBN |
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Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
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|
| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:64402 |
Serial |
8784 |
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| Permanent link to this record |
| |
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| |
|
Author |
Tsuji, K.; Injuk, J.; Van Grieken, R. |
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| |
Title |
X-ray spectrometry: recent technological advances |
Type |
ME1 Book as editor or co-editor |
| |
Year |
2004 |
Publication |
|
Abbreviated Journal |
|
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| |
Volume |
|
Issue |
|
Pages |
616 p. |
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| |
Keywords |
ME1 Book as editor or co-editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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| |
Language |
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Wos |
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Publication Date |
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| |
Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
|
|
| |
ISSN |
|
ISBN |
0-471-48640-x |
Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
|
|
| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:43876 |
Serial |
8786 |
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| Permanent link to this record |
| |
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| |
|
Author |
Van Alsenoy, W.; Bernard, P.; Van Grieken, R. |
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| |
Title |
Zware metalen in Noordzee- en Schelde-sedimenten |
Type |
A3 Journal article |
| |
Year |
1990 |
Publication |
Wtare |
Abbreviated Journal |
|
|
| |
Volume |
5 |
Issue |
|
Pages |
113-121 |
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| |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
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Edition |
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| |
ISSN |
|
ISBN |
|
Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
|
|
| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:116829 |
Serial |
8787 |
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| Permanent link to this record |
| |
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| |
|
Author |
Vincze, L.; Vekemans, B.; Szaloki, I.; Brenker, F.E.; Falkenberg, G.; Rickers, K.; Aerts, K.; Van Grieken, R.; Adams, F. |
|
| |
Title |
X-ray fluorescence microtomography and polycapillary based confocal imaging using synchrotron radiation |
Type |
P1 Proceeding |
| |
Year |
2004 |
Publication |
|
Abbreviated Journal |
|
|
| |
Volume |
|
Issue |
|
Pages |
220-231
T2 - 4th Conference on Developments in X-R |
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| |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
Ibis work illustrates the development of X-ray fluorescence tomography and polycapillary based confocal imaging towards a three-dimensional (313), quantitative analytical method with lateral resolution levels down to the 2-20 mum scale. Detailed analytical characterization is given for polycapillary based confocal XRF imaging, which is a new variant of the 3D micro-XRF technique. Applications for 2D/3D micro-XR-F are illustrated for the analysis of biological (zooplankton) and geological samples (microscopic inclusions in natural diamonds and fluid inclusions in quartz). Based on confocal imaging, fully three-dimensional distributions of trace elements could be obtained, representing a significant generalization of the regular 2D scanning technique for micro-XRF spectroscopy. The experimental work described in this paper has been carried out at the ESRF ID18F microfluorescence end-station and at HASYLAB Beam Line L. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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| |
Language |
|
Wos |
000225665000023 |
Publication Date |
2004-11-02 |
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| |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
|
|
| |
ISSN |
0-8194-5473-7 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
|
|
| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:94812 |
Serial |
8767 |
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| Permanent link to this record |
| |
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| |
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Author |
Vincze, L.; Kukhlevsky, S.V.; Janssens, K. |
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| |
Title |
Simulation of poly-capillary lenses for coherent and partially coherent x-rays |
Type |
P1 Proceeding |
| |
Year |
2004 |
Publication |
Proceedings of the Society of Photo-optical Instrumentation Engineers
T2 – Conference on Advances in Computational Methods for X-Ray and Neutron, Optics, AUG 03-05, 2004, Denver, CO |
Abbreviated Journal |
|
|
| |
Volume |
|
Issue |
|
Pages |
81-85 |
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| |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
