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Author Adams, F.C.; Van Grieken, R.E.
Title Absorption correction for X-ray-fluorescence analysis of aerosol loaded filters Type A1 Journal article
Year 1975 Publication Analytical chemistry Abbreviated Journal (up)
Volume 47 Issue 11 Pages 1767-1773
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1975AN45700013 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113639 Serial 7408
Permanent link to this record
 

 
Author Markowicz, A.A.; Storms, H.M.; Van Grieken, R.E.
Title Absorption correction in electron probe x-ray microanalysis of thin samples Type A1 Journal article
Year 1986 Publication Analytical chemistry Abbreviated Journal (up)
Volume 58 Issue 7 Pages 1282-1285
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1986C594100007 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116524 Serial 7409
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Author Van Dyck, P.M.; Van Grieken, R.E.
Title Absorption correction via scattered radiation in energy-dispersive X-ray fluorescence analysis for samples of variable composition and thickness Type A1 Journal article
Year 1980 Publication Analytical chemistry Abbreviated Journal (up)
Volume 52 Issue 12 Pages 1859-1864
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1980KJ65700021 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116516 Serial 7410
Permanent link to this record
 

 
Author Blockhuys, F.; Claes, M.; Van Grieken, R.; Geise, H.J.
Title Assessing the molecular weight of a conducting polymer by grazing emission XRF Type A1 Journal article
Year 2000 Publication Analytical chemistry Abbreviated Journal (up)
Volume 72 Issue 14 Pages 3366-3368
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000088347100054 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:27915 Serial 7497
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Author Markowicz, A.A.; Van Grieken, R.E.
Title Atomic number correction in electron probe X-ray microanalysis of curved samples and particles Type A1 Journal article
Year 1984 Publication Analytical chemistry Abbreviated Journal (up)
Volume 56 Issue 14 Pages 2798-2801
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1984TU34600040 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116519 Serial 7535
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Author Markowicz, A.A.; Storms, H.M.; Van Grieken, R.E.
Title Bremsstrahlung background in electron-probe X-ray-microanalysis of thin films Type A1 Journal article
Year 1985 Publication Analytical chemistry Abbreviated Journal (up)
Volume 57 Issue 14 Pages 2885-2889
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1985AVD0100033 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113616 Serial 7567
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Author Smits, J.A.; Van Grieken, R.E.
Title Characterization of a 2,2'-diaminodiethylamine-cellulose filter toward metal cation extraction Type A1 Journal article
Year 1980 Publication Analytical chemistry Abbreviated Journal (up)
Volume 52 Issue 9 Pages 1479-1489
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1980KB79500027 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116515 Serial 7610
Permanent link to this record
 

 
Author Van Grieken, R.E.; Bresseleers, C.M.; Vanderborght, B.M.
Title Chelex-100 ion-exchange filter membranes for preconcentration in x-ray-fluorescence analysis of water Type A1 Journal article
Year 1977 Publication Analytical chemistry Abbreviated Journal (up)
Volume 49 Issue 9 Pages 1326-1331
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1977DP25600011 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113632 Serial 7639
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Author Markowicz, A.A.; Van Grieken, R.E.
Title Composition dependence of Bremsstrahlung background in electron-probe x-ray microanalysis Type A1 Journal article
Year 1984 Publication Analytical chemistry Abbreviated Journal (up)
Volume 56 Issue 12 Pages 2049-2051
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1984TL48800021 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116518 Serial 7704
Permanent link to this record
 

