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Author |
Smekens, A.; Knupfer, M.; Berghmans, P.; Van Grieken, R. |
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Title |
The elemental composition and microstructure of soot emitted by different sources |
Type |
A1 Journal article |
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Year |
2000 |
Publication |
Journal of aerosol science |
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Volume |
31 |
Issue |
S1 |
Pages |
917-918 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISSN |
0021-8502; 1879-1964 |
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Call Number |
UA @ admin @ c:irua:31647 |
Serial |
7887 |
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Author |
Silva, F.S.; Godoi, R.H.M.; Tauler, R.; de André, P.A.; Saldiva, P.H.N.; Van Grieken, R.; de Marchi, M.R.R. |
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Title |
Elemental composition of PM2.5 in Araraquara City (Southeast Brazil) during seasons with and without sugar cane burning |
Type |
A2 Journal article |
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Year |
2015 |
Publication |
Journal of environmental protection |
Abbreviated Journal |
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Volume |
6 |
Issue |
5 |
Pages |
426-434 |
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Keywords |
A2 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Particulate matter with an aerodynamic diameter below 2.5 μm (PM2.5), present in polluted air, has been associated with a large spectrum of health impairments, mainly because of its deep deposition into the lungs. Araraquara City (Southeast Brazil) is surrounded by sugar-cane plantations, which are burned to facilitate the harvesting; this process causes environmental pollution due to the large amounts of soot that are released into the atmosphere. In this work, the elemental composition of PM2.5 was studied in two scenarios, namely in sugar-cane harvesting (HV) and in non-harvesting (NHV) seasons. The sampling strategy included one campaign in each season. PM2.5 was collected using a dichotomous sampler (10 L·min-1, 24 h) with PTFE filters. Information concerning the bulk elemental concentration was provided by energy-dispersive X-ray fluorescence. Enrichment factor analysis indicated that S, Cl, K, Cr, Ni, Cu, Zn, As, Cd and Pb were highly enriched relative to their crustal ratios (to Al). Principal component analysis was used to get some insight about the sources of the elements. Principal component 1 (PC1) explained 30.5% of data variance. The elements that had high loading (>0.7) were: S, Cr, As, and Pb; these are associated with combustion of fossil fuels. In principal component 2 (PC2), Cl, Cu, Zn, and Cd showed high loadings; these elements are associated with biomass burning. The Ni concentration found is three times larger than the threshold of risk for lung cancer, as recommended by the World Health Organization. |
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2015-05-04 |
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ISSN |
2152-2197 |
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Call Number |
UA @ admin @ c:irua:125885 |
Serial |
7891 |
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Author |
Van Grieken, R.; Van 't dack, L.; Costa Dantas, C.; Moura de Amorim, W.; Maenhaut, W. |
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Title |
Elemental constituents of atmospheric aerosols in Recife, North-East Brazil |
Type |
A3 Journal article |
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Year |
1982 |
Publication |
Environmental pollution: series B : chemical and physical |
Abbreviated Journal |
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Volume |
4 |
Issue |
2 |
Pages |
143-163 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Few data are available on the inorganic atmospheric pollution in the rapidly expanding cities of South America, like Recife, on the Atlantic Coast of North-east Brazil. Therefore, the elemental composition of atmospheric aerosols was investigated for nine sites in the Recife conurbation and a fairly remote site in the area. Total aerosol samples were collected on cellulose filters for analysis by energy dispersive X-ray fluorescence and cascade impactors were used to collect the aerosols as a function of particle size for subsequent analysis by proton-induced X-ray emission. Local soil aliquots were also analysed. About eighteen elements were quantified in all cases. The average total atmospheric concentrations appeared to be well above natural levels but usually lower than, or comparable with, those of North American and European cities. Dispersal of sea spray and of local soil (often contaminated with, for example, Cu, Zn and Pb from industrial sources) contributes predominantly to the total atmospheric load in Recife. However, the particle size fraction results also indicated strong excesses in the small particle mode for S, K, V, Mn, Ni, Cu, Zn, Br and Pb, mainly in the downtown area. Again, the corresponding enrichment factors were only moderate in comparison with other published urban data. |
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Publication Date |
2003-09-11 |
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ISSN |
0143-148x; 1878-0695 |
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Call Number |
UA @ admin @ c:irua:111437 |
Serial |
7894 |
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Author |
Muia, L.M.; Van Grieken, R. |
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Title |
Energy-dispersive X-ray fluorescence analysis of geological materials in borax beads using Tertian's binary coefficient approach combined with internal standard addition |
Type |
A1 Journal article |
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Year |
