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Author Choël, M.; Deboudt, K.; Osán, J.; Flament, P.; Van Grieken, R.
Title Quantitative determination of low-Z elements in single atmospheric particles on boron substrates by automated scanning electron microscopy: energy-dispersive X-ray spectrometry Type A1 Journal article
Year 2005 Publication Analytical chemistry Abbreviated Journal
Volume 77 Issue 17 Pages 5686-5692
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000231652300046 Publication Date 2005-08-31
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:53593 Serial 8443
Permanent link to this record
 
 
Author Damla, N.; Čevik, U.; Kobya, A.I.; Celik, A.; Celik, N.; Van Grieken, R.
Title Radiation dose estimation and mass attenuation coefficients of cement samples used in Turkey Type A1 Journal article
Year 2010 Publication Journal of hazardous materials Abbreviated Journal
Volume 176 Issue 1/3 Pages 644-649
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract Different cement samples commonly used in building construction in Turkey have been analyzed for natural radioactivity using gamma-ray spectrometry. The mean activity concentrations observed in the cement samples were 52, 40 and 324 Bq kg−1 for 226Ra, 232Th and 40K, respectively. The measured activity concentrations for these radionuclides were compared with the reported data of other countries and world average limits. The radiological hazard parameters such as radium equivalent activities (Raeq), gamma index (Iγ) and alpha index (Iα) indices as well as terrestrial absorbed dose and annual effective dose rate were calculated and compared with the international data. The Raeq values of cement are lower than the limit of 370 Bq kg−1, equivalent to a gamma dose of 1.5 mSv y−1. Moreover, the mass attenuation coefficients were determined experimentally and calculated theoretically using XCOM in some cement samples. Also, chemical compositions analyses of the cement samples were investigated.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000274839700087 Publication Date 2009-11-20
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0304-3894 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:80671 Serial 8448
Permanent link to this record
 
 
Author Lins Galdino, S.M.; Costa Dantas, C.; Van Grieken, R.
Title Radio-isotope neutron activation analysis for vanadium, manganese and tungsten in alloy steels Type A1 Journal article
Year 1987 Publication Analytica chimica acta Abbreviated Journal
Volume 196 Issue Pages 337-343
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract An instrumental neutron activation method for V, Mn and W in alloy steels with a 241 Am/Be isotopic neutron source is described. The samples were irradiated to induce the nuclear reactions 51V(n, γ) 52V, 55Mn(n, γ)56Mn, and 186W(n, γ)187W. The activities were measured with a NaI(TI) detector. Interferences on the measured photopeaks were shown to be negligible by measuring the half-lives of 62V, 56Mn and 187W.These thre elementes were determined in the range 1.512.9% in special steels; manganese in the range 0.51.6% was measured in cast irons. Calibration was done by comparison with results from wet chemistry and x-ray fluorescence spectrometry. The processing times for the vanadium, manganese and tungsten determinations were 11 min, 3 h and 26.3 h, respectively, but these were reduced greatly by intoruding a scheme wherein six samples were simultaneously irradiated and the 56Mn and 187W nuclides were measured sequentially for a series of 66 samples. The average processing time was reduced to 45 min for tungsten with a precision of 4.0% and accuracy of 3.4% and 22.8 min for manganese with a precision of 3.8% and accuracy of 3.1%.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1987K058900044 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2670; 1873-4324 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116445 Serial 8449
Permanent link to this record
 
