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Author Cao, S.; Nishida, M.; Schryvers, D. pdf  doi
openurl 
  Title Quantitative three-dimensional analysis of Ni4Ti3 precipitate morphology and distribution in polycrystalline Ni-Ti Type A1 Journal article
  Year 2011 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 59 Issue 4 Pages 1780-1789  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract The three-dimensional size, morphology and distribution of Ni4Ti3 precipitates in a Ni50.8Ti49.2 polycrystalline shape memory alloy with a heterogeneous microstructure have been investigated using a focused ion beam/scanning electron microscopy slice-and-view procedure. The mean volume, central plane diameter, thickness, aspect ratio and sphericity of the precipitates in the grain interior as well as near to the grain boundary were measured and/or calculated. The morphology of the precipitates was quantified by determining the equivalent ellipsoids with the same moments of inertia and classified according to the Zingg scheme. Also, the pair distribution functions describing the three-dimensional distributions were obtained from the coordinates of the precipitate mass centres. Based on this new data it is suggested that the existence of the heterogeneous microstructure could be due to a very small concentration gradient in the grains of the homogenized material and that the resulting multistage martensitic transformation originates in strain effects related to the size of the precipitates and scale differences of the available B2 matrix in between the precipitates.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000287265100045 Publication Date 2010-12-20  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 34 Open Access  
  Notes Fwo Approved Most recent IF: 5.301; 2011 IF: 3.755  
  Call Number UA @ lucian @ c:irua:85533 Serial 2766  
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Author Malard, B.; Pilch, J.; Sittner, P.; Delville, R.; Curfs, C. pdf  doi
openurl 
  Title In situ investigation of the fast microstructure evolution during electropulse treatment of cold drawn NiTi wires Type A1 Journal article
  Year 2011 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 59 Issue 4 Pages 1542-1556  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract Microstructural changes taking place during the heat treatment of cold-worked NiTi alloy are of key interest in shape memory alloy technology, since they are responsible for setting the austenite shape and functional properties of the heat-treated alloy. In this work, microstructural evolution during non-conventional electropulse heat treatment of thin NiTi filaments was investigated in a unique high-speed in situ synchrotron X-ray diffraction experiment with simultaneous evaluation of the tensile force and electrical resistivity of the treated wire. The in situ results provide direct experimental evidence on the evolution of the internal stress and density of defects during fast heating from 20 °C to ∼700 °C. This evidence is used to characterize a sequence of dynamic recovery and recrystallization processes responsible for the microstructure and superelastic functional property changes during the electropulse treatments.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000287265100023 Publication Date 2010-12-11  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 48 Open Access  
  Notes Approved Most recent IF: 5.301; 2011 IF: 3.755  
  Call Number UA @ lucian @ c:irua:98372 Serial 1583  
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Author Delville, R.; Malard, B.; Pilch, J.; Schryvers, D. pdf  doi
openurl 
  Title Microstructure changes during non-conventional heat treatment of thin NiTi wires by pulsed electric current studied by transmission electron microscopy Type A1 Journal article
  Year 2010 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 58 Issue 13 Pages 4503-4515  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract Transmission electron microscopy, electrical resistivity measurements and mechanical testing were employed to investigate the evolution of microstructure and functional superelastic properties of 0.1 mm diameter as-drawn NiTi wires subjected to a non-conventional heat treatment by controlled electric pulse currents. This method enables a better control of the recovery and recrystallization processes taking place during the heat treatment and accordingly a better control on the final microstructure. Using a stepwise approach of millisecond pulse annealing, it is shown how the microstructure evolves from a severely deformed state with no functional properties to an optimal nanograined microstructure (2050 nm) that is partially recovered through polygonization and partially recrystallized and that has the best functional properties. Such a microstructure is highly resistant against dislocation slip upon cycling, while microstructures annealed for longer times and showing mostly recrystallized grains were prone to dislocation slip, particularly as the grain size exceeds 200 nm.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000279787100020 Publication Date 2010-06-02  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 110 Open Access  
  Notes Multimat; FWO IAA Approved Most recent IF: 5.301; 2010 IF: 3.791  
  Call Number UA @ lucian @ c:irua:83279 Serial 2062  
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Author Idrissi, H.; Renard, K.; Ryelandt, L.; Schryvers, D.; Jacques, P.J. pdf  doi
openurl 
  Title On the mechanism of twin formation in FeMnC TWIP steels Type A1 Journal article
  Year 2010 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 58 Issue 7 Pages 2464-2476  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract Although it is well known that FeMnC TWIP steels exhibit high work-hardening rates, the elementary twinning mechanisms controlling the plastic deformation of these steels have still not been characterized. The aim of the present study is to analyse the extended defects related to the twinning occurrence using transmission electron microscopy. Based on these observations, the very early stage of twin nucleation can be attributed to the pole mechanism with deviation proposed by Cohen and Weertman or to the model of Miura, Takamura and Narita, while the twin growth is controlled by the pole mechanism proposed by Venables. High densities of sessile Frank dislocations are observed within the twins at the early stage of deformation, which can affect the growth and the stability of the twins, but also the strength of these twins and their interactions with the gliding dislocations present in the matrix. This experimental evidence is discussed and compared to recent results in order to relate the defects analysis to the macroscopic behaviour of this category of material.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000276523200018 Publication Date 2010-01-25  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 244 Open Access  
