Records |
Author |
Santer, R.; Schadkowski, C.; Blanchet, A.; Saison, J.-Y.; Poinsot, C.; Ramon, D.; Roekens, E.; Verlinden, L.; Van Grieken, R.; Stranger, M.; Mees, J. |
Title |
Expositions des populations vivant au cœur de l'Euro-région auz polluants atmosphériques: le cas des poussières fines = Blootstelling van de bevolkingsgroepen wonend in het hart van de Euregio aan polluerende atmosferische deeltjes: het geval van de fijne stofdeeltjes |
Type |
Minutes and reports |
Year |
2005 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:56167 |
Serial |
7952 |
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Author |
Struyf, H.; van Roy, W.; Van Vaeck, L.; Van Grieken, R.; Caravatti, P. |
Title |
The feasibility of Fourier transform laser microprobe mass spectrometry for applications of local and surface analysis |
Type |
P3 Proceeding |
Year |
1994 |
Publication |
Proceedings of the European FTMS Workshop |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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UA @ admin @ c:irua:9520 |
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7961 |
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Author |
Van Grieken, R.; Adams, F. |
Title |
Filter absorption correction for X-ray fluorescence analysis of aerosol loaded filters |
Type |
P3 Proceeding |
Year |
1976 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:113635 |
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7968 |
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Author |
Van Grieken, R.; Injuk, J.; Otten, P.; Rojas, C.; van Malderen, H.; Laane, R. |
Title |
Fluxes and sources of heavy metal inputs into the Southern Bight of the North Sea |
Type |
H3 Book chapter |
Year |
1992 |
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Pages |
184-193
T2 - Industrial air pollution: assessment |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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UA @ admin @ c:irua:2859 |
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7975 |
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Author |
Van Grieken, R.; Eyckmans, K. |
Title |
Geen vuiltje aan de Noordzeelucht: aërosolen kennen geen grenzen |
Type |
P3 Proceeding |
Year |
2001 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:36094 |
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7990 |
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Author |
Mabesoone, J.M.; Duarte, P.J.; Van Grieken, R.; Delgao, A.; Freire, E.M.P. |
Title |
Geoquimica dos microclasticos da Bacio do Parnaiba |
Type |
H3 Book chapter |
Year |
1985 |
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Pages |
30-31
T2 - Fanerozoico Nordestino : serie D |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117502 |
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8001 |
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Author |
Van Grieken, R.E.; Markowicz, A.A. |
Title |
Handbook of X-ray spectrometry |
Type |
ME2 Book as editor or co-editor |
Year |
2002 |
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Pages |
1016 p. |
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ME2 Book as editor or co-editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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2 ed. |
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0-8247-0600-5 |
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no |
Call Number |
UA @ admin @ c:irua:36390 |
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8017 |
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Author |
Vanmeert, F. |
Title |
Highly specific X-ray powder diffraction imaging at the macroscopic and microscopic scale |
Type |
Doctoral thesis |
Year |
2019 |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
At or below the surface of painted works of art, valuable information is present that provides insights into an object’s past, such as the artist’s technique and the creative process that was followed or its conservation history, but also on its current state of preservation. Typically, a (very) limited set of small paint samples is taken which provide direct access to the individual paint layers. The chemical build-up of these layers can then be investigated in great detail using various microscopic analytical methods. However, in recent years a new trend towards both elemental and chemical imaging techniques has been set which are capable of visualizing the (often) heterogeneous composition of painted objects on a macroscopic scale. In this dissertation, various forms of specificity attainable with X‑ray powder diffraction (XRPD) imaging are explored: at the chemical, material and spatial level. This high specificity is illustrated throughout several applications stemming from the field of cultural heritage, both at the macroscopic (MA) and microscopic (µ) scale. As a first step, XRPD imaging was transformed to a transportable instrument that can be employed for the in situ investigation of artworks, e.g., inside museums and conservation workshops. With this unique instrument large‑scale maps (cm2 – dm2) reflecting the distribution of crystalline phases on/below the surface of flat painted artefacts can be visualized in a noninvasive manner. In this way compound-specific information was attained which can be related to original pigments or materials that have been added in a later stage