Records |
Author |
de Gendt, S.; Kenis, K.; Mertens, P.W.; Heyns, M.M.; Claes, M.; Van Grieken, R.E.; Bailleul, A.; Knotter, M.; de Bokx, P.K. |
Title |
Use of grazing emission XRF spectrometry for silicon wafer surface contamination measurements |
Type |
P3 Proceeding |
Year |
1996 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:14679 |
Serial |
8720 |
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Author |
Claes, M.; de Bokx, P.; Van Grieken, R. |
Title |
Recent developments of laboratory grazing emission X-ray fluorescence spectrometry |
Type |
P1 Proceeding |
Year |
1999 |
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Issue |
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Pages |
103-107
T2 - Proceedings of the European Conferenc |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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000081658400015 |
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no |
Call Number |
UA @ admin @ c:irua:24718 |
Serial |
8459 |
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Author |
Claes, M.; Gysels, K.; Van Grieken, R.; Harrison, R.M. |
Title |
Inorganic compounds of atmospheric aerosols |
Type |
H3 Book chapter |
Year |
1998 |
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Issue |
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Pages |
95-145
T2 - Atmospheric particles / Harrison, R.M. |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:20968 |
Serial |
8104 |
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Author |
Claes, M.; van Ham, R.; Janssens, K.; Van Grieken, R.; Klockenkämper, R.; von Bohlen, A. |
Title |
Micro-analysis of artists' pigments by grazing-emission X-ray fluorescence spectrometry |
Type |
A3 Journal article |
Year |
1999 |
Publication |
Advances in X-ray analysis |
Abbreviated Journal |
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Volume |
41 |
Issue |
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Pages |
262-277 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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0376-0308 |
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Most recent IF: NA |
Call Number |
UA @ admin @ c:irua:24653 |
Serial |
5709 |
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Author |
Blockhuys, F.; Claes, M.; Van Grieken, R.; Geise, H.J. |
Title |
Assessing the molecular weight of a conducting polymer by grazing emission XRF |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
72 |
Issue |
14 |
Pages |
3366-3368 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000088347100054 |
Publication Date |
2002-07-26 |
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ISSN |
0003-2700; 5206-882x |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:27915 |
Serial |
7497 |
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Author |
Claes, M.; van Dyck, K.; Deelstra, H.; Van Grieken, R. |
Title |
Determination of silicon in organic matrices with grazing-emission X-ray fluorescence spectrometry |
Type |
A1 Journal article |
Year |
1999 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
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Volume |
54 |
Issue |
10 |
Pages |
1517-1524 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The potential of a prototype grazing-emission X-ray fluorescence spectrometer for reliable analysis of sample solutions, obtained by pressurized microwave oven digestion of Si-spiked organic and biological materials, was investigated as part of an inter-laboratory study. The fact that this grazing-emission technique is based on the total reflection phenomenon and wavelength-dispersive detection, gives it the benefit to determine light elements in a sensitive way. Results of the determination of silicon in pork liver, cellulose, urine, serum, spinach, beer, mineral water and horsetail (dry plant extract) samples are presented. Some of the results are compared with those obtained with other analytical techniques. The study proved that determination of silicon traces in biological matrices represents an extremely difficult task, however, measurements of silicon are achieved with acceptable precision. The most important problems still arise when sample pre-treatment is needed prior to analysis. (C) 1999 Elsevier Science B.V. All rights reserved. |
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Wos |
000083433600018 |
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2002-08-30 |
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ISSN |
0584-8547; 1873-3565 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:25943 |
Serial |
7789 |
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Author |
Spolnik, Z.M.; Claes, M.; Van Grieken, R. |
Title |
Determination of trace elements in organic matrices by grazing-emission X-ray fluorescence spectrometry |
Type |
A1 Journal article |
Year |
1999 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
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Volume |
401 |
Issue |
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Pages |
293-298 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000083981600037 |
Publication Date |
2002-07-25 |
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Edition |
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ISSN |
0003-2670; 1873-4324 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:27586 |
Serial |
7792 |
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Author |
Claes, M.; de Bokx, P.; Willard, N.; Veny, P.; Van Grieken, R. |
Title |
Optimization of sample preparation for grazing emission X-ray fluorescence in micro- and trace analysis applications |
Type |
A1 Journal article |
Year |
1997 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
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Volume |
52 |
Issue |
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Pages |
1063-1070 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1997XH53500035 |
Publication Date |
2002-07-26 |
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Series Issue |
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Edition |
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ISSN |
0584-8547; 1873-3565 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:18780 |