  Notes Iap Approved Most recent IF: 5.301; 2010 IF: 3.791  
  Call Number UA @ lucian @ c:irua:82270 Serial 2441  
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Author Bartova, B.; Wiese, N.; Schryvers, D.; Chapman, J.N.; Ignacova, S. pdf  doi
openurl 
  Title Microstructure of precipitates and magnetic domain structure in an annealed Co38Ni33Al29 shape memory alloy Type A1 Journal article
  Year 2008 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 56 Issue 16 Pages 4470-4476  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract The microstructure of a Co38Ni33Al29 ferromagnetic shape memory alloy was determined by conventional transmission electron microscopy (TEM), electron diffraction studies together with advanced microscopy techniques and in situ Lorentz microscopy. Rod-like precipitates, 1060 nm long, of hexagonal close-packed -Co were confirmed to be present by high-resolution TEM. The orientation relationship between the precipitates and B2 matrix is described by the Burgers orientation relationship. The crystal structure of the martensite obtained after cooling is tetragonal L10 with a (111) twinning plane. The magnetic domain structure was determined during an in situ cooling experiment using the Fresnel mode of Lorentz microscopy. While transformation proceeds from B2 austenite to L10 martensite, new domains are nucleated, leading to a decrease in domain width, with the magnetization lying predominantly along a single direction. It was possible to completely describe the relationship between magnetic domains and crystallographic directions in the austenite phase though complications existed for the martensite phase.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000259931300033 Publication Date 2008-06-11  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 23 Open Access  
  Notes Multimat Approved Most recent IF: 5.301; 2008 IF: 3.729  
  Call Number UA @ lucian @ c:irua:72321 Serial 2072  
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Author Yang, Z.; Tirry, W.; Lamoen, D.; Kulkova, S.; Schryvers, D. pdf  doi
openurl 
  Title Electron energy-loss spectroscopy and first-principles calculation studies on a Ni-Ti shape memory alloy Type A1 Journal article
  Year 2008 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 56 Issue 3 Pages 395-404  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000253020900011 Publication Date 2007-12-01  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 20 Open Access  
  Notes Goa; Ec Rtn; Fwo Approved Most recent IF: 5.301; 2008 IF: 3.729  
  Call Number UA @ lucian @ c:irua:67462 Serial 931  
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Author Rotaru, G.-M.; Tirry, W.; Sittner, P.; van Humbeeck, J.; Schryvers, D. pdf  doi
openurl 
  Title Microstructural study of equiatomic PtTi martensite and the discovery of a new long-period structure Type A1 Journal article
  Year 2007 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 55 Issue 13 Pages 4447-4454  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000248436400021 Publication Date 2007-06-04  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 7 Open Access  
  Notes Fwo G.0465.05; Multimat Approved Most recent IF: 5.301; 2007 IF: 3.624  
  Call Number UA @ lucian @ c:irua:65849 Serial 2047  
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Author Viart, N.; Sayed Hassan, R.; Ulhaq-Bouillet, C.; Meny, C.; Panissod, P.; Loison, J.L.; Versini, G.; Huber, F.; Pourroy, G.; Verbeeck, J.; Van Tendeloo, G. pdf  doi
openurl 
  Title Oxidation processes at the metal/oxide interface in CoFe2/CoFe2O4 bilayers deposited by pulsed laser deposition Type A1 Journal article
  Year 2006 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 54 Issue 1 Pages 191-196  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract CoFe2/CoFe2O4 bilayers were made by pulsed laser ablation of a CoFe2 target on Si(I 0 0) substrates. The metallic layer was deposited first, in vacuum. The oxide was then deposited in an oxidizing O-2:N-2 (20:80) atmosphere. Two different procedures were used for the introduction of the oxidizing atmosphere in the deposition chamber: the laser ablation of the target was either stopped (discontinuous deposition process) or maintained (continuous deposition process) during the 20 min necessary for the establishment of the desired O-2:N-2 pressure. In both cases, the different electronegativities of Fe and Co cause an important modification of the Fe/Co ratio at the metal/oxide interface, with a depletion of Fe in the metal region and of Co in the oxide region. In the continuous procedure, the combination of the kinetic energy given by the ablation process to the Fe and Co adatoms with the one they get from their different affinity towards oxidation allows the formation of a low roughness metal/oxide interface with a high (111) preferred orientation of the CoFe2O4 layer, an induced re-crystallisation of the metal layer underneath and an unusual antiferromagnetic metal/oxide magnetic coupling. (c) 2005 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000233784500021 Publication Date 2005-10-15  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 5 Open Access  
  Notes Approved Most recent IF: 5.301; 2006 IF: 3.549  
  Call Number UA @ lucian @ c:irua:56043UA @ admin @ c:irua:56043 Serial 2540  
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Author Tirry, W.; Schryvers, D. pdf  doi
openurl 
  Title Quantitative determination of strain fields around Ni4Ti3 precipitates in NiTi Type A1 Journal article
  Year 2005 Publication Acta materialia Abbreviated Journal Acta Mater  
  Volume 53 Issue 4 Pages 1041-1049  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Oxford Editor  
  Language Wos 000226774500014 Publication Date 2004-12-14  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1359-6454; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 5.301 Times cited 97 Open Access  
  Notes Approved Most recent IF: 5.301; 2005 IF: 3.430  
  Call Number UA @ lucian @ c:irua:55686 Serial 2750  
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