The intensity distributions of the coherent and partially coherent x-rays passed through a poly-capillary lens have been computed at the focal plane. The computations showed that at the appropriate experimental conditions the interference phenomenon does affect the intensity distribution. In the case of the coherent input radiation with the photon energy of 0.1 keV, the interference fringes were observed, while the non-coherent x-ray radiation produced no interference-like intensity distributions. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000225564800008 |
Publication Date |
2004-11-05 |
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| |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
5536 |
Series Issue |
|
Edition |
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| |
ISSN |
0-8194-5474-5 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
|
Times cited |
6 |
Open Access |
|
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| |
Notes |
|
Approved |
Most recent IF: NA |
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| |
Call Number |
UA @ admin @ c:irua:103753 |
Serial |
5832 |
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| Permanent link to this record |
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| |
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Author |
Mabesoone, J.M.; Farias, C.C.; Van Grieken, R.; Duarte, P.J.; Delgado, A.; Freira, E.M.P. |
|
| |
Title |
Parnaiba Basin shales (Northeast Brazil) |
Type |
A1 Journal article |
| |
Year |
1985 |
Publication |
Anais da Academia Brasileira de Ciências |
Abbreviated Journal |
|
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| |
Volume |
57 |
Issue |
|
Pages |
481-495 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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| |
ISSN |
0001-3765; 1678-2690 |
ISBN |
|
Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
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| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:116716 |
Serial |
8357 |
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| Permanent link to this record |
| |
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| |
|
Author |
Shevchenko, V.P.; Lisitsin, A.P.; Kuptsov, V.M.; van Malderen, H.; Martin, J.M.; Van Grieken, R.; Huang, W.W. |
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| |
Title |
Composition of aerosols in the surface boundary layer of the atmosphere over the seas of the Western Russian Arctic |
Type |
A1 Journal article |
| |
Year |
1999 |
Publication |
Oceanology |
Abbreviated Journal |
|
|
| |
Volume |
39 |
Issue |
1 |
Pages |
128-136 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
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| |
ISSN |
0001-4370 |
ISBN |
|
Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
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| |
Notes |
|
Approved |
no |
|
| |
Call Number |
UA @ admin @ c:irua:24721 |
Serial |
7707 |
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| Permanent link to this record |
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| |
|
Author |
Janssens, K.; Dik, J.; Cotte, M.; Susini, J. |
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| |
Title |
Photon-based techniques for nondestructive subsurface analysis of painted cultural heritage artifacts |
Type |
A1 Journal article |
| |
Year |
2010 |
Publication |
Accounts of chemical research |
Abbreviated Journal |
Accounts Chem Res |
|
| |
Volume |
43 |
Issue |
6 |
Pages |
814-825 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
Often, just micrometers below a paintings surface lies a wealth of information, both with Old Masters such as Peter Paul Rubens and Rembrandt van Rijn and with more recent artists of great renown such as Vincent Van Gogh and James Ensor. Subsurface layers may include underdrawing, underpainting, and alterations, and in a growing number of cases conservators have discovered abandoned compositions on paintings, illustrating artists practice of reusing a canvas or panel. The standard methods for studying the inner structure of cultural heritage (CH) artifacts are infrared reflectography and X-ray radiography, techniques that are optionally complemented with the microscopic analysis of cross-sectioned samples. These methods have limitations, but recently, a number of fundamentally new approaches for fully imaging the buildup of hidden paint layers and other complex three-dimensional (3D) substructures have been put into practice. In this Account, we discuss these developments and their recent practical application with CH artifacts. We begin with a tabular summary of 14 IR- and X-ray-based imaging methods and then continue with a discussion of each technique, illustrating CH applications with specific case studies. X-ray-based tomographic and laminographic techniques can be used to generate 3D renditions of artifacts of varying dimensions. These methods are proving invaluable for exploring inner structures, identifying the conservation state, and postulating the original manufacturing technology of metallic and other sculptures. In the analysis of paint layers, terahertz time-domain spectroscopy (THz-TDS) can highlight interfaces between layers in a stratigraphic buildup, whereas macrosopic scanning X-ray fluorescence (MA-XRF) has been employed to measure the distribution of pigments within these layers. This combination of innovative methods provides topographic and color information about the micrometer depth scale, allowing us to look into paintings in an entirely new manner. Over the past five years, several new variants of traditional IR- and X-ray-based imaging methods have been implemented by conservators and museums, and the first reports have begun to emerge in the primary research literature. Applying these state-of-the-art techniques in a complementary fashion affords a more comprehensive view of paintings and other artworks. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000278842500013 |