1991 |
Publication |
X-ray spectrometry |
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Volume |
20 |
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179-183 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISSN |
0049-8246 |
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Call Number |
UA @ admin @ c:irua:662 |
Serial |
7903 |
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Author |
Van Grieken, R.; Robberecht, H.; Shani, J.; Van Dyck, P.; Vos, L. |
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Title |
Energy-dispersive X-ray fluorescence for direct trace analysis of biomedical and environmental samples |
Type |
H3 Book chapter |
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Year |
1982 |
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Abbreviated Journal |
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Pages |
159-178
T2 - X-ray fluorescence (XRF and PIXE) in |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117485 |
Serial |
7904 |
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Author |
Vanderborght, B.; Van Grieken, R. |
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Title |
Energy-dispersive X-ray fluorescence for trace metals analysis of water |
Type |
H3 Book chapter |
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Year |
1975 |
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Pages |
1-9
T2 - Nuclear techniques in environmental resea |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117461 |
Serial |
7905 |
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Author |
Van Grieken, R.; Markowicz, A.; Török, S. |
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Title |
Energy-dispersive X-ray spectrometry : present state and trends |
Type |
A3 Journal article |
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Year |
1986 |
Publication |
Fresenius' Zeitschrift für analytische Chemie |
Abbreviated Journal |
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Volume |
324 |
Issue |
8 |
Pages |
825-831 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Recent development, present state and expected future developments in energy-dispersive X-ray spectrometry are discussed. Attention is paid to the improvements in analytical selectivity, sensitivity, detection limit, quantitative character and applicability range, which are the result of new or better excitation sources, detectors, instrument design, automation, computer software and theoretical developments. |
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2004-11-15 |
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0016-1152 |
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Call Number |
UA @ admin @ c:irua:116642 |
Serial |
7907 |
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Author |
Vanderborght, B.M.; Van Grieken, R.E. |
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Title |
Enrichment of trace metals in water by adsorption on activated carbon |
Type |
A1 Journal article |
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Year |
1977 |
Publication |
Analytical chemistry |
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Volume |
49 |
Issue |
2 |
Pages |
311-316 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISSN |
0003-2700; 5206-882x |
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Call Number |
UA @ admin @ c:irua:116513 |
Serial |
7923 |
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Author |
Van Grieken, R.; Bresseleers, K.; Smits, J.; Vanderborght, B.; Vanderstappen, M. |
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Title |
Enrichment procedures for water analysis by X-ray energy spectrometry |
Type |
P3 Proceeding |
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Year |
1976 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:113634 |
Serial |
7924 |
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Author |
Xhoffer, C.; Van Grieken, R. |
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Title |
Environmental aerosol characterization by single particle analysis techniques |
Type |
H3 Book chapter |
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Year |
1993 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
207-245
T2 - Environmental particles; 2 / Buffle, |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:6267 |
Serial |
7926 |
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Author |
Delalieux, F.; Cardell, C.; Todorov, V.; Dekov, V.; Van Grieken, R. |
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Title |
Environmental conditions controlling the chemical weathering of the Madara Horseman monument, NE Bulgaria |
Type |
A1 Journal article |
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Year |
2001 |
Publication |
Journal of cultural heritage |
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Volume |
2 |
Issue |
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Pages |
43-54 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Edition |
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ISSN |
1296-2074 |
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Call Number |
UA @ admin @ c:irua:32822 |
Serial |
7927 |
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Author |
Jambers, W.; Van Grieken, R.E. |
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Title |
Environmental problems |
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H3 Book chapter |
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Year |
1997 |
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Abbreviated Journal |
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Pages |
803-819
T2 - Handbook of microscopy: applications |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:18789 |
Serial |
7929 |
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Author |
