| Records |
| Author |
Robberecht, H.; Van Grieken, R. |
| Title |
Determination of trace selenium in biological material by preconcentration and X-ray emission spectrometry |
Type |
A1 Journal article |
| Year |
1983 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
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| Volume |
147 |
Issue |
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Pages |
113-121 |
| Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
| Abstract |
Selenium is determined in the ng g−1 to μg g−1 range in biological and environmental samples. A wet digestion procedure was optimized with respect to volatility losses and recovery yields, by using 75Se metabolically incorporated into rat organs. Selenium is preconcentrated from the digestion liquid by a two-step reduction with 4 M HCl and ascorbic acid. The colloidal selenium formed is adsorbed on activated carbon and filtered on a Nucleopore membrane for measurement by energy-dispersive x-ray fluorescence. Almost complete recovery was obtained, and the detection limit was 20 ng, corresponding to 10 ng g−1 for a 2-g sample. Biological reference materials were analyzed with satisfactory results, and the accuracy of the method was good. |
| Address |
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Place of Publication |
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Wos |
A1983QH42100010 |
Publication Date |
2002-07-25 |
| Series Editor |
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Series Title |
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Abbreviated Series Title |
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| Series Volume |
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Series Issue |
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Edition |
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| ISSN |
0003-2670; 1873-4324 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
| Impact Factor |
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Times cited |
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Open Access |
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Notes  |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:116442 |
Serial |
7794 |
| Permanent link to this record |
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| Author |
Robberecht, H.; Van Grieken, R. |
| Title |
Selenium content and speciation in environmental waters determied by X-ray fluorescence spectroscopy |
Type |
H3 Book chapter |
| Year |
1980 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
362-366
T2 - Trace substances in environmental hea |
| Keywords |
H3 Book chapter; Pharmacology. Therapy; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
| Abstract |
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Wos |
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Publication Date |
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Series Title |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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| ISSN |
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ISBN |
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Additional Links |
UA library record |
| Impact Factor |
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Times cited |
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Open Access |
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| Notes |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:117481 |
Serial |
8505 |
| Permanent link to this record |
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| Author |
Robberecht, H.; Van Grieken, R. |
| Title |
Selenium in environmental waters : determination, speciation and concentration levels |
Type |
A1 Journal article |
| Year |
1982 |
Publication |
Talanta : the international journal of pure and applied analytical chemistry |
Abbreviated Journal |
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| Volume |
29 |
Issue |
10 |
Pages |
823-844 |
| Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
| Abstract |
This article reviews the different methods used for the determination of selenium species in all types of environmental waters. Basic difficulties are discussed and the efficiency of the methods is explained in view of the sub-μg/1. concentration levels. Special attention is paid to preconcentration steps. Published data on speciation and concentration levels in various water samples are critically reviewed. |
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Thesis |
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| Publisher |
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Place of Publication |
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Editor |
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| Language |
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Wos |
A1982PK22900004 |
Publication Date |
2002-07-25 |
| Series Editor |
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Series Title |
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Abbreviated Series Title |
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| Series Volume |
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Series Issue |
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Edition |
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| ISSN |
0039-9140; 1873-3573 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
| Impact Factor |
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Times cited |
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Open Access |
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| Notes |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:113627 |
Serial |
8509 |
| Permanent link to this record |