 
Author Markowicz, A.; Van Dyck, P.; Van Grieken, R.
Title Radiometric diameter concept and exact intensities for spherical particles in x-ray fluorescence analysis Type A1 Journal article
Year 1980 Publication X-ray spectrometry Abbreviated Journal
Volume 9 Issue 2 Pages 52-56
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract In X-ray fluorescence analysis the concept of radiometric diameter, d, is often introduced in considerations of the fluorescent intensity from a particulate sample. It represents the mean geometric path of the X-rays through one particle and is usually simply taken to be equal to the volume-to-area ratio of the particle. The effective radiometric path is, however, itself dependent on geometry and absorption effects. Rigorous calculations of the fluorescent intensity from a particle in the π and π/2 geometries were carried out to evaluate the errors involved. It appears that, for π geometry, the discrepancy between these exact results and the intensity calculated via the use of d does not exceed 5.2%. For the π/2 geometry, the errors are much larger and can amount to 50% in realistic cases of X-ray fluorescence analysis. These conclusions are also applicable to monolayers. The effective radiometric diameter approaches d only when absorption effects become negligible, but is smaller in other cases.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1980JN16500003 Publication Date 2005-05-28
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0049-8246 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116482 Serial 8451
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Author Potgieter-Vermaak, S.; Maledi, N.; Wagner, N.; van Heerden, J.H.P.; Van Grieken, R.; Potgieter, J.H.
Title Raman spectroscopy for the analysis of coal : a review Type A1 Journal article
Year 2011 Publication Journal of Raman spectroscopy Abbreviated Journal
Volume 42 Issue 2 Pages 123-129
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract The advances in the characterization of amorphous carbons by Raman spectroscopy over the last four decades are of interest to many industries, especially those involving the combustion, gasification and pyrolysis of coal. Many researchers report on the Raman character of the natural organic matter in carbon-containing compounds, such as coal, and relate the Raman bands to the structural order of the amorphous carbons. The basis of most of these studies evolved around the assignment of the G (graphitic, ∼1580 cm−1) band to crystalline graphite and any other bands, called D bands, (disorder, various from 1100 to 1500 cm−1) to any type of structural disorder in the graphitic structure. Concerning coal analysis, the information gained by Raman investigations has been used to describe char evolution as a function of temperature, the presence of catalysts and different gasification conditions. In addition, researchers looked at maturation, grade, doppleritization and many more aspects of interest. One aspect that has, however, not been addressed by most of the researchers is the natural inorganic matter (NIM) in the carbon-containing compounds. Micro-Raman spectroscopy (MRS) has many advantages over other characterization tools, i.e. in situ analysis, nondestructive, no sample preparation, low detection limit, micrometer-scale characterization, versatility and sensitivity to many amorphous compounds. With the distinct advantages it has over that of other molecular characterization tools, such as powder X-ray diffraction (PXRD), Fourier-transform infrared spectrometry (FT-IR) and scanning electron microscopy with X-ray detection (SEM/EDS), it is surprising that it has not yet been fully exploited up to this point for the characterization of the NIM in coal and other amorphous carbons. This paper reviews the work published on the Raman characterization of the natural organic matter (NOM) of coals and reports on preliminary results of the NIM character of various South African coals, whereby various inorganic compounds and minerals in the coal have been characterized.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000288543000001 Publication Date 2010-03-11
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0377-0486 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:87024 Serial 8452
Permanent link to this record
 
 
Author Roekens, E.; Van Grieken, R.
Title Rates of air pollution induced surface recession and material loss for a cathedral in Belgium Type A1 Journal article
Year 1989 Publication Atmospheric environment Abbreviated Journal
Volume 23 Issue 1 Pages 271-287
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract Runoff water samples were taken at the St. Rombout's Cathedral (Mechelen, Belgium), which was constructed with sandy limestones of Balegem and Gobertingen. Gypsum appeared to be the principal deterioration compound. The mean annual surface recession from the cathedral was calculated to be around 20 μm. Yearly several tons of stone material are flushed away from the cathedral with the rain water.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos Publication Date 2003-08-06
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0004-6981 ISBN Additional Links UA library record
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116455 Serial 8454
Permanent link to this record
 
 
Author Jambers, W.; de Bock, L.; Van Grieken, R.
Title Recent advances in the analysis of individual environmental particles: a review Type A1 Journal article
Year 1995 Publication The analyst Abbreviated Journal
Volume 120 Issue Pages 681-692
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1995QP46100016 Publication Date 2004-03-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:12343 Serial 8458
Permanent link to this record
 