Vazquez, C.; Boeykens, S.; Palacios, O.; Caracciolo, N.; Kontozova-Deutsch, V.; Krupińska, B.; Van Grieken, R. |
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Title |
Estudio de la contaminacion del aire urbano en cuatro museos de Argentina |
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H3 Book chapter |
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Year |
2013 |
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Abbreviated Journal |
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Pages |
271-282
T2 - Patrimonio cultural : la gestion, el |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-987-1323-31-9 |
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Call Number |
UA @ admin @ c:irua:110908 |
Serial |
7936 |
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Author |
Visser, W.J.; Van de Vyver, F.L.; Verbueken, A.H.; d'Haese, P.; Bekaert, A.B.; Van Grieken, R.E.; Duursma, S.A.; de Broe, M.E. |
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Title |
Evaluation of different techniques used to determine aluminium in patients with chronic renal failure |
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P3 Proceeding |
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1985 |
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P3 Proceeding; Pathophysiology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:117496 |
Serial |
7938 |
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Author |
Janssens, K.; Alfeld, M.; Van der Snickt, G.; De Nolf, W.; Vanmeert, F.; Monico, L.; Legrand, S.; Dik, J.; Cotte, M.; Falkenberg, G.; van der Loeff, L.; Leeuwestein, M.; Hendriks, E. |
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Title |
Examination of Vincent van Gogh's paintings and pigments by means of state-of-the-art analytical methods |
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H2 Book chapter |
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2014 |
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Abbreviated Journal |
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373-403
T2 - Science and art : the painted surface |
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Keywords |
H2 Book chapter; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Recent studies in which X-ray beams of macroscopic to (sub) microscopic dimensions were used for non-destructive analysis and characterization of pigments, paint micro samples and/or entire paintings by Vincent van Gogh are concisely reviewed. The overview presented encompasses the use of laboratory and synchrotron radiation-based instrumentation and deals with the use of several variants of X-ray fluorescence (XRF) as a method of elemental analysis and imaging as well as with the combined use of X-ray diffraction (XRD) and X-ray absorption spectroscopy (XAS). Microscopic and macroscopic XRF are variants of the method that are well suited to visualize the elemental distribution of key elements, mostly metals, present in paint multi layers, either on the length scale from 1–100 μm inside micro samples taken from paintings or on the 1–100 cm length scale when the (subsurface) distribution of specific pigments in entire paintings is concerned. In the context of the characterization of van Gogh's pigments subject to natural degradation, the use of methods limited to elemental analysis or imaging usually is not sufficient to elucidate the chemical transformations that have taken place. However, at synchrotron facilities, combinations of μ-XRF with related methods such as μ-XAS and μ-XRD have proven themselves to be very suitable for such studies. Their use is often combined with microscopic Fourier transform infra-red (μ-FTIR) spectroscopy since this method delivers complementary information at more or less the same length scale as the X-ray microprobe techniques. Also in the context of macroscopic imaging of works of art, the complementary use of X-ray based and infra-red based imaging appears very promising; some recent developments are discussed. |
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2020-02-24 |
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978-1-84973-818-7 |
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UA @ admin @ c:irua:190782 |
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7943 |
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Author |
Santer, R.; Schadkowski, C.; Blanchet, A.; Saison, J.-Y.; Poinsot, C.; Ramon, D.; Roekens, E.; Verlinden, L.; Van Grieken, R.; Stranger, M.; Mees, J. |
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Title |
Expositions des populations vivant au cœur de l'Euro-région auz polluants atmosphériques: le cas des poussières fines = Blootstelling van de bevolkingsgroepen wonend in het hart van de Euregio aan polluerende atmosferische deeltjes: het geval van de fijne stofdeeltjes |
Type |
Minutes and reports |
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2005 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:56167 |
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7952 |
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Author |
Struyf, H.; van Roy, W.; Van Vaeck, L.; Van Grieken, R.; Caravatti, P. |
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Title |
The feasibility of Fourier transform laser microprobe mass spectrometry for applications of local and surface analysis |
Type |
P3 Proceeding |
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1994 |
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Proceedings of the European FTMS Workshop |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:9520 |
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7961 |
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Author |
Van Grieken, R.; Stranger, M. |
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Title |
Fijn stof en pollutiegassen in de binnenlucht |
Type |
A2 Journal article |
