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Author	Meynen, V.; Busuioc, A.M.; Beyers, E.; Cool, P.; Vansant, E.F.; Bilba, N.; Mertens, M.; Lebedev, O.; Van Tendeloo, G.
Title	Nanodesign of combined micro- and mesoporous materials for specific applications in adsorption and catalysis			Type	H3 Book chapter
Year	2007	Publication		Abbreviated Journal
Volume		Issue		Pages
Keywords	H3 Book chapter; Electron microscopy for materials research (EMAT); Laboratory of adsorption and catalysis (LADCA)
Abstract
Address
Corporate Author				Thesis
Publisher	Nova	Place of Publication	New York	Editor
Language		Wos		Publication Date	0000-00-00
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN		ISBN		Additional Links	UA library record
Impact Factor		Times cited		Open Access
Notes				Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:63126			Serial	2251
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Author	Lebedev, O.I.; Van Tendeloo, G.; Amelinckx, S.; Leibold, B.; Habermeier, H.U.; Phillipp, F.
Title	Structure and magnetotransport properties of La_2/3Ca_1/3MnO₃ thin films prepared by pulsed laser deposition			Type	P1 Proceeding
Year	1998	Publication	Materials Research Society symposium proceedings T2 – Symposium on Advances in Laser Ablation of Materials at the 1998 MRS, Spring Meeting, April 13-16, 1998, San Francisco, Calif.	Abbreviated Journal
Volume		Issue		Pages	219-224
Keywords	P1 Proceeding; Electron microscopy for materials research (EMAT)
Abstract	La1-xCaxMnO3-delta (LCMO) thin films are grown by pulsed laser deposition on a (100) SrTiO3 substrate at temperatures between 530 degrees C and 890 degrees C. The magnetotransport properties show a high negative magnetoresistance and a shift of the maximum of the R(T) curve as function of temperature. The Curie temperature changes with deposition temperature and film quality in the range of 100-220K. The film quality is characterised by X-ray diffraction and transmission electron microscopy (TEM); film and target compositions were verified by atomic emission spectroscopy. The local structure of the film depends on the growth conditions and substrate temperature. TEM reveals a slight distortion of the film leading to a breakdown of the symmetry from orthorhombic to monoclinic. At the highest growth temperatures, a well defined interface is observed within the LCMO film, parallel to the substrate surface; this interface divides the film into two lamellae with a different microstructure. The lamella close to the substrate is perfectly coherent with the substrate, suggesting that it is strained as a result of the lattice parameter mismatch; the upper lamella shows a typical domain structure with unusual translation interfaces characterised by a displacement vector of the type 1/2[010](m) and 1/2[001](m) when referred ten the monoclinic lattice.
Address
Corporate Author				Thesis
Publisher	Materials research society	Place of Publication	Warrendale	Editor
Language		Wos	000077696000032	Publication Date	2011-04-05
Series Editor		Series Title		Abbreviated Series Title
Series Volume	526	Series Issue		Edition
ISSN	1946-4274;	ISBN		Additional Links	UA library record; WoS full record
Impact Factor		Times cited		Open Access
Notes				Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:95838			Serial	3283
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Author	Vernimmen, J.; Meynen, V.; Mertens, M.; Lebedev, O.I.; Van Tendeloo, G.; Cool, P.
Title	Formation of a Ti-siliceous trimodal material with macroholes, mesopores and zeolitic features via a one-pot templating synthesis			Type	A1 Journal article
Year	2012	Publication	Journal of porous materials	Abbreviated Journal	J Porous Mat
Volume	19	Issue	2	Pages	153-160
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT); Laboratory of adsorption and catalysis (LADCA)
Abstract	Based on a facile one-pot templating synthesis, using a TS-1 zeolite recipe whereby part of the zeolite structure directing agent is replaced by a mesopore templating agent, a trimodal material is formed. The resulting meso-TSM material combines mesoporosity (Ti-MCM-41) with zeolitic features (TS-1) and a unique sheet-like morphology with uniform macroporous voids (macroholes). Moreover, the macrohole formation, mesoporosity and zeolitic properties of the meso-TSM material can be controlled in a straightforward way by adjusting the length of the hydrothermal treatment. This newly developed material may imply great potential for catalytic redox applications and diffusion limitated processes because of its highly tunable character in all three dimensions (micro-, meso- and macroporous scale).
Address
Corporate Author				Thesis
Publisher	Kluwer Academic	Place of Publication	Boston, Mass.	Editor
Language		Wos	000301187600002	Publication Date	2011-03-28
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	1380-2224;1573-4854;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	1.624	Times cited	2	Open Access
Notes	Fwo; Goa			Approved	Most recent IF: 1.624; 2012 IF: 1.348
Call Number	UA @ lucian @ c:irua:88367			Serial	1257
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Author	Van Tendeloo, G.; Lebedev, O.I.; Verbist, K.; Abakumov, A.M.; Shpanchenko, R.V.; Antipov, E.V.; Blank, D.H.A.
Title	The local structure of YBCO based materials by TEM			Type	H1 Book chapter
Year	1999	Publication		Abbreviated Journal
Volume		Issue		Pages	11-19
Keywords	H1 Book chapter; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	Kluwer Academic	Place of Publication	Dordrecht	Editor
Language		Wos	000079308200002	Publication Date	0000-00-00
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN		ISBN		Additional Links	UA library record; WoS full record;
Impact Factor		Times cited		Open Access
Notes				Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:29709			Serial	1833
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Author	Lebedev, O.; Van Tendeloo, G.; Amelinckx, S.; Leibold, B.; Habermeier, H.U.
