Records |
Author |
Van Grieken, R.; Torfs, K. |
Title |
Atmospheric aerosols and deposition near historic buildings: chemistry, sources, interrelationships and relevance |
Type |
P3 Proceeding |
Year |
1996 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:14662 |
Serial |
7515 |
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Author |
Van Grieken, R.; Jaenicke, R.; Koutsenogii, K.P.; Khodzher, T.V.; Kulipanov, G.N. |
Title |
Atmospheric aerosols in the Asian part of the former Soviet Union |
Type |
H1 Book chapter |
Year |
1999 |
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Abbreviated Journal |
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Pages |
197-206
T2 - Baikal as a world natural heritage si |
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H1 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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000184646600030 |
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UA library record; WoS full record |
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no |
Call Number |
UA @ admin @ c:irua:27597 |
Serial |
7517 |
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Author |
Van Grieken, R.; Shevah, Y. |
Title |
Atmospheric deposition and its impact on ecosystems, with particular reference to the Mid-East: proceedings of a symposium held in Tel-Aviv, Israel, on 5-6 June 2000, under the auspices of IUPAC |
Type |
ME3 Book as editor |
Year |
2002 |
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Abbreviated Journal |
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Pages |
170 p. |
Keywords |
ME3 Book as editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:40621 |
Serial |
7521 |
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Author |
Bencs, L.; Horemans, B.; Van Grieken, R.; et al. |
Title |
Atmospheric deposition fluxes to the Belgian marine waters originating from ship emissions : SHIPFLUX : final report |
Type |
Minutes and reports |
Year |
2012 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:107883 |
Serial |
7524 |
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Author |
Van Grieken, R.; de Bock, L.; Injuk, J.; van Malderen, H. |
Title |
Atmospheric deposition of heavy metals in the North Sea as studied by micro- and trace analysis |
Type |
H3 Book chapter |
Year |
1994 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
284-286
T2 - Environmental contamination / Varnava |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:9521 |
Serial |
7525 |
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Author |
Injuk, J.; Van Grieken, R. |
Title |
Atmospheric inputs of heavy metals into the North Sea |
Type |
P3 Proceeding |
Year |
1996 |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:14669 |
Serial |
7526 |
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Author |
Harrison, R.M.; Van Grieken, R.E. |
Title |
Atmospheric particles |
Type |
ME3 Book as editor |
Year |
1998 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
610 p. |
Keywords |
ME3 Book as editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:20971 |
Serial |
7528 |
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Author |
Kontozova-Deutsch, V.; Horemans, B.; Cardell, C.; Van Grieken, R. |
Title |
Atmospheric pollution at the Alhambra monument, Granada, Spain: a preventive conservation study |
Type |
P3 Proceeding |
Year |
2010 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:85522 |
Serial |
7530 |
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Author |
Van Dyck, P.; Van Grieken, R. |
Title |
Automated energy-dispersive X-ray fluorescence analysis for diverse environmental samples |
Type |
H3 Book chapter |
Year |
1982 |
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Pages |
315-324
T2 - Analytical techniques in environmenta |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117484 |
Serial |
7536 |
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Author |
Van Grieken, R.; Artaxo, P.; Xhoffer, C. |
Title |
Automated EPXMA of individual environmental particles |
Type |
P3 Proceeding |
Year |
1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:2860 |
Serial |
7537 |
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Author |
Annegarn, H.J.; Van Grieken, R.E.; Winchester, J.W.; Sellschop, J.P.F.; von Blottnitz, F. |
Title |
Background aerosol concentrations at the Namib-Atlantic interface |
Type |
P3 Proceeding |
Year |
1979 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117465 |
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7546 |
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Van Winckel, T.; De Clippeleir, H.; Mancell-Egala, A.; Rahman, A.; Wett, B.; Bott, C.; Sturm, B.; Vlaeminck, S.E.; Al-Omari, A.; Murthy, S. |
Title |
Balancing flocs and granules by external selectors to increase capacity in high-rate activated sludge systems |
Type |
P3 Proceeding |
Year |
2016 |
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6 p.