 
Author Romero-Pastor, J.; Duran, A.; Rodríguez-Navarro, A.B.; Van Grieken, R.; Cardell, C.
Title Compositional and quantitative microtextural characterization of historic paintings by micro-X-ray diffraction and Raman microscopy Type A1 Journal article
Year 2011 Publication Analytical chemistry Abbreviated Journal (up)
Volume 83 Issue 22 Pages 8420-8428
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract This work shows the benefits of characterizing historic paintings via compositional and microtextural data from micro-X-ray diffraction (μ-XRD) combined with molecular information acquired with Raman microscopy (RM) along depth profiles in paint stratigraphies. The novel approach was applied to identify inorganic and organic components from paintings placed at the 14th century Islamic UniversityMadrasah Yusufiyyain Granada (Spain), the only Islamic University still standing from the time of Al-Andalus (Islamic Spain). The use of μ-XRD to obtain quantitative microtextural information of crystalline phases provided by two-dimensional diffraction patterns to recognize pigments nature and manufacture, and decay processes in complex paint cross sections, has not been reported yet. A simple Nasrid (14th century) palette made of gypsum, vermilion, and azurite mixed with glue was identified in polychromed stuccos. Here also a Christian intervention was found via the use of smalt, barite, hematite, Brunswick green and gold; oil was the binding media employed. On mural paintings and wood ceilings, more complex palettes dated to the 19th century were found, made of gypsum, anhydrite, barite, dolomite, calcite, lead white, hematite, minium, synthetic ultramarine blue, and black carbon. The identified binders were glue, egg yolk, and oil.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000296830200011 Publication Date 2011-10-10
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:92679 Serial 7715
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Author Ro, C.-U.; Osán, J.; Van Grieken, R.
Title Determination of low-Z elements in individual environmental particles using windowless EPMA Type A1 Journal article
Year 1999 Publication Analytical chemistry Abbreviated Journal (up)
Volume 71 Issue 8 Pages 1521-1528
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000079756900007 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:23185 Serial 7782
Permanent link to this record
 

 
Author van Meel, K.; Smekens, A.; Behets, M.; Kazandjian, P.; Van Grieken, R.
Title Determination of platinum, palladium, and rhodium in automotive catalysts using high-energy secondary target X-ray fluorescence spectrometry Type A1 Journal article
Year 2007 Publication Analytical chemistry Abbreviated Journal (up)
Volume 79 Issue 16 Pages 6383-6389
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000248993300042 Publication Date 2007-07-13
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:64781 Serial 7784
Permanent link to this record
 

 
Author Camerani, M.C.; Somogyi, A.; Vekemans, B.; Ansell, S.; Simionovici, A.S.; Steenari, B.-M.; Panas, I.
Title Determination of the cd-bearing phases in municipal solid waste and Biomass single fly ash particles using SR-mu XRF Spectroscopy Type A1 Journal article
Year 2007 Publication Analytical chemistry Abbreviated Journal (up)
Volume 79 Issue 17 Pages 6496-6506
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000249242900017 Publication Date 2007-08-04
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:66600 Serial 7790
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Author Schelles, W.; Van Grieken, R.
Title Direct current glow discharge mass spectrometric analysis of Macor ceramic using a secondary cathode Type A1 Journal article
Year 1996 Publication Analytical chemistry Abbreviated Journal (up)
Volume 68 Issue Pages 3570-3574
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1996VL72900008 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:14655 Serial 7808
Permanent link to this record
 

 
Author Schelles, W.; Van Grieken, R.
Title Direct current glow discharge mass spectrometry for elemental characterization of polymers Type A1 Journal article
Year 1997 Publication Analytical chemistry Abbreviated Journal (up)
Volume 69 Issue Pages 2931-2934
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1997XN42400017 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:18773 Serial 7809
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Author Wouters, L.C.; Van Grieken, R.E.; Linton, R.W.; Bauer, C.F.
Title Discrimination between coprecipitated and adsorbed lead on individual calcite particles using laser microprobe mass analysis Type A1 Journal article
Year 1988 Publication Analytical chemistry Abbreviated Journal (up)
Volume 60 Issue 20 Pages 2218-2220
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1988Q513900012 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116526 Serial 7813
Permanent link to this record
 

 
Author van Espen, P.; Van 't dack, L.; Adams, F.; Van Grieken, R.
Title Effective sample weight from scatter peaks in energy-dispersive x-ray fluorescence Type A1 Journal article
Year 1979 Publication Analytical chemistry Abbreviated Journal (up)
Volume 51 Issue 7 Pages 961-967
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1979GW66100047 Publication Date 2005-03-16
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:111404 Serial 7841
Permanent link to this record
 