Serial |
8340 |
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Author |
Hołynska, B.; Olko, M.; Ostachowicz, B.; Ostachowicz, J.; Wegrzynek, D.; Claes, M.; Van Grieken, R.; de Bokx, P.; Kump, P.; Necemer, M. |
Title |
Performance of total reflection and grazing emission X-ray fluorescence spectrometry for the determination of trace metals in drinking water in relation to other analytical techniques |
Type |
A1 Journal article |
Year |
1998 |
Publication |
Fresenius' journal of analytical chemistry |
Abbreviated Journal |
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Volume |
362 |
Issue |
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Pages |
294-298 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000076461600011 |
Publication Date |
2002-08-25 |
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Series Issue |
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Edition |
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ISSN |
0937-0633; 1432-1130 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:22775 |
Serial |
8372 |
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Author |
Tsuji, K.; Sato, T.; Wagatsuma, K.; Claes, M.; Van Grieken, R. |
Title |
Preliminary experiment of total reflection x-ray fluorescence using two glancing x-ray beams excitation |
Type |
A1 Journal article |
Year |
1999 |
Publication |
The review of scientific instruments |
Abbreviated Journal |
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Volume |
70 |
Issue |
3 |
Pages |
1621-1623 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000079012100006 |
Publication Date |
2002-07-26 |
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Edition |
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ISSN |
0034-6748 |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:23184 |
Serial |
8407 |
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Author |
Claes, M.; de Bokx, P.; Van Grieken, R. |
Title |
Progress in laboratory grazing emission X-ray fluorescence spectrometry |
Type |
A1 Journal article |
Year |
1999 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
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Volume |
28 |
Issue |
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Pages |
224-229 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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000081693400004 |
Publication Date |
2005-12-05 |
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Edition |
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ISSN |
0049-8246 |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:24715 |
Serial |
8423 |
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Author |
Spolnik, Z.M.; Claes, M.; Van Grieken, R.E.; de Bokx, P.K.; Urbach, H.P. |
Title |
Quantification in grazing-emission X-ray fluorescence spectrometry |
Type |
A1 Journal article |
Year |
1999 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
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Volume |
54 |
Issue |
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Pages |
1525-1537 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000083433600019 |
Publication Date |
2002-08-30 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0584-8547; 1873-3565 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:27589 |
Serial |
8432 |
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Author |
Kuczumow, A.; Claes, M.; Schmeling, M.; Van Grieken, R.; de Gendt, S. |
Title |
Quantification problems in light element determination by grazing emission X-ray fluorescence |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
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Volume |
15 |
Issue |
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Pages |
415-421 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000086323700017 |
Publication Date |
2002-07-26 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0267-9477 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:27592 |
Serial |
8437 |
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Author |
van Dyck, K.; Robberecht, H.; van Cauwenbergh, R.; Deelstra, H.; Arnaud, J.; Willemyns, L.; Benijts, F.; Centeno, J.A.; Taylor, H.; Soares, M.E.; Bastos, M.L.; Ferreira, M.A.; d'Haese, P.C.; Lamberts, L.V.; Hoenig, M.; Knapp, G.; Lugowski, S.J.; Moens, L.; Riondato, J.; Van Grieken, R.; Claes, M.; Verheyen, R.; Clement, L.; Uytterhoeven, M. |
Title |
Spectrometric determination of silicon in food and biological samples: an interlaboratory trial |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
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Volume |
15 |
Issue |
6 |
Pages |
735-741 |
Keywords |
A1 Journal article; Behavioural Ecology & Ecophysiology; Pathophysiology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Accuracy and precision of silicon determination in biological matrices (serum, urine, water, beer and spinach) by spectrometric techniques (when necessary after acid destruction) were assessed by means of a collaborative interlaboratory trial. The trial was set up in accordance with ISO 5725-2 (1994). The relative overall repeatability standard deviation was acceptable. It varied between 4% for spinach powder (mean content: 176 mg kg(-1)) and 11% for serum (mean content: 5.33 mg L-1). On the other hand, the relative overall between-laboratory standard deviation was found to vary from a satisfactorily 15% for spinach after destruction (mean content: 3.32 mg L-1) to an unacceptable 107% for spinach powder (mean content: 176 mg kg(-1)). The overall conclusion of the trial was that silicon determination in biological matrices can properly be performed by spectrometric techniques. However, when sample pretreatment (i.e., acid destruction) is needed prior to silicon determination problems still remain. |
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000087419300025 |
Publication Date |
2002-07-26 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0267-9477 |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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no |
Call Number |
UA @ admin @ c:irua:27841 |
Serial |
8574 |
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