 
Author Bruynseels, F.; Van Grieken, R.
Title Recombination reactions and geometry effects in laser microprobe mass analysis studied with 12C/13C bilayers Type A1 Journal article
Year 1986 Publication International journal of mass spectrometry and ion processes Abbreviated Journal
Volume 74 Issue 2-3 Pages 161-177
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract Bilayers of carbon, consisting of a layer of natural carbon and a second layer highly enriched in 13C, were investigated with the LAMMA 500-® instrument. When such a bilayer is perforated by the laser beam, comparable amounts of 12C and 13C are evaporated and partly ionized so that geometry effects and recombination reactions during laser-induced ionization can straightforwardly be studied.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1986G343200003 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0168-1176; 1873-2801 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113611 Serial 8461
Permanent link to this record
 
 
Author Mihucz, V.G.; Varga, Z.; Tatár, E.; Virág, I.; Van Grieken, R.; Koleszár, Z.; Záray, G.
Title Redistribution of uranium and thorium by soil/plant interaction in a recultivated mining area Type A1 Journal article
Year 2008 Publication Microchemical journal Abbreviated Journal
Volume 90 Issue 1 Pages 44-49
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract During the recultivation of the uranium mining area of Kõvágószõlõs (Hungary), the tailings were covered with clay and loess soil layers having a thickness of 30 cm and 100 cm, respectively. In the loess covering layer, acacia (Robinia pseudoacacia), poplars (Populus × albus, Populus × canescens), oak (Quercus pubescens), silver tree (Eleagnus angustifolia) were planted between 1996 and 2004. In order to establish the extent of the uranium and thorium transport from the sludge to the leaves by uptake and translocation processes through roots with a length higher than 1.3 m results in a remarkable redistribution of these pollutants, a gray poplar tree, growing spontaneously in the last uncovered tailing, being selected as reference tree. The U and Th concentrations in the leaves of the above-mentioned trees, in the covering layers as well as in the original sludge were determined by inductively coupled plasma sector field mass spectrometry (ICP-SF-MS). Generally, the Th concentration of the soils was about 4 times higher than that of uranium, while uranium concentration was about 10130 times higher than that of thorium in the leaf samples and its concentration ranged from 28 to 1045 ng g− 1, the last value belonging to the poplar tree growing on the last uncovered tailing. In order to assume the mobility and bioavailability of uranium if the dry leaves fall down, the uranium species in the leaves of the poplar tree growing in the uncovered reservoir were determined applying ultrasound-assisted extraction with distilled water and ammonium acetate as well as high performance liquid chromatographic (HPLC)-ICP-SF-MS technique. About 20% of total uranium could be extracted in form of uranyl cations and a presumably negatively charged uranium compound. Estimations revealed that the annual increment of U in the soil surface layer due to the dead fallen leaves in case of the investigated gray poplar (Populus × canescens) is about 1.2%.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000258744000008 Publication Date 2008-03-21
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0026-265x; 0026-265x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:70717 Serial 8464
Permanent link to this record
 
 
Author Vanderborght, B.; Van Grieken, R.
Title Reduction of trace metal levels in analytical-grade activated carbon Type A1 Journal article
Year 1977 Publication Analytica chimica acta Abbreviated Journal
Volume 89 Issue 2 Pages 399-402
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1977DB52500022 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2670; 1873-4324 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116368 Serial 8466
Permanent link to this record
 