 
Author Johansson, T.B.; Van Grieken, R.E.; Nelson, J.W.; Winchester, J.W.
Title Elemental trace analysis of small samples by proton-induced X-ray-emission Type A1 Journal article
Year 1975 Publication Analytical chemistry Abbreviated Journal (up)
Volume 47 Issue 6 Pages 855-860
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1975AA02900016 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:113638 Serial 7895
Permanent link to this record
 

 
Author Verbueken, A.H.; Van Grieken, R.E.; Paulus, G.J.; De Bruijn, W.C.
Title Embedded ion exchange beads as standards for laser microprobe mass analysis of biological specimens Type A1 Journal article
Year 1984 Publication Analytical chemistry Abbreviated Journal (up)
Volume 56 Issue 8 Pages 1362-1370
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1984SX51800045 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116520 Serial 7898
Permanent link to this record
 

 
Author Van Dyck, P.M.; Török, S.B.; Van Grieken, R.E.
Title Enhancement effect in X-ray fluorescence analysis of environmental samples of medium thickness Type A1 Journal article
Year 1986 Publication Analytical chemistry Abbreviated Journal (up)
Volume 58 Issue 8 Pages 1761-1766
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1986C955500040 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116522 Serial 7915
Permanent link to this record
 

 
Author Vanderborght, B.M.; Van Grieken, R.E.
Title Enrichment of trace metals in water by adsorption on activated carbon Type A1 Journal article
Year 1977 Publication Analytical chemistry Abbreviated Journal (up)
Volume 49 Issue 2 Pages 311-316
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos Publication Date
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116513 Serial 7923
Permanent link to this record
 

 
Author Ro, C.-U.; Kim, H.K.; Van Grieken, R.
Title An expert system for chemical speciation of individual particles using low-Z particle electron probe X-ray microanalysis data Type A1 Journal article
Year 2004 Publication Analytical chemistry Abbreviated Journal (up)
Volume 76 Issue Pages 1322-1327
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000189275100020 Publication Date 2004-02-27
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:43879 Serial 7949
Permanent link to this record
 

 
Author Tsuji, K.; Wagatsuma, K.; Nullens, R.; Van Grieken, R.E.
Title Grazing exit electron probe microanalysis for surface and particle analysis Type A1 Journal article
Year 1999 Publication Analytical chemistry Abbreviated Journal (up)
Volume 71 Issue 13 Pages 2497-2501
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000081265600046 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:24723 Serial 8008
Permanent link to this record
 

 
Author Tsuji, K.; Spolnik, Z.; Wagatsuma, K.; Van Grieken, R.E.; Vis, R.D.
Title Grazing-exit particle-induced X-ray emission analysis with extremely low background Type A1 Journal article
Year 1999 Publication Analytical chemistry Abbreviated Journal (up)
Volume 71 Issue 22 Pages 5033-5036
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000083647100004 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:27588 Serial 8010
Permanent link to this record
 

 
Author Ro, C.-U.; Oh, K.-Y.; Osán, J.; de Hoog, J.; Worobiec, A.; Van Grieken, R.
Title Heterogeneity assessment in individual CaCO3-CaSO4 particles using ultrathin window electron probe X-ray microanalysis Type A1 Journal article
Year 2001 Publication Analytical chemistry Abbreviated Journal (up)
Volume 73 Issue 19 Pages 4574-4583
Keywords A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000171356800012 Publication Date 2002-07-26
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:36085 Serial 8028
Permanent link to this record
 

 
Author Marguí, E.; Fontàs, C.; van Meel, K.; Van Grieken, R.; Queralt, I.; Hidalgo, M.
Title High-energy polarized-beam energy-dispersive X-ray fluorescence analysis combined with activated thin layers for cadmium determination at trace levels in complex environmental liquid samples Type A1 Journal article
Year 2008 Publication Analytical chemistry Abbreviated Journal (up)
Volume 80 Issue 7 Pages 2357-2364
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000254593500015 Publication Date 2008-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:68425 Serial 8032
Permanent link to this record
 