Title	HREM investigation of La(1-x)Ca(x)MnO3-delta thin films			Type	P1 Proceeding
Year	1998	Publication		Abbreviated Journal
Volume		Issue		Pages	517-518
Keywords	P1 Proceeding; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	IOP Publishing Ltd	Place of Publication	Bristol	Editor
Language		Wos	000077019900254	Publication Date	0000-00-00
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0-7503-0565-7	ISBN		Additional Links	UA library record; WoS full record;
Impact Factor		Times cited		Open Access
Notes				Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:95856			Serial	1504
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Author	de Gryse, O.; Clauws, P.; Lebedev, O.; van Landuyt, J.; Vanhellemont, J.; Claeys, C.; Simoen, E.
Title	Chemical and structural characterization of oxygen precipitates in silicon by infrared spectroscopy and TEM			Type	A1 Journal article
Year	2001	Publication	Physica: B : condensed matter T2 – 21st International Conference on Defects in Semiconductors, JUL 16-20, 2001, GIESSEN, GERMANY	Abbreviated Journal	Physica B
Volume	308	Issue		Pages	294-297
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Infrared absorption spectra of polyhedral and platelet oxygen precipitates are analyzed using a modified Day-Thorpe approach (J. Phys.: Condens. Matter 11 (1999) 2551). The aspect ratio has been determined by TEM measurements. The reduced spectral function and the stoichiometry are extracted from the absorption spectra and the concentration of precipitated interstitial oxygen. One set of spectra reveal a Frohlich frequency around 1100 cm(-1) and another around 1110-1120 cm(-1). It is shown that the shift in the Frohlich frequency is not due to a different stoichiometry, but due to the detailed structure in the reduced spectral function. The oxygen precipitates consist of SiO. with gammaapproximate to1.1-1.2+/-0.1. (C) 2001 Elsevier Science B.V. All rights reserved.
Address
Corporate Author				Thesis
Publisher	Elsevier science bv	Place of Publication	Amsterdam	Editor
Language		Wos	000173660100073	Publication Date	2002-10-15
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0921-4526;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	1.386	Times cited	3	Open Access
Notes				Approved	Most recent IF: 1.386; 2001 IF: 0.663
Call Number	UA @ lucian @ c:irua:103389			Serial	345
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Author	Blank, D.H.A.; Rijnders, A.J.H.M.; Verhoeven, M.A.J.; Bergs, R.M.H.; Rogalla, H.; Verbist, K.; Lebedev, O.; Van Tendeloo, G.
Title	Characterisation of multilayer ramp-type REBa₂Cu₃O_7-\delta structures by scanning probe microscopy and high-resolution electron microscopy			Type	A1 Journal article
Year	1997	Publication	Journal of alloys and compounds T2 – Symposium on High Temperature Superconductor Thin Films, Growth, Mechanisms, Interfaces, Multilayers, at the 1996 Spring Meeting of the European-Materials-Society, June 04-07, 1996, Strasbourg, France	Abbreviated Journal	J Alloy Compd
Volume	251	Issue	1-2	Pages	206-208
Keywords	A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT)
Abstract	We studied the morphology of ramps in REBa2CU3O7 (REBCO) epitaxial films on SrTiO3 substrates, fabricated by RF magnetron sputter deposition and pulsed laser deposition (PLD), by scanning probe microscopy (SPM) and high resolution electron microscopy (HREM). The ramps were fabricated by Ar ion beam etching using masks of standard photoresist and TIN. AFM-studies on ramps in sputter deposited films show a strong dependence, i.e. formation of facets and ridges, on the angle of incidence of the ion beam with respect to the substrate surface as well as the rotation angle with respect to the crystal axes of the substrate. Ramps in pulsed laser deposited films did not show this dependence, Furthermore, we studied the effect of an anneal step prior to the deposition of barrier layers (i.e. PrBa2CU3O7, SrTiO3, CeO2) on the ramp. First results show a recrystallization of the ramp surface, resulting in terraces and a non-homogeneous growth of the barrier material on top of it. The thickness variations, for thin layers of barrier material, con even become much larger than expected from the amount of deposited material and are dependent on the deposition and anneal conditions. HREM studies show a well defined interface between barrier layer and electrodes. The angle of the ramp depends on the etch rate of the mask and REBCO, and on the angle of incidence of the ion beam. TiN has a much lower etch rate compared to photoresist, resulting in an angle of the ramp comparable to the angle of incidence, resulting in a low etching rate on the ramp. These results will lead to improved electrical characteristics of ramp-type junctions.
Address
Corporate Author				Thesis
Publisher	Elsevier Science	Place of Publication	Lausanne	Editor
Language		Wos	A1997XM34000046	Publication Date	2002-07-25
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0925-8388;	ISBN		Additional Links	UA library record; WoS full record
Impact Factor	3.133	Times cited		Open Access
Notes				Approved	Most recent IF: 3.133; 1997 IF: 1.035
Call Number	UA @ lucian @ c:irua:95868			Serial	310
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Author	Antipov, E.V.; Putilin, S.N.; Shpanchenko, R.V.; Alyoshin, V.A.; Rozova, M.G.; Abakumov, A.M.; Mikhailova, D.A.; Balagurov, A.M.; Lebedev, O.; Van Tendeloo, G.
