Records |
Author |
Marchetti, A. |
Title |
Novel insights and approaches for the analytical characterization of tangible cultural heritage objects |
Type |
Doctoral thesis |
Year |
2021 |
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Pages |
333 p. |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Cultural heritage represents the vehicle of our cultural identity, handed over from past to future generations throughout human history. As a repository of fundamental cultural and social values, the preservation of all forms of cultural heritage is a responsibility of every society and of humankind as a whole. When it comes to tangible cultural heritage, preservation of heritage translates into preservation of objects and, therefore, of the materials they are constituted of. This crucial task relies heavily on the application of scientific analytical methods to answer material and conservation-related questions. The fundamental contribution of this analytical approach led, in the past decades, to an ever-deepening understanding of the factors governing the degradation of cultural heritage. However, the extreme complexity of the heritage object-environment system results in a massive research field, which inevitably presents relevant open questions. This is where the present PhD work comes into play, attempting to fill knowledge gaps in literature by starting from specific case studies and un-answered research questions. The multianalytical research conducted during this PhD unraveled fundamental information on the properties governing the reactivity and long-term behavior of different classes of materials, from α-brass in an indoor environment to artists’ pigments in the presence of light, moisture and soluble particulate matter (PM). The paramount importance of the synthesis conditions on the composition, physical properties and reactivity of heritage materials was also demonstrated, in particular for stable lead pyroantimonate and unstable Geranium lake artists’ pigments. Moreover, the study and characterization of specific heritage objects, namely a series of 16th century reliquary altarpieces and the painting L’Arlesienne, by Vincent Van Gogh, allowed to obtain relevant insights into their composition and on potential risks for their conservation. The challenging nature of the samples considered, created the perfect opportunity to test an innovative spectroscopic technique, optical photo-thermal IR (O-PTIR), for the characterization of heritage materials. Striking results were obtained, highlighting a great potential for the application of this non-destructive sub-micron molecular spectroscopy to the analysis of cultural heritage. Finally, in the last section of this work, strategies to implement the continuous monitoring of PM levels in indoor environmental quality studies were also considered, with a particular focus on the identification of environmental hazards for the collections housed in specific conservation environments (War Heritage Institute in Brussels and St. Martin’s church in Aalst, BE). |
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UA @ admin @ c:irua:177849 |
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8319 |
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Author |
Stosic, D. |
Title |
Numerical simulations of magnetic skyrmions in atomically-thin ferromagnetic films |
Type |
Doctoral thesis |
Year |
2018 |
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153 p. |
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Doctoral thesis; Condensed Matter Theory (CMT) |
Abstract |
Moore’s Law has driven the electronics industry for the past half century. However, the doubling of transistors about every two years is beginning to break down, owing to fundamental limits that arise as they approach the atomic length. As a result, the search for new pathways for electronics has become crucial. Among potential candidates, the discovery of magnetic textures known as skyrmions has attracted considerable interest and attention in spintronic technology, which relies on both the electron charge and its spin. The unusual topological and particle-like behavior launched skyrmions into the spotlight of scientific research. Topological protected stability, nanoscale size, and low driving currents needed to move them make skyrmions promising candidates for future consumer nanoelectronics. Recent advances in the field have provided all of the basic functions needed for carrying and processing information. In this thesis, we procure to advance the current understanding of skyrmion physics, and explore their potential to replace conventional electronics technology. First, the fundamental properties and lifetimes of racetrack skyrmions at room temperature are investigated. We discover that skyrmions can easily collapse at the boundary in laterally finite systems, and propose ways to improve their stability for constrained geometries. Then, pinning of single skyrmions on atomic defects of distinct origins are studied. We reveal that the preferred pinning positions depend on the skyrmion size and type of defect being considered, and discuss applications where control of skyrmions by defects is of particular interest. Next, we explore other magnetic configurations that can compete with skyrmions when considering new materials, and describe a previously unseen mechanism for collapse of skyrmions into cycloidal spin backgrounds. Finally, switching and interactions between skyrmions with distinct topologies are reported. We find that skyrmions transition to higher or lower topologies by absorbing a unit spin texture. The interactions between skyrmions of different topological charges can be attractive or repulsive, leading to the formation of arranged clusters. We conclude with a numerical library for simulating magnetic skyrmions in various scenarios. |
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UA @ admin @ c:irua:181142 |
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8322 |
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Author |
Cong, S. |
Title |
Numerical study on low-pressure hollow cathode argon arc plasma |
Type |
Doctoral thesis |
Year |
2021 |
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XIX, 126 p. |