T2 - WEFTEC.16, 24 - 28 September 2016, New O |
Keywords |
P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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UA @ admin @ c:irua:151122 |
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7548 |
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Author |
Bottari, F. |
Title |
Bio(inspired) strategies for the electro-sensing of β-lactam antibiotics |
Type |
Doctoral thesis |
Year |
2019 |
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Abbreviated Journal |
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Issue |
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Pages |
205 p. |
Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
In the broad context of food and environmental safety, the development of selective and sensitive analytical tools for the detection of β-lactam antibiotics in milk down to their Maximum Residues Limits (MRL), is still an open challenge. To address this need, the design of new bio(mimetic) electrochemical sensors was investigated in the present thesis. These sensors are based on the intrinsic electrochemistry of β-lactam antibiotics, taking advantages of the characteristic electrochemical fingerprints of the core structures and redox active side chain groups. The electrochemistry of nafcillin (NAF) and the isoxazolyl penicillins (ISOXA) was investigated, identifying the peculiar electrochemical fingerprint of each antibiotic, proving that it is possible to use electrochemistry for the selective detection of these antimicrobial drugs. Once verified the applicability of a direct detection, different sensor configurations were tested mainly focusing on: – the selection and validation of aptamers to be used as bioreceptors in the development of β-lactam biosensors; – the design of biomimetic receptors, particularly molecularly imprinted polymers, and other synthetic electrode modifiers compatible with a direct detection strategy. The selection of novel aptamers was performed following both a traditional FluMag SELEX protocol and a novel variant based on graphene oxide (GO). First results with the modified GO-SELEX are promising but more work still needs to be done to validate this novel approach. The few aptamers for β-lactam antibiotics, already reported in literature by other groups, were poorly characterized up to now. For this reason, a multi-analytical characterization protocol for aptamer binding studies was optimized and validated by focusing on aptamer AMP17 against ampicillin. The protocol combines ITC, nESI-MS and 1H-NMR. Very striking was the fact that the aptamer sequence did not show any sign of specific binding for its target, even if it was used in many other studies in the past. This thesis now offers a validated protocol for testing the affinity and binding capabilities of aptamer sequences. In parallel, the functionalization of the electrode surface with polymer modifiers was studied. In particular we optimized a MIP electrochemical sensor based on 4-aminobenzoic acid for the direct electrochemical detection of CFQ. Another approach was tested based on the intrinsic affinity of NAF for an oPD electropolymerized film on the electrode surface. Both sensors were found to be sensitive and selective for the detection of CFQ and NAF at MRLs in buffer solutions. The proposed protocols are robust and promising for technological transfer. Lastly, the research activity was directed towards milk sample analysis following two parallel routes: the development of a pre-treatment protocol for raw milk, based on solvent addition (ACN or ISO), and the study of β-lactam antibiotics electrochemistry in undiluted raw milk with addition of KNO3 as supporting electrolyte. Both approaches gave encouraging results and the detection of NAF, CFQ and CFU in the micromolar range was achieved, with the second approach in undiluted raw milk. |
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no |
Call Number |
UA @ admin @ c:irua:164996 |
Serial |
7557 |
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Author |
Carvajal-Arroyo, J.M.; Vitor Akaboci, T.R.; Ruscalleda, M.; Colprim, J.; Courtens, E.; Vlaeminck, S.E. |
Title |
Biofilms for one-stage autotrophic nitrogen removal |
Type |
H3 Book chapter |
Year |
2016 |
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Pages |
205-222
T2 - Aquatic biofilms : ecology, water qua |
Keywords |
H3 Book chapter; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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978-1-910190-17-3 |
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Call Number |
UA @ admin @ c:irua:130466 |
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7559 |
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Author |
Gielis, J.; Caratelli, D.; Fougerolle, Y.; Ricci, P.E.; Gerats, T. |
Title |
A biogeometrical model for corolla fusion in Asclepiad flowers |
Type |
H1 Book chapter |
Year |
2017 |
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2 |