 
Author Bruynseels, F.J.; Van Grieken, R.E.
Title Laser microprobe mass spectrometric identification of sulfur species in single micrometer-size particles Type A1 Journal article
Year 1984 Publication Analytical chemistry Abbreviated Journal (up)
Volume 56 Issue 6 Pages 871-873
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos A1984SP09600012 Publication Date 2005-03-08
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116521 Serial 8163
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Author Denoyer, E.; Van Grieken, R.; Adams, F.; Ntausch, D.F.S.
Title Laser microprobe mass spectrometry : 1 : basic principles and performance characteristics Type A1 Journal article
Year 1982 Publication Analytical chemistry Abbreviated Journal (up)
Volume 54 Issue 1 Pages 26a-33a
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos Publication Date 2012-05-29
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:116517 Serial 8164
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Author Marguí, E.; van Meel, K.; Van Grieken, R.; Buendía, A.; Fontás, C.; Hidalgo, M.; Queralt, I.
Title Method for the determination of Pd-catalyst residues in active pharmaceutical ingredients by means of high-energy polarized-beam energy dispersive X-ray fluorescence Type A1 Journal article
Year 2009 Publication Analytical chemistry Abbreviated Journal (up)
Volume 81 Issue 4 Pages 1404-1410
Keywords A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract In medicinal chemistry, Pd is perhaps the most-widely utilized precious metal, as catalyst in reactions which represent key transformations toward the synthesis of new active pharmaceutical ingredients (APIs). The disadvantage of this metal-catalyzed chemistry is that expensive and toxic metal residues are invariably left bound to the desired product. Thus, stringent regulatory guidelines exist for the amount of residual Pd that a drug candidate is allowed to contain. In this work, a rapid and simple method for the determination of Pd in API samples by high-energy polarized-beam energy dispersive X-ray fluorescence spectrometry has been developed and validated according to the specification limits of current legislation (10 mg kg−1 Pd) and the International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use (ICH guidelines). Sample and calibration standards preparation includes a first step of homogenization and then, in a second step, the pressing of the powdered material into pellets without any chemical treatment. The use of several synthetic calibration standards made of cellulose to simulate the API matrix appears to be an effective means to obtain reliable calibration curves with a good spread of data points over the working range. With the use of the best measuring conditions, the limit of detection (0.11 mg kg−1 Pd) as well as the limit of quantitation (0.37 mg kg−1 Pd) achieved meet rigorous requirements. The repeatability of the XRF measurement appeared to be less than 2%, while the precision of the whole method was around 7%. Trueness was evaluated by analyzing spiked API samples at the level of the specification limit and calculating the recovery factor, which was better than 95%. To study the applicability of the developed methodology for the intended purpose, three batches of the studied API were analyzed for their Pd content, and the attained results were comparable to those obtained by the daily routine method (acid digestion plus atomic spectroscopy) used in most pharmaceutical laboratories.
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000263319000015 Publication Date 2009-01-22
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:74340 Serial 8220
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Author Ro, C.-U.; Osán, J.; Szalóki, I.; de Hoog, J.; Worobiec, A.; Van Grieken, R.
Title A Monte Carlo program for quantitative electron-induced x-ray analysis of individual particles Type A1 Journal article
Year 2003 Publication Analytical chemistry Abbreviated Journal (up)
Volume 75 Issue 4 Pages 851-859
Keywords A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation)
Abstract
Address
Corporate Author Thesis
Publisher Place of Publication Editor
Language Wos 000181073800021 Publication Date 2003-02-14
Series Editor Series Title Abbreviated Series Title
Series Volume Series Issue Edition
ISSN 0003-2700; 5206-882x ISBN Additional Links UA library record; WoS full record; WoS citing articles
Impact Factor Times cited Open Access
Notes Approved no
Call Number UA @ admin @ c:irua:40613 Serial 8279
Permanent link to this record