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Doctoral thesis; Philosophy; Educational sciences; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
Abstract |
The low-pressure hollow cathode discharge made of a hollow circular tube and an anode is a type of simple structure discharge system. In particular, under the arc discharge mode, hollow cathodes have high plasma density and energy density with a wide range of adaptability of pressure and current. Low-pressure hollow cathode arc (HCA) discharges have been widely used as plasma sources in various fields such as manufacturing, vacuum welding, and aerospace since the 1960s. Despite the early experimental and applied researches on low-pressure HCA discharges, the basic theoretical study was relatively lagged much behind, resulting in many unanswered questions, such as the optimal discharge operating parameters, the power deposition inside the cathode, the causes of plasma instability, and how to effectively reduce cathode erosion and so on. Due to the special discharge structure of the hollow cathode, it is difficult to make an accurate experimental diagnosis, so a reasonable numerical simulation is an effective study method. However, up to now, there is still a lack of complete and effective numerical models which can evaluate various physical fields in the low-pressure hollow cathode discharges. To address the above problems and difficulties, a comprehensive and self-consistent 2D multi-physical coupling numerical model based on a commercial program of finite element method, the COMSOL Multiphysics, was provided in this paper. The model involves plasma transport, arc flow and heat transfer, and cathode thermal equilibrium, and can consider the effect of an applied magnetic field. The processes of secondary electron emission, thermal-field electron emission, ions and backflow high-energy electrons bombardment, and thermal radiation from the cathode surface are considered in the cathode thermal equilibrium process. Based on the above background, this paper works from the following aspects: In Chapter 1, the basic concepts of low-pressure HCA discharge including the hollow cathode effect, the basic characteristics, and operation modes were introduced firstly; Secondly, the application fields, development history, and overseas and domestic research status of hollow cathode discharge were reviewed; finally, the problems were presented and the research background was explained, and the research purpose of this paper was clarified. In Chapter 2, a complete and self-consistent numerical model of low-pressure hollow cathode discharge was proposed based on the fundamental theory and assumptions, and the set of control equations and boundary conditions in the model were elaborated. In addition, the electron energy distribution function, the collision processes, the solving tools of this model, and calculation schemes were introduced in detail. Finally, a validation example was given to test the rationality and applicability of the numerical model. In Chapter 3, the fundamental plasma properties of low-pressure hollow cathode arcs were investigated. Firstly, the ion Joule heating effect was studied. The results showed that the temperature distributions of the arc and cathode are only able to approach the experimental measurements after considering the ion Joule heating, which shows that the Joule heating of ions is crucial for the heating of the arc plasma. Secondly, by comparing the radial distribution of electron and ion density inside the cathode, the structure of the cathode sheath could be simulated well using this model. Finally, it was shown that the thermal radiation from the cathode surface is an important cooling mechanism of the cathode and only under higher surface emissivity can balance the larger heat flow given by the plasma to the cathode, and the temperature distribution of the cathode shows a non-monotonic increasing trend and is consistent with the profile of experimental measurement so that the so-called active zone is formed. In Chapter 4, the power deposition in the low-pressure HCA was studied in simulation. Two main aspects were considered: the power deposition into particles (both electrons and heavy particles) and the power deposition onto the cathode. It was found that the deposited power into particles increases with the rise of discharge current, but there is no effect on the total power deposition onto the cathode. In high-density plasmas, Coulomb collisions between electrons and ions also become very important, especially since a portion of the deposition energy on heavy particles comes mainly from the energy transfer from electrons to ions. It was also found that regardless of external parameters, half of the power deposition onto the cathode always comes from the particle contribution, while the other half is the net contribution of heat transfer and cathode radiation. The HCA model also allows the simulation of multiple discharge modes for low-pressure HCA discharges over a wide range of gas flow rates. It was also shown that the discharge operating conditions and the external magnetic field can change the distribution of the particle flow on the cathode wall. In Chapter 5, the ion sputtering erosion process on the cathode was simulated by coupling the HCA numerical model with the moving grid technique. The results showed that the ion sputtering erosion on the cathode depends on the ion flux and the plasma potential near the cathode wall and that their distribution and magnitude jointly determine the erosion morphology of the cathode. It was also found that the location of the most severe erosion on the cathode is located in the region of the densest ion flux on the cathode wall, rather than in the longitudinal correspondence with the central region of the internal positive column (IPC). The external magnetic fields can mitigate the cathode erosion and reduce the erosion depth, but stronger magnetic fields lead to a concentration of current density at the cathode tip, which can enhance erosion slightly at the cathode outlet end. Finally, the conclusions and innovation highlights were summarized, and prospects for future work were discussed. |
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Most recent IF: NA |