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Pages |
83-105
T2 - Modeling in mathematics : proceedings |
Keywords |
H1 Book chapter; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
Abstract |
The molecular genetics of flower development have been studied extensively for more than two decades. Fusion of organs and the tendency to oligomery, important characteristics of flower evolution, so far have remained fairly elusive. We present a geometric model for shape and fusion in the corolla of Asclepiads. Examples demonstrate how fusion of petals creates stable centers, a prerequisite for the formation of complex pollination structures via congenital and postgenital fusion events, with the formation of de novo organs, specific to Asclepiads. The development of the corolla reduces to simple inequalities from the MATHS-BOX. The formation of stable centers and of bell and tubular shapes in flowers are immediate and logical consequences of the shape. Our model shows that any study on flowers, especially in evo-devo perspective should be performed within the wider framework of polymery and oligomery and of fusion and synorganization. |
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000442076400007 |
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2017-04-20 |
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978-94-6239-260-1; 978-94-6239-261-8; 2543-0300; 978-94-6239-260-1 |
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UA library record; WoS full record; WoS citing articles |
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UA @ admin @ c:irua:144551 |
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7561 |
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Author |
Xie, Y. |
Title |
Bioreactor strategies for sustainable nitrogen cycling based on mineralization/nitrification, partial nitritation/anammox or sulfur-based denitratation |
Type |
Doctoral thesis |
Year |
2021 |
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iv, 205 p. |
Keywords |
Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
Abstract |
In the biogeochemical flows on Earth, the reactive nitrogen (Nr) level has three times surpassed the safe boundary. The severe transgression of this boundary goes against sustainable planetary development. The modern food production process excessively relies on synthetic Nr fertilizers from the Haber– Bosch process. However, the massive loss of valuable nitrogen resources (i.e., 78-89%) from agriculture has been causing severe nitrogen cascade. Besides, the domestic wastewater in some local areas is discharged without proper treatment, making it a nonnegligible source of Nr pollution for local water bodies. Anthropogenic activities keep pumping out Nr pollution via point-source and non-point-source (NPS) emissions. Compared to the NPS emissions, point sources give visible and identified waste streams. It is vital to intervene the nitrogen cascade from point sources and facilitate humanity back to the safe Nr boundary. The collected and collectible Nr streams from food production, waste management, and recycling secondary raw materials can be used as waste-based fertilizers for agricultural cultivation. Besides the well-investigated recovery of inorganic Nr, organic Nr accounts for a massive Nr proportion on the Earth. Proper handling and treatment make these useful organic fertilizers for soil-based cultivation. However, these organic Nr fertilizers cannot directly apply to fertigation or hydroponic cultivation systems, and further biological conversion via nitrogen mineralization and nitrification to nitrate is essential. Besides the direct Nr cycling, the indirect Nr cycling ‘over the atmosphere’ should also be considered. In this way, the nitrogen cycle can be completed via converting the waste Nr back to nitrogen gas (i.e., Nr removal) and then synthesizing into Nr again. The municipal wastewater treatment plants receive a vast amount of low-strength Nr wastewater (mainly as ammonium) daily. Compared to the conventional nitrification/denitrification process, partial nitritation/anammox (PN/A) is considered a resource- and cost-effective technology for wastewater with a low COD/N ratio. Moreover, the novel autotrophic denitratation/anammox process could be a good Nr removal process for wastewater containing both ammonium and nitrate. This Ph.D. thesis aimed to develop Nr recovery, conversion, and removal bioreactor strategies for different types of waste streams and biomass. Nr recovery was investigated on high-strength Nr waste streams for fertigation or hydroponic applications in Chapters 2 and 3. On the other hand, Nr removal was studied on the medium- to low-strength Nr waste streams in Chapters 4 and 5. In Chapter 2, a novel mineralization and nitrification system was proposed, producing nutrient solutions from solid organic fertilizers for hydroponic systems. Batch tests showed that aerobic incubation at 35°C could realize the NO₃⁻-N production