Title	Structural features, oxygen and fluorine doping in Cu-based superconductors			Type	A1 Journal article
Year	1997	Publication	Physica: C : superconductivity T2 – International Conference on Materials and Mechanisms of, Superconductivity – High Temperature Superconductors V, Feb. 28-Mar. 04, 1997, Beijing, Peoples R. China	Abbreviated Journal	Physica C
Volume	282	Issue	Part 1	Pages	61-64
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	The variation of structures and superconducting properties by changing extra oxygen or fluorine atoms concentration in Hg-based Cu mixed oxides and YBa2Cu3O6+delta was studied. The data obtained by NPD study of Hg-1201 can be considered as an evidence of the conventional oxygen doping mechanism with 2 delta holes per (CuO2) layer. The extra oxygen atom was found to be located in the middle of the Hg mesh only. Different formal charges of oxygen and fluorine inserted into reduced 123 structure results in its distinct variations. The fluorine incorporation into strongly reduced YBa2Cu3O6+delta causes a significant structural rearrangement and the formation of a new compound with a composition close to YBa2Cu3O6F2 (tetragonal alpha = 3.87 Angstrom and c approximate to 13 Angstrom), which structure was deduced from the combined results of X-ray diffraction, electron diffraction and high resolution electron microscopy. Fluorination treatment by XeF2 of nonsuperconducting 123 samples causes an appearance of bulk superconductivity with T-c up to 94K.
Address
Corporate Author				Thesis
Publisher	Elsevier Science	Place of Publication	Amsterdam	Editor
Language		Wos	A1997XZ90400019	Publication Date	2002-07-25
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0921-4534;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	1.404	Times cited	10	Open Access
Notes				Approved	Most recent IF: 1.404; 1997 IF: 2.199
Call Number	UA @ lucian @ c:irua:95866			Serial	3237
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Author	Köster, S.; Moshnyaga, V.; Samwer, K.; Lebedev, O.I.; Van Tendeloo, G.; Shapoval, O.; Belenchuk, A.
Title	Doping of interfaces in (La_0.7Sr_0.3MnO₃)_1-x:(MgO)_x composite films			Type	A1 Journal article
Year	2002	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	81	Issue	9	Pages	1648-1650
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000177549200036	Publication Date	2002-09-30
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	35	Open Access
Notes				Approved	Most recent IF: 3.411; 2002 IF: 4.207
Call Number	UA @ lucian @ c:irua:54802			Serial	751
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Author	Hezareh, T.; Razavi, F.S.; Kremer, R.K.; Habermeier, H.-U.; Lebedev, O.I.; Kirilenko, D.; Van Tendeloo, G.
Title	Effect of PbZr_0.52Ti_0.48O₃ thin layer on structure, electronic and magnetic properties of La_0.65Sr_0.35MnO₃ and La_0.65Ca_0.30MnO₃ thin-films			Type	A1 Journal article
Year	2011	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	109	Issue	11	Pages	113707,1-113707,8
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Epitaxial thin film heterostructures of high dielectric PbZr<sub>1-x</sub>Ti<sub>x</sub>O<sub>3</sub> (PZT) and La<sub>1-x</sub>A<sub>x</sub>MnO<sub>3</sub> (A-divalent alkaline earth metals such as Sr (LSMO) and Ca (LCMO)) were grown on SrTiO<sub>3</sub> substrates and their structure, temperature dependence of electrical resistivity, and magnetization were investigated as a function of the thickness of the LSMO(LCMO) layer. The microstructures of the samples were analyzed by TEM. By applying an electric field across the PZT layer, we applied a ferrodistortive pressure on the manganite layer and studied the correlations between lattice distortion and electric transport and magnetic properties of the CMR materials.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000292214700069	Publication Date	2011-06-06
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	4	Open Access
Notes				Approved	Most recent IF: 2.068; 2011 IF: 2.168
Call Number	UA @ lucian @ c:irua:90964			Serial	843
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Author	Verbeeck, J.; Lebedev, O.I.; Van Tendeloo, G.; Silcox, J.; Mercey, B.; Hervieu, M.; Haghiri-Gosnet, A.M.
Title	Electron energy-loss spectroscopy study of a (LaMnO₃)₈(SrMnO₃)₄ heterostructure			Type	A1 Journal article
Year	2001	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	79	Issue	13	Pages	2037-2039
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	An epitaxially grown heterostructure consisting of alternating layers of LaMnO3 (8 unit cells) and SrMnO3 (4 unit cells) on a SrTiO3 substrate has been studied by a combination of electron energy-loss spectroscopy (EELS) and high-resolution transmission electron microscopy (HRTEM) on an atomic scale. Excitation edges of all elements are captured with subnanometer spatial accuracy, and parametrized to obtain chemical profiles. The fine-edge structure of O K and Mn L-2,L-3 edges are interpreted as signatures of the local electronic structure and show a spatial modulation of the concentration of holes with O 2p character. The chemical concentration is found to be different for the bottom and top interface of a SrMnO3 layer. HRTEM complements the EELS results and confirms the asymmetry of the interfaces. (C) 2001 American Institute of Physics.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000171015200036	Publication Date	2002-07-26
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	19	Open Access
Notes				Approved	Most recent IF: 3.411; 2001 IF: 3.849
Call Number	UA @ lucian @ c:irua:54799UA @ admin @ c:irua:54799			Serial	933
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Author	Razavi, F.S.; Gross, G.; Habermeier, H.-U.; Lebedev, O.; Amelinckx, S.; Van Tendeloo, G.; Vigliante, A.