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UA @ admin @ c:irua:178725 |
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8323 |
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Author |
Van Grieken, R. |
Title |
Ocean-atmosphere interactions and oil pollution |
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P3 Proceeding |
Year |
1974 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117457 |
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8325 |
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Gielis, J.; Verhulst, R.; Caratelli, D.; Ricci, P.E.; Tavkhelidze, I. |
Title |
On means, polynomials and special functions |
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A1 Journal article |
Year |
2014 |
Publication |
The teaching of mathematics |
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17 |
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1 |
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1-20 |
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A1 Journal article; Educational sciences; Sustainable Energy, Air and Water Technology (DuEL) |
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1451-4966; 2406-1077 |
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UA @ admin @ c:irua:128660 |
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8327 |
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Deutsch, F.; Stranger, M.; Kaplinskii, A.E.; Samek, L.; Joos, P.; Van Grieken, R. |
Title |
On the impact of precipitation amount on the concentration of elements and ions in urban aerosol particles |
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A3 Journal article |
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2003 |
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Atmospheric and oceanic optics |
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16 |
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10 |
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850-855 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:43561 |
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8330 |
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Van Grieken, R.; Speecke, A.; Hoste, J. |
Title |
On the precision of oxygen determinations in steel by 14-MeVv neutron activation |
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A1 Journal article |
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1970 |
Publication |
Analytica chimica acta |
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52 |
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2 |
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275-280 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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The precision of the 14-MeV neutron activation determination of oxygen in steel has been examined as a function of the oxygen content for a large number of steel and cast iron samples. The experimental and the statistically expected standard deviations have been compared. In the conditions used, 2.5 counts from 16N were registered for each p.p.m. of oxygen in the samples. The neutron flux was monitored by a simultaneously irradiated oxygen standard. |
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2002-07-25 |
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0003-2670; 1873-4324 |
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UA @ admin @ c:irua:116362 |
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8332 |
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de Hoog, J.; Osán, J.; Worobiec, A.; Ro, C.-U.; Szalóki, I.; Joos, P.; Van Grieken, R. |
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Optimisation of light element analysis of individual particles using UTW-EPMA |
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A1 Journal article |
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2000 |
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Journal of aerosol science |
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31 |
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S1 |
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388-389 |
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A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0021-8502; 1879-1964 |
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UA @ admin @ c:irua:31642 |
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8336 |
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Robberecht, H.; Van Grieken, R.; Van der Sloot, H.A. |
Title |
OPtimized selenite determination in environmental waters by X-ray fluorescence |
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H3 Book chapter |
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1980 |
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463-468
T2 - Analytical techniques in environmenta |
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H3 Book chapter; Pharmacology. Therapy; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117482 |
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8343 |
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Kontozova, V.; Godoi, R.; Krata, A.; Van Grieken, R. |
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Oszklenie ochronne i jego wpływ na średniowieczne okna witrazowe: z perspektywy chemii atmosfery: studium przypadku kaplica Sainte Chapelle w Paryzu |
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A3 Journal article |
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2007 |
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Analityka |
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3 |
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20-25 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:65079 |
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8349 |
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Mozo, I.; Lacoste, L.; Aussenac, J.; De Cocker, P.; Vlaeminck, S.E.; Sperandio, M.; Caligaris, M.; Barillon, B.; Martin Ruel, S. |
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Overcoming the challenges for mainstream deammonification on municipal wastewater in warm and cold areas |
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P3 Proceeding |
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2016 |
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3 p.