efficiency above 90% from a novel microbial fertilizer. Subsequently, in the stirred tank bioreactor test, NO₃⁻-N production efficiency stabilized in a range of 44-51% under the influent loading rate of 400 mg TN L⁻¹ d⁻¹ at a 5-day HRT. Using Ca(OH)₂ and Mg(OH)₂ as pH control reagents generated the nutrient solutions with different P, Ca, and Mg nutrient levels. After modeling the nutrient balancing process, the proportion of organic-sourced NO₃⁻-N in the Hoagland nutrient solution (HNS) of Ca(OH)₂ scenario was 92.7%, while only 37.4% in the Mg(OH)₂ scenario. Compared to commercial scenarios, the total costs of the organic-sourced HNS can be cost-competitive for hydroponic cultivation. In Chapter 3, the Nr recovery as nitrate (NO₃⁻-N) from diluted human urine (around 670 mg N L⁻¹) was explored in a trickling filter (TF) for the first time. A novel concept of in-situ integrating the TF system into hydroponic systems was proposed as meaningful progress towards sustainable agriculture. The difference between synthetic and real urine in nitrification efficiency was found to be negligible. The full nitrification of alkalinized real urine was realized in the pH-controlled TF by calcium hydroxide (Ca(OH)₂) at around pH 6. The TF could handle different urine collection batches and maintain relatively stable nitrification performance, with NO₃⁻-N production efficiency and rate of 88±3% and 136±4 mg N L⁻¹ d⁻¹, respectively. The optimal HLR to realize this nitrification performance was 2 m³ m⁻² h⁻¹, with energy consumption of 1.8 kWh electricity kg⁻¹ NO₃⁻-N production. Ca(OH)₂, as a cheap base, its triple advantages on urine alkalinization, full nitrification, and macronutrient supplementation were successfully demonstrated in our proposed concept. In Chapter 4, towards more sustainable wastewater treatment, the feasibility of one-stage partial nitritation/anammox (PN/A) was investigated in three parallel packed-bed trickling filters (TFs), with three types of carrier materials of different specific surface areas. Synthetic wastewater containing 100-250 mg NH₄⁺-N L⁻¹ was tested to mimic medium-strength household waste streams after carbon removal. Interestingly, the cheap carrier based on expanded clay achieved similar rates as commercially used plastic carrier materials. The top passive ventilation combined with an optimum hydraulic loading rate of 1.8 m³ m⁻² h⁻¹ could reach approximately 60% total nitrogen (TN) removal at a rate of 300 mg N L⁻¹ d⁻¹. A relatively low NO₃⁻-N production (13%) via PN/A was achieved in TFs. Most of the TN removal took place in the top compartment, where anammox activity was the highest. Energy consumption estimation (0.78 kWh electricity g⁻¹ N removed) suggested that the proposed process could be a suitable low-cost alternative for nitrogen removal. In Chapter 5, coupling sulfur-driven denitratation (SDN) with anammox was proposed to treat the wastewater containing both NO₃⁻-N and NH₄⁺-N, like the secondary effluents of mainstream PN/A processes. To explore the feasibility of sufficient and stable NO₂⁻-N accumulation via SDN in the long term, the effects of pH setpoints, residual NO₃⁻-N level, and biomass-specific NO₃⁻-N loading rate (BSNLR) were investigated. Alternating the pH setpoints between 7.0 and 8.5 could temporarily stimulate the NO₂⁻-N accumulation. Both the residual NO₃⁻-N and BSNLR showed highly positive correlations with the NO₂⁻-N accumulation efficiency. Under the control of pH 8.5, 1.0±0.8 mg NO₃⁻-N L⁻¹ and 150±42 mg NO₃⁻-N g⁻¹ VSS d⁻¹, SDN could produce 6.4±1.0 mg NO₂⁻-N L⁻¹ in the short term. Thiobacillus members may play a crucial role in managing the NO₂⁻-N accumulation, but the reduction of abundance and possible adaptation significantly impaired the efficacy of control strategies in the long run. Overall, novel technologies have been proposed to sustainably convert Nr in waste streams and biomass. The decision for Nr recovery versus removal and synthesis should be based on specific cases with the best environmental, economic, and human-health sustainability. In the future, the Nr management concepts should be further improved to make the nitrogen cycle more sustainable with higher resource use efficiency and less Nr emissions to the environment. Although the thesis is mainly focused on limited types of Nr waste streams, it pointed out the direction of sustainable Nr management and could facilitate the Nr back to the safe boundary in the long run. |
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UA @ admin @ c:irua:182099 |
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7563 |
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Van Eynde, E. |
Title |
Biotemplate silica-titania diatoms for gas phase photocatalysis |
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Doctoral thesis |
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2015 |
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184 p. |