Title	Epitaxial strain induced metal insulator transition in La_0.9Sr_0.1MnO₃ and La_0.88Sr_0.1MnO₃ thin films			Type	A1 Journal article
Year	2000	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	76	Issue	2	Pages	155-157
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	We are reporting an unexpected metal insulator transition at the ferromagnetic phase-transition temperature for thin films of La0.9Sr0.1MnO3 (< 50 nm), grown on a (100) face of SrTiO3 substrate. For the thicker films (> 50 nm), similar to the single crystal, no such transition is observed below T-C. Additionally, we observe the suppression of the features associated with charge or orbital ordering in intentionally La-deficient thin films of La0.88Sr0.1MnO3 (< 75 nm). In thin films, transmission electron microscopy reveals a compressive strain due to the epitaxial growth, that is, lattice parameters adopt those of the cubic lattice of SrTiO3. As the film thickness increases, coherent microtwinning is observed in the films and the films relax to a orthorhombic structure. (C) 2000 American Institute of Physics. [S0003-6951(00)00402-2].
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000084541000009	Publication Date	2002-07-26
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	91	Open Access
Notes				Approved	Most recent IF: 3.411; 2000 IF: 3.906
Call Number	UA @ lucian @ c:irua:99441			Serial	1073
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Author	Verbist, K.; Lebedev, O.I.; Van Tendeloo, G.; Verhoeven, M.A.J.; Rijnders, A.J.H.M.; Blank, D.H.A.; Rogalia, H.
Title	Ga segregation in DyBa₂Cu₃O_7-\delta/PrBa₂Cu_3-xGa_xO_7-\delta/DyBa₂Cu₃O_7-\delta ramp-type Josephson junctions			Type	A1 Journal article
Year	1997	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	70	Issue	9	Pages	1167-1169
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	A1997WL14700036	Publication Date	0000-00-00
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951; 1077-3118	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	8	Open Access
Notes				Approved	Most recent IF: 3.411; 1997 IF: 3.033
Call Number	UA @ lucian @ c:irua:21426			Serial	1312
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Author	Maignan, A.; Singh, K.; Simon, C.; Lebedev, O.I.; Martin, C.; Tan, H.; Verbeeck, J.; Van Tendeloo, G.
Title	Magnetic and magnetodielectric properties of erbium iron garnet ceramic			Type	A1 Journal article
Year	2013	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	113	Issue	3	Pages	033905-5
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	An Er3Fe5O12 ceramic has been sintered in oxygen atmosphere at 1400 °C for dielectric measurements. Its structural quality at room temperature has been checked by combining transmission electron microscopy and X-ray diffraction. It crystallizes in the cubic space group Ia3d with a = 12.3488(1). The dielectric permittivity ([variantgreekepsilon]′) and losses (tan δ) measurements as a function of temperature reveal the existence of two anomalies, a broad one between 110 K and 80 K, attributed to the Er3+ spin reorientation, and a second sharper feature at about 45 K associated to the appearance of irreversibility on the magnetic susceptibility curves. In contrast to the lack of magnetic field impact on [variantgreekepsilon]′ for the former anomaly, a complex magnetic field effect has been evidenced below 45 K. The isothermal [variantgreekepsilon]′(H) curves show the existence of positive magnetodielectric effect, reaching a maximum of 0.14% at 3 T and 10 K. Its magnitude decreases as H is further increased. Interestingly, for the lowest H values, a linear regime in the [variantgreekepsilon]′(H) curve is observed. From this experimental study, it is concluded that the [variantgreekepsilon]′ anomaly, starting above the compensation temperature Tc (75 K) and driven by the internal magnetic field, is not sensitive to an applied external magnetic field. Thus, below 45 K, it is the magnetic structure which is responsible for the coupling between spin and charge in this iron garnet.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000313670600042	Publication Date	2013-01-16
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	15	Open Access
Notes	Vortex; Countatoms ECASJO_;			Approved	Most recent IF: 2.068; 2013 IF: 2.185
Call Number	UA @ lucian @ c:irua:106182UA @ admin @ c:irua:106182			Serial	1861
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Author	Ignatova, V.A.; Lebedev, O.I.; Watjen, U.; van Vaeck, L.; van Landuyt, J.; Gijbels, R.; Adams, F.
Title	Metal and composite nanocluster precipitate formation in silicon dioxide implanted with Sb+ ions			Type	A1 Journal article
Year	2002	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	92	Issue	8	Pages	4336-4341
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT); Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT)
Abstract
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000178318000024	Publication Date	2002-10-07
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	5	Open Access
Notes				Approved	Most recent IF: 2.068; 2002 IF: 2.281
Call Number	UA @ lucian @ c:irua:39872			Serial	2005
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Author	Maignan, A.; Lebedev, O.I.; Van Tendeloo, G.; Martin, C.; Hébert, S.
Title	Negative magnetoresistance in a V³⁺/V⁴⁺ mixed valent vanadate			Type	A1 Journal article
Year	2010	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	96	Issue	23	Pages	232502,1-232502,3
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	The magnetotransport and magnetic properties of the PbV6O11 vanadate, crystallizing in the P63mc space group, reveal the existence of a negative magnetoresistance related to its ferromagnetic state (TC ∼ 90 K). The maximum effect is observed at 20 K reaching −30% in 9 T. The structural study of this ceramic reveals a V/Pb ratio smaller than expected from the formula. This is explained by the presence of numerous stacking faults observed by high resolution transmission electron microscopy. The existence of these planar defects acting as resistive barriers along the c axis could be responsible for tunneling magnetoresistance.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000278695900045	Publication Date	2010-06-08
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited		Open Access
Notes				Approved	Most recent IF: 3.411; 2010 IF: 3.841
Call Number	UA @ lucian @ c:irua:83293			Serial	2291
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Author	Gryse, O.D.; Clauws, P.; van Landuyt, J.; Lebedev, O.; Claeys, C.; Simoen, E.; Vanhellemont, J.