Publication Date |
2010-05-12 |
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| |
Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
|
|
| |
ISSN |
0001-4842 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
20.268 |
Times cited |
78 |
Open Access |
|
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| |
Notes |
; This research was supported by the Interuniversity Attraction Poles Programme-Belgian Science Policy (IUAP VI/16). The text also presents results of FWO (Brussels, Belgium) projects nr. G.0704.08 and G.0179.09 and from the UA-BOF GOA programme. ; |
Approved |
Most recent IF: 20.268; 2010 IF: 21.852 |
|
| |
Call Number |
UA @ admin @ c:irua:83983 |
Serial |
5772 |
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| Permanent link to this record |
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| |
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Author |
Cotte, M.; Susini, J.; Dik, J.; Janssens, K. |
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| |
Title |
Synchrotron-based X-ray absorption spectroscopy for art conservation: looking back and looking forward |
Type |
A1 Journal article |
| |
Year |
2010 |
Publication |
Accounts of chemical research |
Abbreviated Journal |
Accounts Chem Res |
|
| |
Volume |
43 |
Issue |
6 |
Pages |
705-714 |
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| |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
|
| |
Abstract |
A variety of analytical techniques augmented by the use of synchrotron radiation (SR), such as X-ray fluorescence (SR-XRF) and X-ray diffraction (SR-XRD), are now readily available, and they differ little, conceptually, from their common laboratory counterparts. Because of numerous advantages afforded by SR-based techniques over benchtop versions, however, SR methods have become popular with archaeologists, art historians, curators, and other researchers in the field of cultural heritage (CH). Although the CH community now commonly uses both SR-XRF and SR-XRD, the use of synchrotron-based X-ray absorption spectroscopy (SR-XAS) techniques remains marginal, mostly because CH specialists rarely interact with SR physicists. In this Account, we examine the basic principles and capabilities of XAS techniques in art preservation. XAS techniques offer a combination of features particularly well-suited for the chemical analysis of works of art. The methods are noninvasive, have low detection limits, afford high lateral resolution, and provide exceptional chemical sensitivity. These characteristics are highly desirable for the chemical characterization of precious, heterogeneous, and complex materials. In particular, the chemical mapping capability, with high spatial resolution that provides information about local composition and chemical states, even for trace elements, is a unique asset. The chemistry involved in both the objects history (that is, during fabrication) and future (that is, during preservation and restoration treatments) can be addressed by XAS. On the one hand, many studies seek to explain optical effects occurring in historical glasses or ceramics by probing the molecular environment of relevant chromophores. Hence, XAS can provide insight into craft skills that were mastered years, decades, or centuries ago but were lost over the course of time. On the other hand, XAS can also be used to characterize unwanted reactions, which are then considered alteration phenomena and can dramatically alter the objects original visual properties. In such cases, the bulk elemental composition is usually unchanged. Hence, monitoring oxidation state (or, more generally, other chemical modifications) can be of great importance. Recent applications of XAS in art conservation are reviewed and new trends are discussed, highlighting the value (and future possibilities) of XAS, which remains, given its potential, underutilized in the CH community. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000278842500003 |
Publication Date |
2010-01-08 |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
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Edition |
|
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| |
ISSN |
0001-4842 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
20.268 |
Times cited |
74 |
Open Access |
|
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| |
Notes |
; ; |
Approved |
Most recent IF: 20.268; 2010 IF: 21.852 |
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| |
Call Number |
UA @ admin @ c:irua:83982 |
Serial |
5861 |
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| Permanent link to this record |
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| |
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Author |
Vandeputte, D.F.; Verbueken, A.H.; Jacob, W.A.; Van Grieken, R.E. |
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| |
Title |