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Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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978-90-5728-500-4 |
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UA @ admin @ c:irua:130503 |
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7564 |
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Gielis, J.; Caratelli, D.; Tavkelidze, I.; Fougerolle, Y.; Ricci, P.E.; Gerats, T. |
Title |
Bulky knots and links generated by cutting generalized Mobius-Listing bodies and applications in the natural sciences |
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H2 Book chapter |
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2013 |
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167-183
T2 - Math Art Summit : Koninklijke Vlaamse |
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H2 Book chapter; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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978-90-6569-119-4 |
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UA @ admin @ c:irua:110955 |
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7569 |
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Caen, J.; Schalm, O.; Janssens, K. |
Title |
Caractérisation historique et chimique des peintures en grisaille et du verre de vitrail dans l'oeuvre de J.-B. Capronnier (1814 – 1891) et J.-B. Bethune (1821 – 1894) |
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P3 Proceeding |
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2000 |
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P3 Proceeding; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:112007 |
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7576 |
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Godoi, R.H.M.; Bittencourt, A.V.L.; Hirata, P.Y.; Jafelicci Junior, M.; dos Reis Neto, J.M.; de Souza Sarkis, J.E.; Zara, L.F.; Van Grieken, R. |
Title |
Caracterização dos sistemas iônicos e particulado no reservatório |
Type |
H3 Book chapter |
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2011 |
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170-188
T2 - Eutrofização em reservatórios : gestã |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-85-7335-286-3 |
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UA @ admin @ c:irua:97170 |
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7577 |
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Sóti, V. |
Title |
Catalytic detoxification of lignocellulose hydrolyzate |
Type |
Doctoral thesis |
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2019 |
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XXVII, 243 p. |
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Doctoral thesis; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL); Biochemical Wastewater Valorization & Engineering (BioWaVE) |
Abstract |
The present PhD research investigated the possibility of catalytic detoxification of poplar wood based and steam exploded lignocellulosic hydrolyzate with different types of laccase enzymes, with special focus on ethanol and lactic acid products at industrially relevant parameters: high final product concentration, high initial substrate loading and integrated processes. The simultaneous saccharification and fermentation (SSF) process was taken as a base case and five types of laccases were thoroughly investigated on their utilization potential. Phenolic removal from the liquid xylose rich fraction (XRF) was higher with fungal laccases (65-90 %) compared to approximately 30 % removal with bacterial laccase. Moreover, the optimal pH of fungal laccases was close to pH 4.5, the optimum for cellulase, while the bacterial laccase worked at basic pH. Integrating laccase treatment and hydrolysis together showed that fungal laccases have negative impact on final sugar concentration, while bacterial laccase had a strong positive effect. Although bacterial laccase removed less phenol and although its optimal conditions are difficult to integrate with hydrolysis, its enhancing effect on cellulase activity makes it a better candidate for application. The presence of the solid fraction (SF) alters the phenolic concentration evolution significantly, thus screening experiments with the liquid fraction alone do not provide sufficient information for the combined process. Magnetic Cross-Linked Enzyme Aggregates (m-CLEAs) immobilization was assessed for bacterial laccase. m-CLEAs decreased phenolic concentration faster at every pH compared to free bacterial laccase; however, the removal was caused by adsorption rather than by enzyme activity. Although the size of m-CLEAs particles are in the µm range, around 90 % of the initial catalyst mass was recycled from a dense (15 % substrate loading) mixture via magnetic separation. The high recycling rate is promising; m-CLEAs immobilization method can have industrial utilization potential. Minimum sugar revenue (MSR) estimations show that currently hardwood based MSR is 70 % more expensive than corn grain based MSR. About 7-10 fold cellulase activity increase will be needed until MSR will be competitive with corn grain MSR. However, m-CLEAs cellulase can already be competitive if the corn prices are in the higher regime of last year’s prices. |