Title	Oxide phase determination in silicon using infrared spectroscopy and transmission electron microscopy techniques			Type	A1 Journal article
Year	2002	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	91	Issue	4	Pages	2493-2498
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Infrared absorption spectra of polyhedral and platelet oxygen precipitates in silicon are analyzed using a modified Day-Thorpe approach [J. Phys.: Condens. Matter 11, 2551 (1999)]. The aspect ratio of the precipitates is determined by transmission electron microscopy analysis. The reduced spectral function and the stoichiometry of the precipitate are extracted from the absorption spectra and the amount of precipitated interstitial oxygen. The experimental absorption spectra can be divided in a set with a Frohlich frequency of around 1100 cm(-1) and in a set with a Frohlich frequency between 1110 and 1120 cm(-1). It is shown that the shift in the Frohlich frequency is not due to a differing stoichiometry, but to the detailed structure of the reduced spectral function. Inverse modeling of the spectra suggests that the oxide precipitates consist of substoichiometric SiOgamma with gamma=1.17+/-0.14. (C) 2002 American Institute of Physics.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000173553800114	Publication Date	2002-07-26
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	27	Open Access
Notes				Approved	Most recent IF: 2.068; 2002 IF: 2.281
Call Number	UA @ lucian @ c:irua:103372			Serial	2542
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Author	Verbist, K.; Lebedev, O.I.; Van Tendeloo, G.; Tafuri, F.; Granozio, F.M.; Di Chiara, A.; Bender, H.
Title	A potential method to correlate electrical properties and microstructure of a unique high-T_c superconducting Josephson junction			Type	A1 Journal article
Year	1999	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	74	Issue	7	Pages	1024-1026
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	A method to correlate microstructure from cross-section transmission electron microscopy (TEM) investigations and transport properties of a single well characterized high-T-c artificial grain boundary junction is reported. A YBa2Cu3O7-delta 45 degrees twist junction exhibiting the typical phenomenology of high T-c Josephson weak links was employed. The TEM sample preparation is based on focused ion beam etching and allows to easily localize the electron transparent area on a microbridge. The reported technique opens clear perspectives in the determination of the microstructural origin of variations in Josephson junction properties, such as the spread in I-c and IcRN values and the presence of different transport regimes in nominally identical junctions. (C) 1999 American Institute of Physics. [S0003-6951(99)03404-X].
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000078571400043	Publication Date	2002-07-26
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	5	Open Access
Notes				Approved	Most recent IF: 3.411; 1999 IF: 4.184
Call Number	UA @ lucian @ c:irua:102912			Serial	2686
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Author	Wouters, J.; Lebedev, O.I.; Van Tendeloo, G.; Yamada, H.; Sato, N.; Vanacken, J.; Moshchalkov, V.V.; Verbiest, T.; Valev, V.K.
Title	Preparing polymer films doped with magnetic nanoparticles by spin-coating and melt-processing can induce an in-plane magnetic anisotropy			Type	A1 Journal article
Year	2011	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	109	Issue	7	Pages	076105-076105,3
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Faraday rotation has been used to investigate a series of polymer films doped with magnetic iron oxide nanoparticles. The films have been prepared by spin-coating and melt-processing. In each case, upon varying the angle of optical incidence on the films, an in-plane magnetic anisotropy is observed. The effect of such an anisotropy on the Faraday rotation as a function of the angle of optical incidence is verified by comparison with magnetically poled films. These results demonstrate that care should be taken upon analyzing the magnetic behavior of such films on account of the sample preparation techniques themselves being able to affect the magnetization.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000289949000166	Publication Date	2011-04-12
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	10	Open Access
Notes	Fwo; Iap; Iwt			Approved	Most recent IF: 2.068; 2011 IF: 2.168
Call Number	UA @ lucian @ c:irua:89917			Serial	2709
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Author	Kalkert, C.; Krisponeit, J.-O.; Esseling, M.; Lebedev, O.I.; Moshnyaga, V.; Damaschke, B.; Van Tendeloo, G.; Samwer, K.
Title	Resistive switching at manganite/manganite interfaces			Type	A1 Journal article
Year	2011	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	99	Issue	13	Pages	132512-132512,3
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	We report bipolar resistive switching between the interfaces of manganite nanocolumns. La0.7Sr0.3MnO3 films were prepared on Al2O3 substrates, where the films grow in nanocolumns from the substrate to the surface. Conductive atomic force microscopy directly detects that the resistive switching is located at the boundaries of the grains. Furthermore, mesoscopic transport measurements reveal a tunnel magnetoresistance. In combination with the resistive switching, this leads to a total of four different resistive states.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000295618000052	Publication Date	2011-09-29
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	10	Open Access
Notes				Approved	Most recent IF: 3.411; 2011 IF: 3.844
Call Number	UA @ lucian @ c:irua:91884			Serial	2881
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Author	Lebedev, O.I.; Verbeeck, J.; Van Tendeloo, G.; Dubourdieu, C.; Rosina, M.; Chaudouët, P.