Laser microprobe mass analysis (LAMMA) to study lead intoxication at the subcellular level |
Type |
A3 Journal article |
| |
Year |
1986 |
Publication |
Acta pharmacologica et toxicologica |
Abbreviated Journal |
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| |
Volume |
59 |
Issue |
S:7 |
Pages |
617-619 |
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| |
Keywords |
A3 Journal article; Pharmacology. Therapy; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
2010-07-29 |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
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Series Issue |
|
Edition |
|
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| |
ISSN |
0001-6683 |
ISBN |
|
Additional Links |
UA library record |
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| |
Impact Factor |
|
Times cited |
|
Open Access |
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| |
Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:116771 |
Serial |
8158 |
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| Permanent link to this record |
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Author |
Bottari, F.; Daems, E.; de Vries, A.-M.; Van Wielendaele, P.; Trashin, S.; Blust, R.; Sobott, F.; Madder, A.; Martins, J.C.; De Wael, K. |
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Title |
Do aptamers always bind? The need for a multifaceted analytical approach when demonstrating binding affinity between aptamer and low molecular weight compounds |
Type |
A1 Journal article |
| |
Year |
2020 |
Publication |
Journal Of The American Chemical Society |
Abbreviated Journal |
J Am Chem Soc |
|
| |
Volume |
142 |
Issue |
46 |
Pages |
jacs.0c08691-19630 |
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| |
Keywords |
A1 Journal article; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Medical Biochemistry |
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| |
Abstract |
In this manuscript, we compare different analytical methodologies to validate or disprove the binding capabilities of aptamer sequences. This was prompted by the lack of a universally accepted and robust quality control protocol for the characterization of aptamer performances coupled with the observation of independent yet inconsistent data sets in the literature. As an example, we chose three aptamers with a reported affinity in the nanomolar range for ampicillin, a β-lactam antibiotic, used as biorecognition elements in several detection strategies described in the literature. Application of a well-known colorimetric assay based on aggregation of gold nanoparticles (AuNPs) yielded conflicting results with respect to the original report. Therefore, ampicillin binding was evaluated in solution using isothermal titration calorimetry (ITC), native nano-electrospray ionization mass spectrometry (native nESI-MS), and 1H-nuclear magnetic resonance spectroscopy (1H NMR). By coupling the thermodynamic data obtained with ITC with the structural information on the binding event given by native nESI-MS and 1H NMR we could verify that none of the ampicillin aptamers show any specific binding with their intended target. The effect of AuNPs on the binding event was studied by both ITC and 1H NMR, again without providing positive evidence of ampicillin binding. To validate the performance of our analytical approach, we investigated two well-characterized aptamers for cocaine/quinine (MN4), chosen for its nanomolar range affinity, and l-argininamide (1OLD) to show the versatility of our approach. The results clearly indicate the need for a multifaceted analytical approach, to unequivocally establish the actual detection potential and performance of aptamers aimed at small organic molecules. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000592911000024 |
Publication Date |
2020-11-09 |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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| |
Series Volume |
|
Series Issue |
|
Edition |
|
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| |
ISSN |
0002-7863 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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| |
Impact Factor |
15 |
Times cited |
|
Open Access |
|
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| |
Notes |
|
Approved |
Most recent IF: 15; 2020 IF: 13.858 |
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| |
Call Number |
UA @ admin @ c:irua:173136 |
Serial |
6488 |
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| Permanent link to this record |
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Author |
Johansson, T.B.; Nelson, J.W.; Van Grieken, R.E.; Winchester, J.W. |
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| |
Title |
Elemental analysis of aerosol-size fractions by proton-induced X-ray-emission |
Type |
A1 Journal article |
| |
Year |
1973 |
Publication |
Transactions of the American Nuclear Society |
Abbreviated Journal |
|
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| |
Volume |
17 |
Issue |
Nov |
Pages |
103-103 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Editor |
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Wos |
A1973R161300114 |
Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-018x |
ISBN |
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Additional Links |