 
Author Godoi, R.H.M.; Godoi, A.F.L.; de Quadros, L.C.; Polezer, G.; Silva, T.O.B.; Yamamoto, C.I.; Van Grieken, R.; Potgieter-Vermaak, S.
Title Risk assessment and spatial chemical variability of PM collected at selected bus stations Type A1 Journal article
Year 2013 Publication Air quality, atmosphere & health Abbreviated Journal
Volume Issue Pages 1-11
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract The chemical characterization of particulate matter inside and outside of confined bus shelters has been discerned for the first time. Transit patrons are at risk due to the close vicinity of densely trafficked areas resulting in elevated pollution footprints. Incomplete combustion processes, as well as exhaust and wear and tear emissions from public and personal transportation vehicles, are key contributors to degraded urban air quality and are often implicated as causal to various diseases in humans. Urban planning, therefore, includes efficient public transport systems to mitigate the effect. The bus rapid transit system was inaugurated in Curitiba to ensure dedicated traffic lanes, major bus interchanges and semi-confined bus stops called tube stations. To assess the chemical risk that the passengers are exposed to, an investigation of the aerosol inside and outside five of these tube stations was launched. Electron probe X-ray micro-analysis and X-ray fluorescence were used to determine the elemental composition of individual and of bulk particle samples. An aethalometer quantified the black carbon. Elemental concentrations inside the shelters were in general higher than outside, especially for traffic-related elements. The lead concentration exceeded the NAAS standard at times, although the average was below the guideline. The biogenic, organic and soot clusters showed the highest abundance for the city centre sites. The overall carcinogenic risk could be classed as moderate, and the risk was significant at two sites during one of the sampling campaigns. The non-carcinogenic risk is well below the significant value.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000328332500006 Publication Date 2013-11-01
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 1873-9318 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:111086 Serial 8484
Permanent link to this record
 
 
Author Cardell, C.; Delalieux, F.; Roumpopoulos, K.; Moropoulou, A.; Auger, F.; Van Grieken, R.
Title Salt-induced decay in calcareous stone monuments and buildings in a marine environment in SW France Type A1 Journal article
Year 2003 Publication Construction and building materials Abbreviated Journal
Volume 17 Issue Pages 165-179
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000181682600003 Publication Date 2003-03-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0950-0618 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:40839 Serial 8489
Permanent link to this record
 
 
Author Van Grieken, R.; Van de Velde, R.; Robberecht, H.
Title Sample contamination from a commercial grinding unit Type A1 Journal article
Year 1980 Publication Analytica chimica acta Abbreviated Journal
Volume 118 Issue 1 Pages 137-143
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract The contamination of ground samples by a commercially available Lovibond McCrone Micronizing Mill is discussed. Tracer and weighing experiments showed that abrasion of corundum grinding elements was important, introducing 620 mg of abrasion products per minute of wet grinding. Agate grinding elements were abraded at ⩽6 mg min-1. The abrasion products and grinding elements were analyzed by x-ray fluorescence, spark-source mass spectrometry and neutron activation analysis. Contamination in trace element analysis of geological materials is likely to be negligible for agate grinding elements and, except for a few transition metals, also for corundum grinding elements. Contamination of typical biological samples is significant for a few elements even when agate elements are used, and is absolutely prohibitive for trace analysis when corundum elements are used.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1980JZ95100016 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2670; 1873-4324 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116436 Serial 8492
Permanent link to this record
 
 
Author Ravindra, K.; Bencs, L.; Wauters, E.; de Hoog, J.; Deutsch, F.; Roekens, E.; Bleux, N.; Berghmans, P.; Van Grieken, R.
Title Seasonal and site-specific variation in vapour and aerosol phase PAHs over Flanders (Belgium) and their relation with anthropogenic activities Type A1 Journal article
Year 2006 Publication Atmospheric environment : an international journal Abbreviated Journal
Volume 40 Issue 4 Pages 771-785
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000235764300016 Publication Date 2005-11-29
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 1352-2310 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:55412 Serial 8499
Permanent link to this record
 