Title	Structure and properties of artificial [(La_0.7Sr_0.3MnO₃)_m(SrTiO₃)_n]₁₅ superlattices on (001)SrTiO₃			Type	A1 Journal article
Year	2003	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	94	Issue	12	Pages	7646-7656
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Complex [(La0.7Sr0.3MnO3)(m)(SrTiO3)(n)] [(LSMO)(m)/(STO)(8)](15) superlattices with different layer thicknesses (m=5, 8, 12, 16, 32) have been prepared using pulsed liquid injection metalorganic chemical vapor deposition. Transmission electron microscopy and electron diffraction reveal a very clear and well-separated layer sequence. The remarkable microstructure, as well as the ferromagnetic transition temperature, depends on the LSMO layer thickness. Apart from a very clear layer sequence, electron microscopy shows evidence of a self-assembled nanostructure formation: SrMnO3 nanoinclusions and associated SrTiO3-SrMnO3 thin walls. A formation model and growth mechanism for the self-assembled structure is proposed, based on high resolution and energy filtered elemental imaging. (C) 2003 American Institute of Physics.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000186969900042	Publication Date	2003-12-04
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	22	Open Access
Notes				Approved	Most recent IF: 2.068; 2003 IF: 2.171
Call Number	UA @ lucian @ c:irua:54822			Serial	3292
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Author	Lebedev, O.I.; Hamet, J.F.; Van Tendeloo, G.; Beaumont, V.; Raveau, B.
Title	Structure and properties of the YBa₂Cu₃O_7-x/LaAlO₃ superlattices			Type	A1 Journal article
Year	2001	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	90	Issue	10	Pages	5261-5267
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000171918700061	Publication Date	2002-07-26
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	13	Open Access
Notes				Approved	Most recent IF: 2.068; 2001 IF: 2.128
Call Number	UA @ lucian @ c:irua:54821			Serial	3294
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Author	Rossell, M.D.; Lebedev, O.I.; Van Tendeloo, G.; Hayashi, N.; Terashima, T.; Takano, M.
Title	Structure of epitaxial Ca₂Fe₂O₅ films deposited on different perovskite-type substrates			Type	A1 Journal article
Year	2004	Publication	Journal of applied physics	Abbreviated Journal	J Appl Phys
Volume	95	Issue	9	Pages	5145-5152
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000220875400096	Publication Date	2004-04-14
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0021-8979;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.068	Times cited	16	Open Access
Notes				Approved	Most recent IF: 2.068; 2004 IF: 2.255
Call Number	UA @ lucian @ c:irua:54828			Serial	3310
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Author	Chen, L.; Kirilenko, D.; Stesmans, A.; Nguyen, X.S.; Binnemans, K.; Goderis, B.; Vanacken, J.; Lebedev, O.; Van Tendeloo, G.; Moshchalkov, V.V.
Title	Symmetry and electronic states of Mn²⁺ in ZnS nanowires with mixed hexagonal and cubic stacking			Type	A1 Journal article
Year	2010	Publication	Applied physics letters	Abbreviated Journal	Appl Phys Lett
Volume	97	Issue	4	Pages	041918,1-041918,3
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Electron spin resonance and electronic spectroscopy techniques were used to study the symmetry and electronic structure of Mn2+ dopants in solvothermally synthesized ZnS nanowires. The average diameter of ∼ 5 nm leads to the observable quantum confinement effects in the photoluminescence excitation spectra. The results clearly demonstrate the three symmetry locations of Mn2+ incorporation. Together with the inferred Mn2+ center densities, these data indicate a much higher efficiency of Mn2+ substitution in the nanowire sample with about two times larger diameter.
Address
Corporate Author				Thesis
Publisher	American Institute of Physics	Place of Publication	New York, N.Y.	Editor
Language		Wos	000281059200038	Publication Date	2010-08-02
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0003-6951;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.411	Times cited	5	Open Access
Notes	Methusalem			Approved	Most recent IF: 3.411; 2010 IF: 3.841
Call Number	UA @ lucian @ c:irua:84869			Serial	3403
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Author	Shen, Y.; Turner, S.; Yang, P.; Van Tendeloo, G.; Lebedev, O.I.; Wu, T.
Title	Epitaxy-enabled vapor-liquid-solid growth of tin-doped indium oxide nanowires with controlled orientations			Type	A1 Journal article
Year	2014	Publication	Nano letters	Abbreviated Journal	Nano Lett
Volume	14	Issue	8	Pages	4342-4351
Keywords	A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT)
Abstract	Controlling the morphology of nanowires in bottom-up synthesis and assembling them on planar substrates is of tremendous importance for device applications in electronics, photonics, sensing and energy conversion. To date, however, there remain challenges in reliably achieving these goals of orientation-controlled nanowire synthesis and assembly. Here we report that growth of planar, vertical and randomly oriented tin-doped indium oxide (ITO) nanowires can be realized on yttria-stabilized zirconia (YSZ) substrates via the epitaxy-assisted vaporliquidsolid (VLS) mechanism, by simply regulating the growth conditions, in particular the growth temperature. This robust control on nanowire orientation is facilitated by the small lattice mismatch of 1.6% between ITO and YSZ. Further control of the orientation, symmetry and shape of the nanowires can be achieved by using YSZ substrates with (110) and (111), in addition to (100) surfaces. Based on these insights, we succeed in growing regular arrays of planar ITO nanowires from patterned catalyst nanoparticles. Overall, our discovery of unprecedented orientation control in ITO nanowires advances the general VLS synthesis, providing a robust epitaxy-based approach toward rational synthesis of nanowires.