T2 - 13th IWA Leading-Edge Conference on Wate |
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P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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UA @ admin @ c:irua:151137 |
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8351 |
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Margui, E.; Van Grieken, R. |
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Overview of most commonly used analytical techniques for elemental analysis |
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A3 Journal article |
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2014 |
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Petro Industry News |
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8-10 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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1472-0590 |
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UA @ admin @ c:irua:114599 |
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8352 |
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Mabesoone, J.M.; Farias, C.C.; Van Grieken, R.; Duarte, P.J.; Delgado, A.; Freira, E.M.P. |
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Parnaiba Basin shales (Northeast Brazil) |
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A1 Journal article |
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1985 |
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Anais da Academia Brasileira de Ciências |
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57 |
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481-495 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0001-3765; 1678-2690 |
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UA @ admin @ c:irua:116716 |
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8357 |
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Wegrzynek, D.; Van Grieken, R.; Eisma, D. |
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Particle analysis of sediments from the Gulf of Lions, suspended matter from the Rhone river, and Sahara dust |
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H3 Book chapter |
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1994 |
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51-60
T2 - Particles and particle-water interactio |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:9525 |
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8358 |
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Dekov, V.; van Alsenoy, V.; Onar, N.; van Put, A.; Van Grieken, R. |
Title |
Partitioning of heavy metals between estuarine sediments and dissolved phase as a function of salinity, pH and time (Scheldt estuary) |
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A1 Journal article |
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2001 |
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Geologica Balcanica |
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30 |
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3/4 |
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65-76 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISSN |
0324-0894 |
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UA library record |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:36086 |
Serial |
8362 |
Permanent link to this record |
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|
|
Author |
Verreydt, G.; Bronders, J.; van Keer, I.; Diels, L.; Vanderauwera, P. |
Title |
Passive samplers for monitoring VOCs in groundwater : prospects related to mass flux measurements |
Type |
P3 Proceeding |
Year |
2011 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
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Keywords |
P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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|
ISBN |
978-1-907161-16-2 |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:110412 |
Serial |
8364 |
Permanent link to this record |
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|
|
Author |
van de Vijver, F.L.; Vanheule, A.O.; Verbueken, A.H.; Van Grieken, R.; d'Haese, P.; Visser, W.J.; Bekaert, A.B.; Buyssens, N.; de Broe, M.E. |
Title |
Patterns of iron storage in patients with severe renal failure |
Type |
A1 Journal article |
Year |
1984 |
Publication |
Contributions to nephrology |
Abbreviated Journal |
|
Volume |
38 |
Issue |
|
Pages |
153-166 |
Keywords |
A1 Journal article; Pharmacology. Therapy; Pathophysiology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Abbreviated Series Title |
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|
Edition |
|
ISSN |
0302-5144 |
ISBN |
|
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UA library record |
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|
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|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116707 |
Serial |
8366 |
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|
|
Author |
Buysse, C. |
Title |
Perovskite capillaries for gas separation in sustainable energy production |
Type |
Doctoral thesis |
Year |
2011 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
201 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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|
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|
Approved |
no |
Call Number |
UA @ admin @ c:irua:90548 |
Serial |
8373 |
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|
|
Author |
Brunekreef, B.; Janssen, N., A.H.; de Hartog, J., J.; Oldenwening, M.; Meliefste, K.; Hoek, G.; Lanki, T.; Timonen, K., L.; Vallius, M.; Pekkanen, J.; Van Grieken, R. |
Title |