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Year |
2006 |
Publication |
ARGUS milieumagazine |
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Volume |
4 |
Issue |
2 |
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18 |
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A2 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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1379-4957 |
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no |
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UA @ admin @ c:irua:58863 |
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7967 |
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Author |
Van Grieken, R.; Adams, F. |
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Title |
Filter absorption correction for X-ray fluorescence analysis of aerosol loaded filters |
Type |
P3 Proceeding |
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Year |
1976 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:113635 |
Serial |
7968 |
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Author |
Van Grieken, R.; Injuk, J.; Otten, P.; Rojas, C.; van Malderen, H.; Laane, R. |
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Title |
Fluxes and sources of heavy metal inputs into the Southern Bight of the North Sea |
Type |
H3 Book chapter |
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Year |
1992 |
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Pages |
184-193
T2 - Industrial air pollution: assessment |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:2859 |
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7975 |
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Author |
Van Grieken, R.; Eyckmans, K. |
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Title |
Geen vuiltje aan de Noordzeelucht: aërosolen kennen geen grenzen |
Type |
P3 Proceeding |
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2001 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:36094 |
Serial |
7990 |
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Author |
Van Grieken, R.; Speecke, A.; Hoste, J. |
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Title |
Geometry errors in 14 MeV neutron activation analysis |
Type |
A3 Journal article |
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Year |
1973 |
Publication |
Journal of radioanalytical chemistry |
Abbreviated Journal |
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Volume |
13 |
Issue |
1 |
Pages |
225-233 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The effects of inaccurate sample sizes and sample positioning on 14 MeV neutron activation analysis results are estimated for 30, 20 and 10 mm diameter targets. It appears that axial positioning is the most critical parameter and that using a larger tritium target will yield an overall improvement of the reproducibility. |
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2006-10-11 |
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ISSN |
0134-0719; 2064-2857 |
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no |
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Call Number |
UA @ admin @ c:irua:116453 |
Serial |
7999 |
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Author |
Mabesoone, J.M.; Duarte, P.J.; Van Grieken, R.; Delgao, A.; Freire, E.M.P. |
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Title |
Geoquimica dos microclasticos da Bacio do Parnaiba |
Type |
H3 Book chapter |
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1985 |
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Pages |
30-31
T2 - Fanerozoico Nordestino : serie D |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:117502 |
Serial |
8001 |
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Author |
Roekens, E.; Van Grieken, R. |
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Title |
Gevolgen van luchtverontreiniging op historische gebouwen |
Type |
A2 Journal article |
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1987 |
Publication |
Ons erfdeel |
Abbreviated Journal |
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30 |
Issue |
2 |
Pages |
361-366 |
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A2 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0030-2651 |
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no |
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Call Number |
UA @ admin @ c:irua:116776 |
Serial |
8003 |
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Author |
Van Schandevijl, R.; Van Grieken, R.; Hoste, J. |
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Title |
The half-life of 28Al |
Type |
A3 Journal article |
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Year |
1971 |
Publication |
Journal of radioanalytical chemistry |
Abbreviated Journal |
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9 |
Issue |
1 |
Pages |
55-60 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The half-life of28Al was redetermined on aluminium samples of different origin. Three different counting techniques were applied. The availability of highly purified samples (up to 99.9999%), the use of very fast electronic counting equipment and a complete automatisation allowed a good precision to be obtained in the final result of 2.2405 min. |
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2006-10-11 |
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0134-0719; 2064-2857 |
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no |
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Call Number |
UA @ admin @ c:irua:116451 |
Serial |
8016 |
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Author |
Van Grieken, R.E.; Markowicz, A.A. |
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Title |
Handbook of X-ray spectrometry |
Type |
ME2 Book as editor or co-editor |