 
Author Alejo, D.; Morales, M.C.; de la Torre, J.B.; Grau, R.; Bencs, L.; Van Grieken, R.; van Espen, P.; Sosa, D.; Nuñez, V.
Title Seasonal trends of atmospheric nitrogen dioxide and sulfur dioxide over North Santa Clara, Cuba Type A1 Journal article
Year 2013 Publication Environmental monitoring and assessment Abbreviated Journal
Volume 185 Issue 7 Pages 6023-6033
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract Atmospheric nitrogen dioxide (NO2) and sulfur dioxide (SO2) levels were monitored simultaneously by means of Radiello passive samplers at six sites of Santa Clara city, Cuba, in the cold and the warm seasons in 2010. The dissolved ionic forms of NO2 and SO2 as nitrate and sulfite plus sulfate, respectively, were determined by means of ion chromatography. Analysis of NO2 as nitrite was also performed by UVVis spectrophotometry. For NO2, significant t tests show good agreement between the results of IC and UVVis methods. The NO2 and SO2 concentrations peaked in the cold season, while their minimum levels were experienced in the warm season. The pollutant levels do not exceed the maximum allowable limit of the Cuban Standard 39:1999, i.e., 40 μg/m3 and 50 μg/m3 for NO2 and SO2, respectively. The lowest pollutant concentrations obtained in the warm season can be attributed to an increase in their removal via precipitation (scavenging) while to the decreased traffic density and industrial emission during the summer holidays (e.g., July and August).
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000319753600053 Publication Date 2012-12-03
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 1420-2026; 1573-2967 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:107293 Serial 8501
Permanent link to this record
 
 
Author Saxena, D.P.; Joos, P.; Van Grieken, R.; Subramanian, V.
Title Sedimentation rate of the floodplain sediments of the Yamuna river basin (tributary of the river Ganges, India) by using <tex>210Pb</tex> and <tex>137Cs</tex> techniques Type A1 Journal article
Year 2002 Publication Journal of radioanalytical and nuclear chemistry Abbreviated Journal
Volume 251 Issue 3 Pages 399-408
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000174851200010 Publication Date 2002-12-28
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0236-5731; 1588-2780 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:36664 Serial 8502
Permanent link to this record
 
 
Author Robberecht, H.; Van Grieken, R.
Title Selenium in environmental waters : determination, speciation and concentration levels Type A1 Journal article
Year 1982 Publication Talanta : the international journal of pure and applied analytical chemistry Abbreviated Journal
Volume 29 Issue 10 Pages 823-844
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract This article reviews the different methods used for the determination of selenium species in all types of environmental waters. Basic difficulties are discussed and the efficiency of the methods is explained in view of the sub-μg/1. concentration levels. Special attention is paid to preconcentration steps. Published data on speciation and concentration levels in various water samples are critically reviewed.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1982PK22900004 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0039-9140; 1873-3573 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113627 Serial 8509
Permanent link to this record
 
 
Author Godoi, R.H.M.; Kontozova, V.; Van Grieken, R.
Title The shielding effect of the protective glazing of historical stained glass windows from an atmospheric chemistry perspective: case study Sainte Chapelle, Paris Type A1 Journal article
Year 2006 Publication Atmospheric environment : an international journal Abbreviated Journal
Volume 40 Issue 7 Pages 1255-1265
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000236210300007 Publication Date 2005-11-29
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 1352-2310 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:55838 Serial 8518
Permanent link to this record
 
 
Author Markowicz, A.; Storms, H.; Van Grieken, R.
Title A simple absorption correction for electron probe X-ray microanalysis of bulk samples Type A1 Journal article
Year 1986 Publication X-ray spectrometry Abbreviated Journal
Volume 15 Issue 2 Pages 115-119
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract A simple procedure is proposed for the calculation of the absorption correction factor in electron-probe x-ray microanalysis. It is based on the concept of an effective depth of x-ray production, assuming a rectangular depth distribution function for x-ray generation. This effective x-ray production depth is expressed as a fraction of the x-ray excitation depth given by Whelan's expression. Adequate values for this fraction are presented. Two versions are considered. In the first the effective x-ray production is a function of both the characteristic x-ray energy and the atomic numbers of the matrix elements, whereas in the second one, which is indicated for routine use, the energy dependence is neglected. Calculations pointed to satisfactory results, even for low x-ray energies and high overvoltages.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1986C017300007 Publication Date 2005-05-28
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0049-8246 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113872 Serial 8524
Permanent link to this record
 