and even degradation/secondary products that have formed spontaneously inside the paint layers. Additionally, with MA‑XRPD imaging it was possible to link quantitative information of pigment compositions and preferred orientation effects to the 2D compound‑specific distribution images, allowing for a further distinction between very similar artists’ materials. Furthermore, promising results for the limited depth-selectivity of this technique, obtained by exploiting the small shift in the position of the diffraction signals originating from the layered sequence of the pigments, are shown. Finally, a minute paint sample from Wheat stack under a cloudy sky by Van Gogh was investigated at a synchrotron radiation facility with tomographic µ‑XRPD imaging at the microscopic scale. The high chemical and spatial specificity of this imaging method was exploited to further elucidate the degradation pathway of the red lead pigment. |
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no |
Call Number |
UA @ admin @ c:irua:159805 |
Serial |
8043 |
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Author |
Abreu Alfonso, Y. |
Title |
Hyperfine parameters and radiation damage in semiconductors and superconducting materials |
Type |
Doctoral thesis |
Year |
2014 |
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Issue |
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Pages |
126 p. |
Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:116686 |
Serial |
8047 |
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Author |
Bondarenko, I.; Treiger, B.; Van Grieken, R.; van Espen, P. |
Title |
IDAS: a new Windows based software for multivariate analysis of atmospheric aerosol composition data bases |
Type |
H3 Book chapter |
Year |
1995 |
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Pages |
308-315
T2 - Space and time in environmental infor |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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no |
Call Number |
UA @ admin @ c:irua:12357 |
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8049 |
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Author |
Salvadó, N.; Butí, S.; Pradell, T.; Beltran, V.; Cinque, G.; Juanhuix, J. |
Title |
Identification and distribution of metal soaps and oxalates in oil and tempera paint layers in fifteenth-century altarpieces using synchrotron radiation Techniques |
Type |
H1 Book chapter |
Year |
2019 |
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Pages |
195-210
T2 - Metal soaps in art : conservation and |
Keywords |
H1 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The formation and distribution of metal soaps produced as a result of the reactivity and aging of the materials in a fifteenth-century egg tempera and oil paintings on wood are presented. The painting technique involves the application of several paint layers over a ground using, sometimes in the same paint layer sequence, drying oil and egg yolk binders. We show, with a selection of examples, how the use of thin sections and a combination of various micro-sensitive analytical techniques is adequate to obtain the high-quality data necessary for the unambiguous identification of metal soaps and metal oxalates as well as their distribution in the paint layers. The techniques include micro infrared spectroscopy (μSR-FTIR) and micro X-ray diffraction (μSR-XRD) with synchrotron radiation, optical microscopy (OM), and scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDS). The data obtained sheds light about the underlying reaction and aging mechanisms happening in each paint layer and among them. This helps to define the state of conservation of the artworks. |
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2019-03-23 |
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ISBN |
978-3-319-90616-4; 2366-6226; 978-3-319-90617-1 |
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no |
Call Number |
UA @ admin @ c:irua:172891 |
Serial |
8051 |
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Author |
Verbueken, A.; Verpooten, G.; Nouwen, E.; de Broe, M.; Van Grieken, R. |
Title |
Identification of inorganic and organic microliths in kidney sections by laser microprobe mass analysis (LAMMA) |
Type |
P3 Proceeding |
Year |
1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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no |
Call Number |
UA @ admin @ c:irua:117510 |
Serial |
8054 |
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Author |
de Nolf, W. |
Title |
Imaging of crystalline phase distributions by means of scanning and tomographic X-ray powder diffraction |
Type |
Doctoral thesis |
Year |
2013 |
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Pages |
407 p. |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:110910 |
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8057 |
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Author |
Storms, H.; Artaxo, P.; Bruynseels, F.; Van Grieken, R. |
Title |
Individual particle analysis by automated EPMA for the improvement of source apportionment for remote aerosols |
Type |
H3 Book chapter |
Year |
1987 |
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343-345
T2 - Microbeam analysis 1987 / Geiss, R.H. |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117525 |
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8077 |
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Author |