Address
Corporate Author				Thesis
Publisher		Place of Publication	Washington	Editor
Language		Wos	000340446200022	Publication Date	2014-06-27
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	1530-6984;1530-6992;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	12.712	Times cited	33	Open Access
Notes	European Union Seventh Framework Programme under Grant 312483 – ESTEEM; FWOl; esteem2_ta			Approved	Most recent IF: 12.712; 2014 IF: 13.592
Call Number	UA @ lucian @ c:irua:118622			Serial	1075
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Author	Volkova, N.E.; Lebedev, O.I.; Gavrilova, L.Y.; Turner, S.; Gauquelin, N.; Seikh, M.M.; Caignaert, V.; Cherepanov, V.A.; Raveau, B.; Van Tendeloo, G.
Title	Nanoscale ordering in oxygen deficient quintuple perovskite Sm_2-\epsilonBa_3+\epsilonFe₅O_15-\delta : implication for magnetism and oxygen stoichiometry			Type	A1 Journal article
Year	2014	Publication	Chemistry of materials	Abbreviated Journal	Chem Mater
Volume	26	Issue	21	Pages	6303-6310
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	The investigation of the system SmBaFe-O in air has allowed an oxygen deficient perovskite Sm2-epsilon Ba3+epsilon Fe5O15-delta (delta = 0.75, epsilon = 0.125) to be synthesized. In contrast to the XRPD pattern which gives a cubic symmetry (a(p) = 3.934 angstrom), the combined HREM/EELS study shows that this phase is nanoscale ordered with a quintuple tetragonal cell, a(p) X a(p) X 5(ap). The nanodomains exhibit a unique stacking sequence of the A-site cationic layers along the crystallographic c-axis, namely SmBaBa/SmBa/SmBaSm, and are chemically twinned in the three crystallographic directions. The nanoscale ordering of this perovskite explains its peculiar magnetic properties on the basis of antiferromagnetic interactions with spin blockade at the boundary between the nanodomains. The variation of electrical conductivity and oxygen content of this oxide versus temperature suggest potential SOFC applications. They may be related to the particular distribution of oxygen vacancies in the lattice and to the 3d(5)(L) under bar configuration of iron.
Address
Corporate Author				Thesis
Publisher		Place of Publication		Editor
Language		Wos	000344905600029	Publication Date	2014-10-07
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0897-4756;1520-5002;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	9.466	Times cited	16	Open Access
Notes	The UrFU authors were financially supported by the Ministry of Education and Science of Russian Federation (project N 4.1039.2014/K) and by UrFU under the Framework Program of development of UrFU through the «Young scientists UrFU» competition. The CRISMAT authors gratefully acknowledge the EC, the CNRS and the French Minister of Education and Research for financial support through their Research, Strategic and Scholarship programs. This work was supported by funding from the European Research Council under the Seventh Framework Program (FP7), ERC grant N°246791 – COUNTATOMS. S.T. gratefully acknowledges the fund for scientific research Flanders for a post-doctoral fellowship and for financial support under contract number G004413N. N.G. acknowledges funding from the European Research Council under the 7th Framework Program (FP7), ERC starting grant number 278510 – VORTEX; ECASJO_;			Approved	Most recent IF: 9.466; 2014 IF: 8.354
Call Number	UA @ lucian @ c:irua:122137			Serial	2269
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Author	Lebedev, O.I.; Verbeeck, J.; Van Tendeloo, G.; Amelinckx, S.; Ravazi, F.S.; Habermeier, H.-U.
Title	Structure and microstructure of La_1-xSr_xMnO₃ (x=0.16) films grown on a SrTiO₃(110) substrate			Type	A1 Journal article
Year	2001	Publication	Philosophical magazine: A: physics of condensed matter: defects and mechanical properties	Abbreviated Journal	Philos Mag A
Volume	81	Issue	12	Pages	2865-2884
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract
Address
Corporate Author				Thesis
Publisher		Place of Publication	London	Editor
Language		Wos	000172348000008	Publication Date	2007-07-08
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0141-8610;1460-6992;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	2.136	Times cited	12	Open Access
Notes				Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:57132			Serial	3290
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Author	Verbeeck, J.; Lebedev, O.I.; Van Tendeloo, G.; Mercey, B.
Title	SrTiO₃(100)/(LaMnO₃)_m(SrMnO₃)_n layered heterostructures: a combined EELS and TEM study			Type	A1 Journal article
Year	2002	Publication	Physical review : B : condensed matter and materials physics	Abbreviated Journal	Phys Rev B
Volume	66	Issue	18	Pages	184426
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Epitaxially grown heterostructures consisting of alternating layers of LaMnO(3) (LMO, 9 or 15 unit cells) and SrMnO(3) (SMO, 4 or 6 unit cells) on a SrTiO(3)(100) (STO(100)) substrate have been studied by a combination of high resolution transmission electron microscopy (HRTEM), electron diffraction, quantitative electron energy loss spectroscopy (EELS) with model fitting, energy filtered TEM (EFTEM) and imaging spectroscopy on an atomic scale. The combination of these techniques is necessary for the structural, chemical, and electronic characterization of these heterostructures. A model is proposed containing chemically and structurally sharp interfaces. The SrMnO(3) layers are stabilized in a Pm3m structure between two LMO layers. Tensile stress causes oxygen deficiency in the SMO layers increasing the number of 3d electrons on the Mn sites to resemble the Mn(3+) sites in LMO. The energy loss near edge structure (ELNES) of O and Mn is compared for both LMO and SMO layers and shows that the Mn-O bonds have a partially covalent character. The absence of a strong valency effect in the Mn ELNES is due to the oxygen vacancies in SMO.