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UA @ admin @ c:irua:180125 |
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7584 |
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Sleegers, N. |
Title |
Cephalosporin antibiotics : electrochemical fingerprints and redox pathways investigated by mass spectral analysis |
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Doctoral thesis |
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2021 |
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208 p. |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Antwerp Electrochemical and Analytical Sciences Lab (A-Sense Lab) |
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Most recent IF: NA |
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UA @ admin @ c:irua:181014 |
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7588 |
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Kontozova, V.; Deutsch, F.; Godoi, R.; Godoi, A.F.; Joos, P.; Van Grieken, R. |
Title |
Characterisation of air pollutants in museum showcases |
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P3 Proceeding |
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2002 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:39524 |
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7592 |
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Van Grieken, R.; Gysels, K.; Hoornaert, S.; Joos, P.; Osán, J.; Szalóki, I.; Worobiec, A. |
Title |
Characterisation of individual aerosol particles for atmospheric and cultural heritage studies |
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H3 Book chapter |
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2000 |
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215-228
T2 - Environmental challenges / Belkin, Sh |
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H3 Book chapter; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:31694 |
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7597 |
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Bernard, P.C.; Van Grieken, R.E.; Eisma, D. |
Title |
Characterisation of individual suspension particles in the Ems estuary |
Type |
P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117514 |
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7599 |
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Zhang, L. |
Title |
Characteristic diagnosis of atmospheric discharge plasma and kinetics study of reactive species |
Type |
Doctoral thesis |
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2021 |
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XVIII, 148 p. |
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Doctoral thesis; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
Abstract |
Low-temperature plasma has received extensive attention due to its promising application prospects in the field of air pollutants degradation and energy conversion. To fulfill the need for particular applications, constructing stable plasma sources and investigating the interaction mechanisms between plasma and substances have been hot research topics. This thesis reports the diagnosis and improvement of plasma sources, diagnosis of the active species in plasma and a modeling study of chemical kinetics processes. The main research contents are as follows: In Chapter 3, a diffuse sine AC dielectric barrier discharge (DBD) is successfully obtained by optimizing the electrode structure. It is found that using double-layer dielectric plates can limit the discharge current intensity and significantly improve the discharge uniformity. The electrical characteristics and gas temperature with different operating time show that the discharge stability is also improved by using double-layer dielectric plates. In Chapter 4, nanosecond pulses are employed to generate diffuse DBD plasmas. Three main discharge stages are distinguished by ICCD images, i.e., the streamer breakdown from the needle tip to the plate electrode, the regime transition from streamer to diffuse plasma, and the propagation of surface discharge on the plate electrode surface. The chapter reveales that in nanosecond pulsed discharges the vibrational temperature of N2 increases with the discharge duration, while the rotational temperature mainly stays constant, which means electron energy is transferred into the vibrational levels, but gas heating is not obvious during the discharge pulse. In Chapter 5, both sine AC DBD and nanosecond pulsed DBD, studied in Chapter 2 and 3, are used for formaldehyde degradation. It is found that nanosecond pulsed DBD has more homogenous characteristics, better stability, and lower plasma gas temperature. Moreover, the energy consumption of nanosecond pulsed DBD is much lower than that of AC DBD. In Chapter 6, a 0D chemical kinetics model is developed to investigate the underlying plasma chemistry of methane dry reforming in a nanosecond pulsed discharge. An overview of the dominant reaction pathways of CO2 and CH4 conversion into the major products is given. Furthermore, most of the CO2 molecules are populated into vibrational states during the pulse. Hence, the vibrational states of CO2 play an important role in its dissociation process. In general, this PhD thesis contributes to a better insight in the mechanisms of sinusoidal AC DBD and nanosecond pulsed DBD plasmas and their applications, i.e., decomposition of formaldehyde and dry reforming of methane. |
