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Author Ustarroz, J.; Gupta, U.; Hubin, A.; Bals, S.; Terryn, H. pdf  doi
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  Title Electrodeposition of Ag nanoparticles onto carbon coated TEM grids : a direct approach to study early stages of nucleation Type A1 Journal article
  Year (down) 2010 Publication Electrochemistry communications Abbreviated Journal Electrochem Commun  
  Volume 12 Issue 12 Pages 1706-1709  
  Keywords A1 Journal article; Electron microscopy for materials research (EMAT)  
  Abstract An innovative experimental approach to study the electrodeposition of small nanoparticles and the early stages of electrochemical nucleation and growth is presented. Carbon coated gold TEM grids are used as substrates for the electrodeposition of silver nanoparticles so that electrochemical data, FESEM, HAADFSTEM and HRTEM data can be acquired from the same sample without the need to remove the particles from the substrate. It is shown that the real distribution of nanoparticles cannot be resolved by FESEM whereas HAADFSTEM analysis confirms that a distribution of small nanoparticles (d ≈ 12 nm) coexist with large nanoparticles corresponding to a bimodal size distribution. Besides, particles grown under the same conditions have been found to present different structures such as monocrystals, polycrystals or aggregates of smaller particles.  
  Address  
  Corporate Author Thesis  
  Publisher Place of Publication Amsterdam Editor  
  Language Wos 000285904700010 Publication Date 2010-10-09  
  Series Editor Series Title Abbreviated Series Title  
  Series Volume Series Issue Edition  
  ISSN 1388-2481; ISBN Additional Links UA library record; WoS full record; WoS citing articles  
  Impact Factor 4.396 Times cited 52 Open Access  
  Notes Fwo Approved Most recent IF: 4.396; 2010 IF: 4.287  
  Call Number UA @ lucian @ c:irua:87612 Serial 900  
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