 
Author Vandecasteele, C.; Van Grieken, R.; Hoste, J.
Title Simultaneous determination of chromium and silicon in steel by 14-mev neutron activation analysis Type A1 Journal article
Year 1974 Publication Analytica chimica acta Abbreviated Journal
Volume 72 Issue 1 Pages 31-36
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract Chromium and silicon are determined simultaneously in steel by 14-MeV neutron activation analysis. The activities of 52V(Eγ=1.43 MeV,TView the MathML source=3.76 min) from 52Cr(n,p)52V and 28Al (Eγ=1.78 MeV; TView the MathML source=2.24 min) from 28Si(n,p)28Al are evaluated by mixed γ-ray spectrometry. The influence of manganese and phosphorus, the main interfering elements, is negligible for most stainless steels. The count rate should be limited, to avoid 52V pulse pile-up effects interfering in the 28Al energy region. Precisions in the 2-10% range are reached, depending on the concentrations, for a 10-min analysis time. Results for a series of steel samples are compared with industrial analyses.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1974U036600002 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2670; 1873-4324 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116366 Serial 8527
Permanent link to this record
 
 
Author de Bock, L.A.; Joos, P.E.; Noone, K.J.; Pockalny, R.A.; Van Grieken, R.E.
Title Single particle analysis of aerosols, observed in the marine boundary layer during the Monterey Area Ship Tracks Experiment (MAST), with respect to cloud droplet formation Type A1 Journal article
Year 2000 Publication Journal of atmospheric chemistry Abbreviated Journal
Volume 37 Issue Pages 299-329
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000089349400005 Publication Date 2002-12-22
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0167-7764 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:31674 Serial 8531
Permanent link to this record
 
 
Author Dekov, V.M.; van Put, A.; Eisma, D.; Van Grieken, R.
Title Single particle analysis of suspended matter in the Makasar Strait and Flores Sea with particular reference to tin-bearing particles Type A1 Journal article
Year 1999 Publication Journal of sea research Abbreviated Journal
Volume 41 Issue Pages 35-53
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000079367500004 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 1385-1101 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:23183 Serial 8533
Permanent link to this record
 
 
Author Jambers, W.; Dekov, V.; Van Grieken, R.
Title Single particle and inorganic characterization of rainwater collected above the North Sea Type A1 Journal article
Year 2000 Publication The science of the total environment Abbreviated Journal
Volume 256 Issue Pages 133-150
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000088065200006 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0048-9697; 1879-1026 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:31673 Serial 8535
Permanent link to this record
 