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UA @ admin @ c:irua:183166 |
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7605 |
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Klaassen, L.; van der Snickt, G.; Legrand, S.; Higgitt, C.; Spring, M.; Vanmeert, F.; Rosi, F.; Brunetti, B.G.; Postec, M.; Janssens, K. |
Title |
Characterization and removal of a disfiguring oxalate crust on a large altarpiece by Hans Memling |
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H1 Book chapter |
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2019 |
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263-282
T2 - Metal soaps in art / Casadio, F. [edi |
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H1 Book chapter; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Antwerp Cultural Heritage Sciences (ARCHES) |
Abstract |
During the conservation treatment of Memling’s Christ with Singing and Music-making Angels, three panel paintings that are among the most monumental works in early Netherlandish art, the conservators came across insoluble surface layers containing calcium oxalates. A very thin and irregular layer of this type, hardly visible to the naked eye, was spread across the surface of all three panels. A much thicker layer forming an opaque and highly disfiguring crust that obscured the composition (Figs. 15.1 and 15.7) was locally present on areas of dark copper-containing paint, where multiple layers of old discolored coatings and accretions remained in place before the most recent cleaning. This article describes the application of a wide range of analytical techniques in order to fully understand the stratigraphy and composition of the crusts on the Memling paintings. FTIR spectroscopy in transmission and reflection mode, micro-ATR-FTIR imaging and macro-rFTIR scanning, SEM-EDX, mobile XRD, and SR-μXRD showed that the crusts contained two related Ca-based oxalate salts, whewellite and weddellite, and were separated from the original paint surface by varnish, indicating that they did not originate from degradation of the original paint but from a combination of microbial action and a thick accumulation of dirt. Supported by the results from these different analytical techniques, which when used together proved to be very effective in providing complementary information that addressed this specific conservation problem, and aided by the presence of the intermediate varnish layer(s), the conservators were able to remove most of the crusts with spectacular results. |
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2019-03-23 |
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978-3-319-90616-4 |
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UA @ admin @ c:irua:190778 |
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7609 |
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Oh, K.-Y.; Ro, C.-U.; Kim, H.K.; Van Grieken, R. |
Title |
Characterization of aerosol particles at Seoul, Korea, using ultrathin window EPMA |
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P3 Proceeding |
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2000 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:34106 |
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7612 |
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Oh, K.-Y.; Ro, C.-U.; Kim, H.K.; Kim, Y.-P.; Van Grieken, R. |
Title |
Characterization of aerosol particles collected at Kosan and 1100 Hill sites, Cheju Island, Korea, using ultrathin window EPMA |
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2000 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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no |
Call Number |
UA @ admin @ c:irua:34105 |
Serial |
7613 |
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Author |
Van Grieken, R.; Adams, F. |
Title |
Characterization of air particulate matter by X-ray, Raman and mass spectrometric techniques |
Type |
H3 Book chapter |
Year |
1986 |
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Issue |
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Pages |
57-89
T2 - Chemistry of the multiphase atmospheric |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:117503 |
Serial |
7614 |
Permanent link to this record |