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Year |
2002 |
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Pages |
1016 p. |
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ME2 Book as editor or co-editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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2 ed. |
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0-8247-0600-5 |
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Call Number |
UA @ admin @ c:irua:36390 |
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8017 |
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Author |
Ravindra, K.; Mittal, A.K.; Van Grieken, R. |
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Title |
Health risk assessment of urban suspended particulate matter with special reference to polycyclic aromatic hydrocarbons: a review |
Type |
A3 Journal article |
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2001 |
Publication |
Reviews on environmnetal health |
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16 |
Issue |
3 |
Pages |
169-189 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:36128 |
Serial |
8019 |
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Author |
Ramesh, R.; Subramanian, V.; Van Grieken, R. |
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Title |
Heavy metal distribution in sediments of Krishna River basin, India |
Type |
A1 Journal article |
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Year |
1990 |
Publication |
Environmental geology and water sciences |
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Volume |
15 |
Issue |
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Pages |
207-216 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Edition |
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ISSN |
0177-5146 |
ISBN |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:116933 |
Serial |
8022 |
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Author |
Biksham, G.; Subramanian, V.; Ramanathan, A.; Van Grieken, R. |
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Title |
Heavy metal distribution in the Godavari river basin |
Type |
A1 Journal article |
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Year |
1991 |
Publication |
Environmental geology and water sciences |
Abbreviated Journal |
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Volume |
17 |
Issue |
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Pages |
117-126 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0177-5146 |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:55571 |
Serial |
8023 |
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Author |
Vanmeert, F. |
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Title |
Highly specific X-ray powder diffraction imaging at the macroscopic and microscopic scale |
Type |
Doctoral thesis |
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Year |
2019 |
Publication |
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Abbreviated Journal |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
At or below the surface of painted works of art, valuable information is present that provides insights into an object’s past, such as the artist’s technique and the creative process that was followed or its conservation history, but also on its current state of preservation. Typically, a (very) limited set of small paint samples is taken which provide direct access to the individual paint layers. The chemical build-up of these layers can then be investigated in great detail using various microscopic analytical methods. However, in recent years a new trend towards both elemental and chemical imaging techniques has been set which are capable of visualizing the (often) heterogeneous composition of painted objects on a macroscopic scale. In this dissertation, various forms of specificity attainable with X‑ray powder diffraction (XRPD) imaging are explored: at the chemical, material and spatial level. This high specificity is illustrated throughout several applications stemming from the field of cultural heritage, both at the macroscopic (MA) and microscopic (µ) scale. As a first step, XRPD imaging was transformed to a transportable instrument that can be employed for the in situ investigation of artworks, e.g., inside museums and conservation workshops. With this unique instrument large‑scale maps (cm2 – dm2) reflecting the distribution of crystalline phases on/below the surface of flat painted artefacts can be visualized in a noninvasive manner. In this way compound-specific information was attained which can be related to original pigments or materials that have been added in a later stage and even degradation/secondary products that have formed spontaneously inside the paint layers. Additionally, with MA‑XRPD imaging it was possible to link quantitative information of pigment compositions and preferred orientation effects to the 2D compound‑specific distribution images, allowing for a further distinction between very similar artists’ materials. Furthermore, promising results for the limited depth-selectivity of this technique, obtained by exploiting the small shift in the position of the diffraction signals originating from the layered sequence of the pigments, are shown. Finally, a minute paint sample from Wheat stack under a cloudy sky by Van Gogh was investigated at a synchrotron radiation facility with tomographic µ‑XRPD imaging at the microscopic scale. The high chemical and spatial specificity of this imaging method was exploited to further elucidate the degradation pathway of the red lead pigment. |
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UA library record |
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UA @ admin @ c:irua:159805 |
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8043 |
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