UA library record; WoS full record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:113643 |
Serial |
7880 |
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Author |
Rather, J.A.; Pilehvar, S.; De Wael, K. |
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Title |
A biosensor fabricated by incorporation of a redox mediator into a carbon nanotube/nafion composite for tyrosinase immobilization : detection of matairesinol, an endocrine disruptor |
Type |
A1 Journal article |
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Year |
2013 |
Publication |
The analyst |
Abbreviated Journal |
Analyst |
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Volume |
238 |
Issue |
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Pages |
204-210 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
An electrochemical matairesinol biosensor was fabricated by immobilizing tyrosinase on a poly(thionine)/nafion/multi-walled carbon nanotube composite film. A polymeric film of the redox dye thionine enables the stable immobilization of tyrosinase while acting as a mediator for the enzymatic process has been incorporated into the carbon nanotube/nafion composite film. The immobilization method is based on crosslinking of the tyrosinase layer with an electropolymerized film of poly(thionine). The good homogenization of the electron conductor CNTs in the integrated films provides the possibility of a three-dimensional electron conductive network. The biosensor was characterized by electrochemical impedance spectroscopy and electrochemical characterization. The composite electrode exhibits catalytic activity, high sensitivity, stability and is applicable over a wide range of concentrations from 180 nM to 4.33 μM with a detection limit (LOD) of 37 nM. The obtained results suggest that the developed sensor can be successfully used for the determination of phenolic endocrine disruptors over a concentration range covering their environmental levels. |
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Wos |
000311823200025 |
Publication Date |
2012-10-26 |
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Series Title |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
0003-2654 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.885 |
Times cited |
23 |
Open Access |
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Notes |
; The authors are highly thankful for the mobility grant (Non-Europe Postdoc Fellowship) for one of the authors (Jahangir Ahmad Rather) supported by the Belgian Federal Science Policy (Belspo) co-funded by the Marie Curie Actions from the European Commission. ; |
Approved |
Most recent IF: 3.885; 2013 IF: 3.906 |
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Call Number |
UA @ admin @ c:irua:101648 |
Serial |
5490 |
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Author |
Florea, A.; Cowen, T.; Piletsky, S.; De Wael, K. |
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Title |
Electrochemical analysis of cocaine in real samples based on electrodeposited biomimetic affinity ligands |
Type |
A1 Journal article |
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Year |
2019 |
Publication |
The analyst |
Abbreviated Journal |
Analyst |
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Volume |
144 |
Issue |
15 |
Pages |
4639-4646 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
A selective electrochemical sensor for direct detection of cocaine was developed based on molecularly imprinted polymers electropolymerized onto graphene-modified electrodes. Palladium nanoparticles were integrated in the sensing layer for the benefit of enhancing the communication between imprinted sites and electrode and improving their homogenous distribution. The molecularly imprinted polymer was synthesized by cyclic voltammetry using p-aminobenzoic acid as high affinity monomer selected by computational modeling, and cocaine as template molecule. Experimental parameters related to the electrochemical deposition of palladium nanoparticles, pH, composition of electropolymerization mixture, extraction and rebinding condition were studied and optimized. Under optimized conditions the oxidation peak current varied linearly with cocaine concentration in the range of 100-500 µM, with a detection limit of 50 µM (RSD 0.71%, n=3). The molecularly imprinted sensor was able to detect cocaine in saliva and river water with good recoveries after sample pretreatment and was successfully applied for screening real street samples for cocaine. |
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Place of Publication |
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Wos |
000476812000021 |
Publication Date |
2019-06-10 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2654 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.885 |
Times cited |
3 |
Open Access |
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Notes |
; This project has received funding from the European Union's Horizon 2020 research and innovation programme under the Marie Sklodowska-Curie Grant Agreement No. 753223 Narcoreader. ; |
Approved |
Most recent IF: 3.885 |
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Call Number |
UA @ admin @ c:irua:160062 |
Serial |
5586 |
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| Permanent link to this record |
