Records |
Author |
Vincze, L.; Vekemans, B.; Szaloki, I.; Brenker, F.E.; Falkenberg, G.; Rickers, K.; Aerts, K.; Van Grieken, R.; Adams, F. |
Title |
X-ray fluorescence microtomography and polycapillary based confocal imaging using synchrotron radiation |
Type |
P1 Proceeding |
Year |
2004 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
220-231
T2 - 4th Conference on Developments in X-R |
Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Ibis work illustrates the development of X-ray fluorescence tomography and polycapillary based confocal imaging towards a three-dimensional (313), quantitative analytical method with lateral resolution levels down to the 2-20 mum scale. Detailed analytical characterization is given for polycapillary based confocal XRF imaging, which is a new variant of the 3D micro-XRF technique. Applications for 2D/3D micro-XR-F are illustrated for the analysis of biological (zooplankton) and geological samples (microscopic inclusions in natural diamonds and fluid inclusions in quartz). Based on confocal imaging, fully three-dimensional distributions of trace elements could be obtained, representing a significant generalization of the regular 2D scanning technique for micro-XRF spectroscopy. The experimental work described in this paper has been carried out at the ESRF ID18F microfluorescence end-station and at HASYLAB Beam Line L. |
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000225665000023 |
Publication Date |
2004-11-02 |
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Series Issue |
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Edition |
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ISSN |
0-8194-5473-7 |
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no |
Call Number |
UA @ admin @ c:irua:94812 |
Serial |
8767 |
Permanent link to this record |
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Author |
Marguí, E.; Van Grieken, R. |
Title |
X-ray fluorescence spectrometry and related techniques : an introduction |
Type |
MA3 Book as author |
Year |
2013 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
148 p. |
Keywords |
MA3 Book as author; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISBN |
978-1-60650-391-1 |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:106179 |
Serial |
8768 |
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Author |
Eeckhaoudt, S.; Jacob, W.; Witters, H.; Van Grieken, R. |
Title |
X-ray micro-analysis of aluminium in pumpkinseed gills |
Type |
A1 Journal article |
Year |
1993 |
Publication |
European journal of morphology |
Abbreviated Journal |
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Volume |
31 |
Issue |
|
Pages |
42-45 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1993LQ28900009 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0924-3860 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:6370 |
Serial |
8769 |
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Author |
Eeckhaoudt, S.; Jacob, W.; Witters, H.; Van Grieken, R. |
Title |
X-ray micro-analysis of aluminium in pumpkinseed gills |
Type |
A1 Journal article |
Year |
1992 |
Publication |
European journal of morphology |
Abbreviated Journal |
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Volume |
30 |
Issue |
|
Pages |
296-299 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISSN |
0924-3860 |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:2846 |
Serial |
8770 |
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Author |
Szalóki, I.; Osán, J.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
2006 |
Publication |
Analytical chemistry |
Abbreviated Journal |
|
Volume |
78 |
Issue |
12 |
Pages |
4069-4096 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
000238252600016 |
Publication Date |
2006-06-10 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:58857 |
Serial |
8771 |
Permanent link to this record |
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Author |
Szalóki, I.; Osán, J.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
2004 |
Publication |
Analytical chemistry |
Abbreviated Journal |
|
Volume |
76 |
Issue |
12 |
Pages |
3445-3470 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
000222011100014 |
Publication Date |
2004-06-14 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:46259 |
Serial |
8772 |
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Author |
Szalóki, I.; Török, S.B.; Injuk, J.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
2002 |
Publication |
Analytical chemistry |
Abbreviated Journal |
|
Volume |
74 |
Issue |
12 |
Pages |
2895-2918 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Wos |
000176253700020 |
Publication Date |
2002-07-26 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:39517 |
Serial |
8773 |
Permanent link to this record |
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Author |
Szalóki, I.; Török, S.B.; Ro, C.-U.; Injuk, J.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Analytical chemistry |
Abbreviated Journal |
|
Volume |
72 |
Issue |
12 |
Pages |
211-233 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
000087661500018 |
Publication Date |
2002-07-26 |
Series Editor |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Times cited |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:27850 |
Serial |
8774 |
Permanent link to this record |
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Author |
Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
H3 Book chapter |
Year |
2000 |
Publication |
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Abbreviated Journal |
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Volume |
15 |
Issue |
|
Pages |
13269-13443
T2 - Encyclopedia of analytical chemis |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:31650 |
Serial |
8775 |
Permanent link to this record |
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Author |
Török, S.; Labar, J.; Schmeling, M.; Van Grieken, R. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1998 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