Address
Corporate Author				Thesis
Publisher		Place of Publication	Lancaster, Pa	Editor
Language		Wos	000179633100062	Publication Date	2002-11-27
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	0163-1829;1095-3795;	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	3.836	Times cited	32	Open Access
Notes				Approved	Most recent IF: 3.836; 2002 IF: NA
Call Number	UA @ lucian @ c:irua:54741			Serial	3563
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Author	Maccato, C.; Simon, Q.; Carraro, G.; Barreca, D.; Gasparotto, A.; Lebedev, O.I.; Turner, S.; Van Tendeloo, G.
Title	Zinc and copper oxides functionalized with metal nanoparticles : an insight into their nano-organization			Type	A1 Journal article
Year	2012	Publication	Journal of advanced microscopy research	Abbreviated Journal
Volume	7	Issue	2	Pages	84-90
Keywords	A1 Journal article; Electron microscopy for materials research (EMAT)
Abstract	Ag/ZnO and Au/CuxO (x = 1, 2) nanocomposites supported on Si(100) and polycrystalline Al2O3 were synthesised by hybrid approaches, combining chemical vapor deposition (either thermal or plasma-assisted) of host oxide matrices and subsequent radio frequency-sputtering of guest metal particles. The influence of the adopted synthetic parameters on the nanocomposite morphological and compositional features was investigated by field emission-scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. Results confirm the synthesis of ZnO and CuxO nanoarchitectures, characterized by a tailored morphology and an intimate metal/oxide contact. A careful control of the processing conditions enabled a fine tuning of the mutual constituent distribution, opening thus attractive perspectives for the engineering of advanced nanomaterials.
Address
Corporate Author				Thesis
Publisher		Place of Publication		Editor
Language		Wos		Publication Date	2012-12-04
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	2156-7573;2156-7581;	ISBN		Additional Links	UA library record
Impact Factor		Times cited		Open Access
Notes	Esteem			Approved	Most recent IF: NA
Call Number	UA @ lucian @ c:irua:105298			Serial	3932
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Author	Bigiani, L.; Gasparotto, A.; Andreu, T.; Verbeeck, J.; Sada, C.; Modin, E.; Lebedev, O.I.; Morante, J.R.; Barreca, D.; Maccato, C.
Title	Au-manganese oxide nanostructures by a plasma-assisted process as electrocatalysts for oxygen evolution : a chemico-physical investigation			Type	A1 Journal article
Year	2020	Publication	Advanced sustainable systems	Abbreviated Journal
Volume		Issue		Pages	2000177-11
Keywords	A1 Journal article; Engineering sciences. Technology; Electron microscopy for materials research (EMAT)
Abstract	Earth-abundant and eco-friendly manganese oxides are promising platforms for the oxygen evolution reaction (OER) in water electrolysis. Herein, a versatile and potentially scalable route to gold-decorated manganese oxide-based OER electrocatalysts is reported. In particular, MnxOy(MnO2, Mn2O3) host matrices are grown on conductive glasses by plasma assisted-chemical vapor deposition (PA-CVD), and subsequently functionalized with gold nanoparticles (guest) as OER activators by radio frequency (RF)-sputtering. The final selective obtainment of MnO2- or Mn2O3-based systems is then enabled by annealing under oxidizing or inert atmosphere, respectively. A detailed material characterization evidences the formation of high-purity Mn(x)O(y)dendritic nanostructures with an open morphology and an efficient guest dispersion into the host matrices. The tailoring of Mn(x)O(y)phase composition and host-guest interactions has a remarkable influence on OER activity yielding, for the best performing Au/Mn(2)O(3)system, a current density of approximate to 5 mA cm(-2)at 1.65 V versus the reversible hydrogen electrode (RHE) and an overpotential close to 300 mV at 1 mA cm(-2). Such results, comparing favorably with literature data on manganese oxide-based materials, highlight the importance of compositional control, as well as of surface and interface engineering, to develop low-cost and efficient anode nanocatalysts for water splitting applications.
Address
Corporate Author				Thesis
Publisher		Place of Publication		Editor
Language		Wos	000572376000001	Publication Date	2020-09-25
Series Editor		Series Title		Abbreviated Series Title
Series Volume		Series Issue		Edition
ISSN	2366-7486	ISBN		Additional Links	UA library record; WoS full record; WoS citing articles
Impact Factor	7.1	Times cited	4	Open Access	Not_Open_Access
Notes	; Padova University (DOR 2017-2019 and P-DiSC #03BIRD2018-UNIPD OXYGENA projects), as well as the INSTM Consortium (INSTMPD004 – NETTUNO project) and AMGA Foundation (Mn4Energy project), are gratefully acknowledged for financial support. The Qu-Ant-EM microscope was partially funded by the Hercules fund from the Flemish Government. J.V. acknowledges funding from a GOA project “Solarpaint” from the University of Antwerp and from EU H2020 823717 ESTEEM3 project. The authors thank Dr. Daniele Valbusa, Dr. Gianluca Corr, Dr. Andrea Gallo, and Dr. Dileep Khrishnan for helpful experimental assistance. ; esteem3TA; esteem3reported			Approved	Most recent IF: 7.1; 2020 IF: NA
Call Number	UA @ admin @ c:irua:171937			Serial	6457
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