 
Author Jambers, W.; Dekov, V.; Van Grieken, R.
Title Single particle characterisation of inorganic and organic North Sea suspension Type A1 Journal article
Year 1999 Publication Marine chemistry Abbreviated Journal
Volume 67 Issue Pages 17-32
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000082709500002 Publication Date 2002-07-25
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0304-4203; 1872-7581 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:27581 Serial 8536
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Author Jambers, W.; Van Grieken, R.
Title Single particle characterisation of inorganic suspension in Lake Baikal Type A1 Journal article
Year 1997 Publication Environmental science and technology Abbreviated Journal
Volume 31 Issue Pages 1525-1533
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos Publication Date
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0013-936x; 1520-5851 ISBN Additional Links UA library record
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:18776 Serial 8538
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Author Hoornaert, S.; Godoi, R.H.M.; Van Grieken, R.
Title Single particle characterisation of the aerosol in the marine boundary layer and free troposphere over Tenerife, NE Atlantic, during ACE-2 Type A1 Journal article
Year 2003 Publication Journal of atmospheric chemistry Abbreviated Journal
Volume 46 Issue Pages 271-293
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000186253500003 Publication Date 2003-11-04
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0167-7764 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:43521 Serial 8539
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Author Ro, C.-U.; Hwang, H.; Kim, H.K.; Chun, Y.; Van Grieken, R.
Title Single-particle characterization of four “Asian Dust” samples collected in Korea, using low-Z particle electron probe X-ray microanalysis Type A1 Journal article
Year 2005 Publication Environmental science and technology Abbreviated Journal
Volume 39 Issue 6 Pages 1409-1419
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000227636300012 Publication Date 2005-03-11
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0013-936x; 1520-5851 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:51591 Serial 8540
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Author Ro, C.-U.; Kim, H.; Oh, K.-Y.; Yea, S.K.; Lee, C.B.; Jang, M.; Van Grieken, R.
Title Single-particle characterization of urban aerosol particles collected in three Korean cities using low-Z electron probe x-ray microanalysis Type A1 Journal article
Year 2002 Publication Environmental science and technology Abbreviated Journal
Volume 36 Issue 22 Pages 4770-4776
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000179348500010 Publication Date 2002-11-13
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0013-936x; 1520-5851 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:40617 Serial 8541
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Author Krata, A.; Kontozova-Deutsch, V.; Bencs, L.; Deutsch, F.; Van Grieken, R.
Title Single-run ion chromatographic separation of inorganic and low-molecular-mass organic anions under isocratic elution: application to environmental samples Type A1 Journal article
Year 2009 Publication Talanta : the international journal of pure and applied analytical chemistry Abbreviated Journal
Volume 79 Issue 1 Pages 16-21
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract For the isocratic ion chromatography (IC) separation of low-molecular-mass organic acids and inorganic anions three different anion-exchange columns were studied: IonPac AS14 (9 ìm particle size), Allsep A-2 (7 ìm particle size), and IC SI-50 4E (5 ìm particle size). A complete baseline separation for all analyzed anions (i.e., F−, acetate, formate, Cl−, NO2−, Br−, NO3−, HPO42− and SO42−) in one analytical cycle of shorter than 17 min was achieved on the IC SI-50 4E column, using an eluent mixture of 3.2 mM Na2CO3 and 1.0 mM NaHCO3 with a flow rate of 1.0 mL min−1. On the IonPac AS14 column, it was possible to separate acetate from inorganic anions in one run (i.e., less than 9 min), but not formate, under the following conditions: 3.5 mM Na2CO3 plus 1.0 mM NaHCO3 with a flow rate of 1.2 mL min−1. Therefore, it was necessary to adapt a second run with a 2.0 mM Na2B4O7 solution as an eluent under a flow rate of 0.8 mL min−1 for the separation of organic ions, which considerably enlarged the analysis time. For the Allsep A-2 column, using an eluent mixture of 1.2 mM Na2CO3 plus 1.5 mM NaHCO3 with a flow rate of 1.6 mL min−1, it was possible to separate almost all anions in one run within 25 min, except the fluoride-acetate critical pair. A Certified Multianion Standard Solution PRIMUS for IC was used for the validation of the analytical methods. The lowest RSDs (less than 1%) and the best LODs (0.02, 0.2, 0.16, 0.11, 0.06, 0.05, 0.04, 0.14 and 0.09 mg L−1 for F−, Ac−, For−, Cl−, NO2−, Br−, NO3−, HPO42− and SO42−, respectively) were achieved using the IC SI-50 4E column. This column was applied for the separation of concerned ions in environmental precipitation samples such as snow, hail and rainwater.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000266187600004 Publication Date 2009-03-06
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0039-9140; 1873-3573 ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:75475 Serial 8542
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Author Smekens, A.; Berghmans, P.; Van Grieken, R.
Title The size distribution and surface area of soot emitted by different sources Type A1 Journal article
Year 2000 Publication Journal of aerosol science Abbreviated Journal
Volume 31 Issue S1 Pages 706-707
Keywords (up) A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos Publication Date
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0021-8502; 1879-1964 ISBN Additional Links UA library record
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:31643 Serial 8545
Permanent link to this record