70 |
Issue |
|
Pages |
495r-517r |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Wos |
000074161100020 |
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Series Editor |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:20967 |
Serial |
8776 |
Permanent link to this record |
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Author |
Török, S.B.; Labar, J.; Injuk, J.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1996 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
R68 |
Issue |
|
Pages |
467-485 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Edition |
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ISSN |
0003-2700; 5206-882x |
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UA library record |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:14650 |
Serial |
8777 |
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Author |
Török, S.B.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1992 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
64r |
Issue |
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Pages |
180-196 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
A1992HZ51800011 |
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ISSN |
0003-2700; 5206-882x |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:2823 |
Serial |
8778 |
Permanent link to this record |
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Author |
Markowicz, A.A.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1990 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
62 |
Issue |
12 |
Pages |
101r-113r |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Publication Date |
2006-11-06 |
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Edition |
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ISSN |
0003-2700; 5206-882x |
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UA library record |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116527 |
Serial |
8779 |
Permanent link to this record |
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Author |
Markowicz, A.A.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
60 |
Issue |
12 |
Pages |
28r-42r |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Publication Date |
2005-03-08 |
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Edition |
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ISSN |
0003-2700; 5206-882x |
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no |
Call Number |
UA @ admin @ c:irua:116525 |
Serial |
8780 |
Permanent link to this record |
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Author |
Markowicz, A.A.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1986 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
58 |
Issue |
5 |
Pages |
279r-294r |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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2005-03-08 |
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0003-2700; 5206-882x |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:116523 |
Serial |
8781 |
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Author |
Markowicz, A.A.; Van Grieken, R.E. |
Title |
X-ray spectrometry |
Type |
A1 Journal article |
Year |
1984 |
Publication |
Reviews in analytical chemistry |
Abbreviated Journal |
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Volume |
56 |
Issue |
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Pages |
241r-250r |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Edition |
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ISSN |
0048-752x |
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no |
Call Number |
UA @ admin @ c:irua:116709 |
Serial |
8782 |
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Author |
Van Grieken, R.; Delalieux, F. |
Title |
X-ray spectrometry for air pollution and cultural heritage research |
Type |
P3 Proceeding |
Year |
2004 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:51259 |
Serial |
8783 |
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Author |
Van Grieken, R.; Makarovska, Y.; van Meel, K.; Worobiec, A. |
Title |
X-ray spectrometry for analysis of atmospheric particulate matter: detection limits versus legal levels |
Type |
H3 Book chapter |
Year |
2007 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
153-161
T2 - Topics in X-ray spectrometry / Vázque |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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no |
Call Number |
UA @ admin @ c:irua:64402 |
Serial |
8784 |
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Author |
Van Grieken, R.; Worobiec, A. |
Title |
X-ray spectrometry for preventive conservation of cultural heritage |
Type |
A1 Journal article |
Year |
2011 |
Publication |
Pramåna: a journal of physics |
Abbreviated Journal |
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Volume |
72 |
Issue |
2 |
Pages |
191-200 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
Analytical chemistry does play a key role in the chemical characterization of the environment and it appears that X-ray spectrometry, in its many forms, is one of the most relevant analytical techniques in preventive conservation, as it is in cultural heritage research in general. X-ray spectrometry has indeed been the method of choice for the characterization of the inorganic composition of atmospheric aerosols, for a long time. We have, over the last decade, intensively used various forms of X-ray spectrometry, viz., mostly energy-dispersive X-ray fluorescence, e.g. with polarized high-energy beam excitation, and automated electron probe X-ray microanalysis, together with other techniques, to identify particle types and their sources in indoor environments, including museums, while gaseous indoor pollutants were assessed using passive diffusion samplers. In each case, both bulk aerosols and individual aerosol particles were studied. For microanalysis of single particles, we have investigated a