Personal, indoor, and outdoor exposures to PM2.5 and its components for groups of cardiovascular patients in Amsterdam and Helsinki |
Type |
Minutes and reports |
Year |
2005 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
|
Keywords |
Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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|
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|
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|
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:51816 |
Serial |
8374 |
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|
|
Author |
Vanderborght, B.; Van Grieken, R. |
Title |
Perspectieven voor energie-dispersieve X-stralen fluorescentie bij de wateranalyse |
Type |
A3 Journal article |
Year |
1975 |
Publication |
Hydrographica |
Abbreviated Journal |
|
Volume |
1 |
Issue |
|
Pages |
19-26 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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|
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|
Additional Links |
UA library record |
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|
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116643 |
Serial |
8375 |
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|
|
Author |
Vandeputte, D.F.; Jacob, W.A.; Van Grieken, R.E. |
Title |
Phosphorus, calcium and lead distribution in collagen in lead induced soft tissue calcification : an ultrastructural and X-ray microanalytical study |
Type |
A1 Journal article |
Year |
1990 |
Publication |
Matrix |
Abbreviated Journal |
|
Volume |
10 |
Issue |
1 |
Pages |
33-37 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Repeated intraperitoneal injections of lead acetate in rats caused a calcification of the skin of the abdomen near the site of the injections. In the lead-induced calcifications, electron dense collagen bundles could be observed. On the surface of the collagen fibrils, needle-like crystals were visible. With energy-dispersive X-ray analysis, phosphorus, calcium and lead were detected in the electron dense collagen bundles. X-ray maps of the P-Kα, Ca-Kα, and Pb-Lα plus Pb-Lβ lines showed an equivalent distribution along the collagen fibrils for phosphorus and calcium. The occurrence of the most electron dense areas in the STEM-image was comparable to the lead distribution. A good correlation existed between the structural and the elemental images of the same area. Although the medicinal use of preparations containing lead is no longer recommended, some are still prescribed. From our results we can conclude that they should not be applied to injured or inflamed skin. |
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2012-04-16 |
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ISSN |
0934-8832 |
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|
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116930 |
Serial |
8377 |
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Author |
Van Hal, M. |
Title |
Photo(electro)catalytic air purification and soot degradation with simultaneous energy recovery |
Type |
Doctoral thesis |
Year |
2021 |
Publication |
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Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
XXXII, 203 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
Abstract |
Today’s society is increasingly challenged by a range of urgent environmental problems. Air pollution is one of these pressing topics. This thesis will mainly focus on the degradation of volatile organic compounds (VOCs) and particulate matter (PM) – more specifically soot. A second globally urging topic is the quest for sustainable energy production. To simultaneously target both environmental problems, a photoelectrochemical (PEC) cell will be studied in this thesis, combining air purification and sustainable energy production in a single device. Photocatalysis is used at the anode of the PEC cell to drive the air purification process, while the energy contained in the degraded compounds is (partially) recovered at the cathode, either as H2 gas or electricity. The first two experimental chapters focus on the proof of concept of such an unbiased all-gas phase PEC cell targeting VOC degradation, using both TiO2- and WO3-based photocatalysts. In the two following experimental chapters the photocatalytic soot oxidation capacity of these TiO2- and WO3-based photocatalysts was studied. In the final experimental chapter the previously obtained results were combined, striving towards an efficient, sunlight-driven and soot-degrading waste gas-to-energy PEC cell. |
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Approved |
Most recent IF: NA |
Call Number |
UA @ admin @ c:irua:184521 |
Serial |
8378 |
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Author |
Smits, M. |
Title |
Photocatalytic degradation of diesel soot : from application to reaction mechanism |
Type |
Doctoral thesis |
Year |
2013 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
160 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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Abbreviated Series Title |
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Edition |
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ISSN |
|
ISBN |
978-90-5728-415-1 |
Additional Links |
UA library record |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:108803 |
Serial |
8380 |
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Author |
Liu, X.; Van Winckel, T.; Kjellerup, B.V.; Takacs, I.; Sturm, B.; Vlaeminck, S.E.; Al-Omari, A.; Murthy, S.; De Clippeleir, H. |
Title |
Pinpointing bioflocculation limitations for enhanced carbon management in high-rate activated sludge |
Type |
P3 Proceeding |
Year |
2017 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
6 p.