Wegrzynek, D.; Eisma, D.; Van Grieken, R. |
Title |
Individual particle analysis of sediments from the Gulf of Lions, suspensions from the Rhône river and dust of Saharan origin: preliminary results |
Type |
P3 Proceeding |
Year |
1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:2861 |
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8078 |
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Author |
Kontozova, V.; Godoi, R.H.M.; Spolnik, Z.; Worobiec, A.; Deutsch, F.; Van Grieken, R. |
Title |
Influence of gaseous and particulate air pollutants on stained glass windows: case study in the Basilica Saint Urbain in Troyes, France |
Type |
P3 Proceeding |
Year |
2005 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:52359 |
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8092 |
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Author |
Anaf, W. |
Title |
The influence of particulate matter on cultural heritage : chemical characterisation of the interaction between the atmospheric environment and pigments |
Type |
Doctoral thesis |
Year |
2014 |
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Pages |
319 p. |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:119329 |
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8095 |
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Author |
Claes, M.; Gysels, K.; Van Grieken, R.; Harrison, R.M. |
Title |
Inorganic compounds of atmospheric aerosols |
Type |
H3 Book chapter |
Year |
1998 |
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Pages |
95-145
T2 - Atmospheric particles / Harrison, R.M. |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:20968 |
Serial |
8104 |
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Author |
Potgieter-Vermaak, S.; Van Grieken, R.; Potgieter, J.H. |
Title |
Integrated analytical techniques for analysing individual environmental particles |
Type |
H2 Book chapter |
Year |
2012 |
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Pages |
123-141
T2 - Spectroscopic properties of inorganic |
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H2 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-1-84973-395-3 |
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UA @ admin @ c:irua:109314 |
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8108 |
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Author |
Van Grieken, R.; Darchuk, L.; Kontozova, V.; Potgieter-Vermaak, S.; van Meel, K.; Stefaniak, E.; Worobiec, A. |
Title |
Integration of analysis techniques of different scales using X ray induced and electron induced X ray spectrometry for applications in preventive conservation and environmental monitoring |
Type |
H2 Book chapter |
Year |
2011 |
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Pages |
53-56
T2 - Integration of nuclear spectrometry met |
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H2 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
In the past years, and also within the framework of this CRP, we have used a combination of several nuclear and non-nuclear techniques in fundamental research and especially in various applications. Most work has been done with energy-dispersive X ray fluorescence in combination with electron probe X ray microanalysis, but several other more common analysis techniques have been used as well. The applications have included mostly preventive conservation (e.g. characterisation of damaging atmospheric particles in many museums) and environmental monitoring (e.g. for atmospheric particles in relation to their health effects in outdoor and especially indoor environments). Fundamental aspects have been in the optimising of interfaced electron microprobe and Raman microprobe analysis and the evaluation of the potential of such an instrument for atmospheric aerosols; quite a few unexpected and unpredicted problems have appeared in the latter study. |
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978-92-0-121310-5 |
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Call Number |
UA @ admin @ c:irua:97169 |
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8110 |
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Author |
Johansson, T.B.; Van Grieken, R.E.; Winchester, J.W. |
Title |
Interpretation of aerosol trace metal particle size distributions |
Type |
H3 Book chapter |
Year |
1975 |
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356-365
T2 - Nuclear techniques in environmental r |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117460 |
Serial |
8117 |
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Author |
Van Grieken, R. |
Title |
Introduction: considering the role of X-ray spectrometry in chemical analysis and outlining the volume |
Type |
H3 Book chapter |
Year |
2004 |
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1-11
T2 - X-ray spectrometry: recent technological |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:43877 |
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8121 |
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Author |
Godoi, R.H.M.; Kontozova, V.; Godoi, A.F.L.; Van Grieken, R. |
Title |
Investigation of individual particles and gaseous air pollutants in showcases |
Type |
H3 Book chapter |
Year |
2004 |
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147-150
T2 - Air pollution and cultural heritage / |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:48941 |