dozen techniques, but for wide, real-life applications, automated electron probe X-ray microanalysis is the most rewarding. We have first studied atmospheric aerosols in and around the Correr Museum in Venice, many other museums in Austria, Japan and England, and in the caves with prehistoric rock paintings in Altamira, Spain. Very recently, measurements were done in the Metropolitan Museum of Art in New York and theWawel Castle in Cracow, in Italian and Polish mountain churches, in a number of museums in Belgium and the Netherlands, and in cathedrals with medieval stained glass windows. In the Correr museum, it appeared that the particles most threatening for the Bellini paintings were released by the deteriorating plaster renderings, and this could be avoided by simply improving the rendering on the museum walls. In the Wawel Castle, outdoor pollution particles, like fine soot from diesel traffic, entering via leaks in the windows and doors, and also street-deicing salts and coal burning pollution particles, brought in by visitors, mostly in winter, were found to be most worrisome. Urgent questions that are not solved at this moment pertain to the deposition processes from the atmosphere to the cultural heritage items, the critical surface interactions that take place on these items, and the establishment of suitable particle concentration standards. |
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000288861000002 |
Publication Date |
2011-05-20 |
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Series Issue |
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Edition |
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ISSN |
0304-4289; 0973-7111 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:87025 |
Serial |
8785 |
Permanent link to this record |
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|
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Author |
Tsuji, K.; Injuk, J.; Van Grieken, R. |
Title |
X-ray spectrometry: recent technological advances |
Type |
ME1 Book as editor or co-editor |
Year |
2004 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
|
Pages |
616 p. |
Keywords |
ME1 Book as editor or co-editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
|
ISBN |
0-471-48640-x |
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
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Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:43876 |
Serial |
8786 |
Permanent link to this record |
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|
|
Author |
Van Alsenoy, W.; Bernard, P.; Van Grieken, R. |
Title |
Zware metalen in Noordzee- en Schelde-sedimenten |
Type |
A3 Journal article |
Year |
1990 |
Publication |
Wtare |
Abbreviated Journal |
|
Volume |
5 |
Issue |
|
Pages |
113-121 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116829 |
Serial |
8787 |
Permanent link to this record |
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Author |
Felipe Montiel, N.; Parrilla, M.; Beltrán, V.; Nuyts, G.; Van Durme, F.; De Wael, K. |
Title |
The opportunity of 6-monoacetylmorphine to selectively detect heroin at preanodized screen printed electrodes |
Type |
A1 Journal Article |
Year |
2021 |
Publication |
Talanta |
Abbreviated Journal |
Talanta |
Volume |
|
Issue |
|
Pages |
122005 |
Keywords |
A1 Journal Article; Antwerp X-ray Analysis, Electrochemistry and Speciation (AXES) ; |
Abstract |
The illicit consumption of heroin is an increasing concern in our society. For this reason, rapid analytical methods to seize heroin samples in the field are of paramount importance to hinder drug trafficking, and thus prevent the availability of heroin in the drug market. The present work reports on the enriched electrochemical fingerprint of heroin, allowing its selective detection in street samples, based on the use of electrochemical pretreated screen printed electrodes (p-SPE). The voltammetric identification is built on two oxidation peaks of both heroin and its degradation product 6-monoacetylmorphine (6-MAM), generated in alkaline conditions. Interestingly, an anodic pretreatment of the screen printed electrodes (SPE) shifts the peak potential of paracetamol (the most encountered cutting agent in heroin seizures), allowing the detection of 6-MAM peak, overlapping with the paracetamol signal in the case of untreated SPE. Subsequently, the characterization of the p-SPE with scanning electron microscopy, cyclic voltammetry, electrochemical impedance spectroscopy, Raman and Fourier transform infrared (FTIR) spectroscopy is provided to demonstrate local changes on the surface of the electrode. From an analytical perspective, p-SPE provide higher sensitivity (0.019 μA μM-1), excellent reproducibility (6-MAM, RSD = 2.85%, and heroin RSD = 0.91%, n = 5) and lower limits of detection (LOD) (5.2 μM) in comparison to untreated SPE. The proposed protocol which integrates a tailor-made script is interrogated against common cutting agents, and finally, validated with the screening of 14 street samples, also analyzed by standard methods. Besides, a comparison with portable spectroscopic techniques on the confiscated samples shows the better performance of the electrochemical strategy. Overall, this sensing approach offers promising results for the rapid on-site profiling of suspicious heroin samples, also in the presence of paracetamol. |
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000656959000033 |
Publication Date |
2021-01-20 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0039-9140 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
4.162 |
Times cited |
|
Open Access |
OpenAccess |
Notes |
This project has received funding from the European Union’s Horizon 2020 research and innovation programme under the grant agreement No 833787, BorderSens. The authors acknowledge financial support from the University of Antwerp (IOF). |
Approved |
Most recent IF: 4.162 |
Call Number |
AXES @ axes @c:irua:174844 |
Serial |
6663 |
Permanent link to this record |