T2 - WEF Nutrient Symposium 2017, 12 - 14 Jun |
Keywords |
P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:151118 |
Serial |
8384 |
Permanent link to this record |
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|
Author |
Belov, I. |
Title |
Plasma-assisted conversion of carbon dioxide |
Type |
Doctoral thesis |
Year |
2017 |
Publication |
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Pages |
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Doctoral thesis; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:146275 |
Serial |
8387 |
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Author |
Van Wesenbeeck, K. |
Title |
Plasma catalysis as an efficient and sustainable air purification technology |
Type |
Doctoral thesis |
Year |
2016 |
Publication |
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Abbreviated Journal |
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Volume |
|
Issue |
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Pages |
171 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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|
ISBN |
978-90-5728-514-1 |
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UA library record |
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|
Approved |
no |
Call Number |
UA @ admin @ c:irua:135267 |
Serial |
8388 |
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Author |
Blommaerts, N. |
Title |
Plasmonic core shell nanoparticles : from synthesis to photocatalytic applications |
Type |
Doctoral thesis |
Year |
2019 |
Publication |
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Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
153 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
Abstract |
Het gebruik van plasmon-actieve nanodeeltjes heeft de laatste 10 jaar zeer veel interesse gewekt bij onderzoekers in verschillende toepassingsdomeinen zoals fotokatalyse of oppervlakte versterkte Raman spectroscopie. Er is echter een grote limiterende factor bij het gebruik van edelmetaal nanodeeltjes zoals goud en zilver en dat is de stabiliteit. Deze oxideren en aggregeren snel, zeker in oxidatieve omgeving zoals in lucht. Een interessante aanpak om plasmon-actieve nanodeeltjes te stabiliseren, is om ze te omgeven in een schil, met andere woorden om een kern-schil nanodeeltje te vormen. Er zijn een heel aantal verschillende manieren waarop kern-schil nanodeeltjes gesynthetiseerd kunnen worden. In eerste instantie werden metaal nanodeeltjes omgeven door een (dunne) TiO2 laag. Afhankelijk van de hoeveelheid TiO2 precursor kon de dikte van de laag gecontroleerd worden tot enkele nanometers dik. De stalen werden getest voor de fotokatalytische afbraak van een vaste laag stearinezuur waarbij toevoeging van 2 wt% metaal@TiO2 op P25 leidde tot een significante verbetering in afbraakefficiëntie in vergelijking met zuiver P25. Een andere manier voor het stabiliseren van metaal nanodeeltjes is door ze te omgeven met een polymeerschil. Op deze manier kon de laagdikte gecontroleerd worden met sub-nanometer controle wat een zeer belangrijke factor is voor de hoeveelheid near-field versterking dat buiten de polymeer schil kan gaan. Een XTT test werd uitgevoerd om te bepalen wat de zuurstofactivatie snelheid was van goud en zilver (en goud-zilver bimetallische) nanodeeltjes, al dan niet omgeven door een (niet-)geleidende polymeer laag. Wanneer de stalen gecoat werden met vier niet-geleidende polymeerlagen zakte de zuurstofactivatie nagenoeg tot nul. Aan de andere kant, als goud nanodeeltjes werden omgeven door een geleidende schil was er nog steeds zuurstofactivatie, hoewel lager dan in het geval van goud zonder laag. Het laatste deel van deze thesis focuste meer op mogelijke toepassingen in luchtzuivering. In dit werk werd een glazen buis, gecoat aan de binnenkant met (Ag@polymer gemodificeerd) TiO2, als een spiraal rond een UVA lamp gewikkeld. De geoptimaliseerde spiraalreactor werd dan vergeleken met een conventionele cilindervormige fotoreactor, met dezelfde dimensies en totale katalysatorbelading, over een grote range aan experimentele condities. Uit de resultaten bleek dat de spiraalreactor significant betere afbraakefficiënties vertoonde in vergelijking met de conventionele cilindervormige reactor over een grote range aan debieten. Een adsorptiestap in combinatie met de geoptimaliseerde spiraalreactor zou kunnen leiden tot een zeer krachtige luchtzuiveringstechnologie. |
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no |
Call Number |
UA @ admin @ c:irua:164835 |
Serial |
8389 |
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Author |
Bencs, L.; Ravindra, K.; Van Grieken, R. |
Title |
Platinum : environmental pollution and health effects |
Type |
H2 Book chapter |
Year |
2011 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
580-595
T2 - Encyclopedia of environmental health |
Keywords |
H2 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISBN |
978-0-444-52273-3 |
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|
Approved |
no |
Call Number |
UA @ admin @ c:irua:93109 |
Serial |
8390 |
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Author |
Trincavelli, J.; Montoro, S.; Van Grieken, R.; van Espen, P. |
Title |
Prediction of Mα/Lα intensity ratios and the use in the spectra evaluation |
Type |
P3 Proceeding |
Year |
1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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no |
Call Number |
UA @ admin @ c:irua:2863 |
Serial |
8405 |
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Author |
Goossenaerts, C.; Verbueken, A.; Van Grieken, R. |
Title |
Preliminary LAMMA investigations on healthy and acid rain affected spruce needles |
Type |
P3 Proceeding |
Year |
1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117511 |
Serial |
8409 |
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