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8126 |
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Author |
van der Snickt, G. |
Title |
James Ensor's pigments studied by means of portable and synchrotron radiation-based X-ray techniques : evolution, context and degradation |
Type |
Doctoral thesis |
Year |
2012 |
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Pages |
501 p. |
Keywords |
Doctoral thesis; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:100628 |
Serial |
8135 |
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Author |
Van Grieken, R.; Fobe, B. |
Title |
Kultuurpatrimonium, zure regen en energie |
Type |
A3 Journal article |
Year |
1990 |
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Energie en milieu: tijdschrift over energie en leefmilieu |
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1 |
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10-11 |
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A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0777-4850 |
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no |
Call Number |
UA @ admin @ c:irua:116827 |
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8143 |
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Author |
Otten, P.; Bruynseels; Van Grieken, R. |
Title |
LAMMA analysis of inorganic ammonium compounds in individual marine aerosol particles |
Type |
P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117509 |
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8147 |
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Author |
Verbueken, A.; Paulus, G.; Van de Vyver, F.; Verpooten, G.; de Broe, M.; Van Grieken, R. |
Title |
LAMMA : calibration and application to nephrotoxicology studies |
Type |
P3 Proceeding |
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1983 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:117491 |
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8149 |
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Author |
Verbueken, A.H.; Paulus, G.J.; Van de Vyver, F.L.; Verpooten, G.A.; Visser, W.J.; de Broe, M.E.; Van Grieken, R.E. |
Title |
LAMMA in nephrotoxicity studies |
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P3 Proceeding |
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1984 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:117492 |
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8150 |
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Author |
Bruynseels, F.; Artaxo, P.; Storms, H.; Van Grieken, R. |
Title |
LAMMA-study of aerosol samples collected in the Amazon basin |
Type |
H3 Book chapter |
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1987 |
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355-358
T2 - Microbeam analysis 1987 / Geiss, R.H. |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117527 |
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8151 |
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Author |
Hellemans, K. |
Title |
Laser ablation ICP-MS as a tool for surface analysis in comparison to other elemental analysis methods |
Type |
Doctoral thesis |
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2019 |
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229 p. |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Dit onderzoek presenteert een overzicht van de mogelijkheden van LA-ICP-MS als een techniek voor kwantitatieve analyse, bepalen van isotoopverhoudingen en elementaire beeldvorming. Hiervoor wordt de techniek zelf voorgesteld en worden de belangrijkste parameters die een invloed hebben op de kwaliteit van een LA-ICP-MS meting beschreven. Voor kwantitieve analyse worden de huidige calibratiestrategieën voor LA-ICP-MS toegelicht, zowel op het vlak van selectie en bereiding van standaarden als op het vlak van dataverwerking. Daarnaast werd een nieuwe calibratiestrategie voorgesteld, gebaseerd op een lineaire combinatie van standaarden. Een case study met de traditionele calibratiestrategie uit de literatuur werd uitgevoerd en vergeleken met data van SEM-EDX om een referentiekader te schetsen voor de performantie van de techniek. In een tweede case study werd onze nieuwe calibratiestrategie toegepast en werd er uitsluitend gebruik gemaakt van LA-ICP-MS, wat uitstekende resultaten opleverde. Met het oog op het bepalen van isotoopverhoudingen, werd er onderzocht wat de limieten zijn van het gebruik van een lage resolutie quadrupool massaspectrometer voor deze bepaling. Dit stelde ons in staat om de te verwachten accuraatheid en precisie in te schatten. De performantie bleek goed genoeg te zijn om weapon-grade plutonium te onderscheiden van global fall-out, zoals het werd aangetoond in de case study omtrent dit onderwerp. Uiteindelijk hebben we ook LA-ICP-MS geëvalueerd als een techniek voor elementaire beeldvorming, waarbij we tevens de meest courante multivariate data analyse hebben beschreven. Om de techniek te plaatsen tegenover andere elementaire technieken, werd een historisch verffragment geanalyseerd dat in het verleden reeds geanalyseerd was met SEM-EDX and μ-XRD. Op die manier konden we de resultaten accuraat vergelijken met de andere technieken. |
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Call Number |
UA @ admin @ c:irua:160063 |
Serial |
8152 |
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