Records |
Author |
Belmans, F.; Van Grieken, R.; Brügmann, L. |
Title |
Geochemical characterization of recent sediments in the Baltic Sea by bulk and electron microprobe analysis |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Marine chemistry |
Abbreviated Journal |
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Volume |
42 |
Issue |
|
Pages |
223-236 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1993LK11300006 |
Publication Date |
2003-08-08 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0304-4203; 1872-7581 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Times cited |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:6255 |
Serial |
7994 |
Permanent link to this record |
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Author |
Bernard, P.C.; Van Grieken, R.E.; Brügmann, L. |
Title |
Geochemistry of suspended matter from the baltic sea : 1 : results of individual particle characterization by automated electron microprobe |
Type |
A1 Journal article |
Year |
1989 |
Publication |
Marine chemistry |
Abbreviated Journal |
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Volume |
26 |
Issue |
2 |
Pages |
155-177 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Automated electron probe X-ray microanalysis was used to characterize some 15 000 individual suspension particles from 50 samples of suspended matter collected from different depths at 18 stations throughout the Baltic Sea and the transient area to the North Sea. For each particle, 14 minor and major elements were determined and size information data were obtained. To process this huge amount of results, multivariate analysis techniques were invoked: the particles were classified into specific types and the abundance variations of these groups were studied. It appeared that 80% of all investigated particles contained mostly silicon, and seemed to consist of quartz, and K-rich and Fe-rich aluminosilicates. The abundance of BaSO4 particles averaged 5% throughout the Baltic Sea, but amounted to up to 44% at some stations. The abundance of the Fe-rich particles varied significantly with location and depth, and averaged ∼ 4%. They were often found to be associated with significant amounts of P. Both of these particle types and the Mn-rich particles are thought to be mainly authigenic. Calcium carbonate particles are more abundant towards the North Sea (which seems to act as a source). Principal component analysis of the data revealed that most of the compositional variability can be explained by differences between deep and surface waters and by the influences of inflowing North Sea waters. Additional information about the types and sources of the suspended matter in the Baltic Sea was gained from the comparison and correlation of the single particle results with different fractions of the bulk concentrations of elements such as Al, Ca, Mn, Fe, Zn and Ba. |
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Wos |
A1989T986200005 |
Publication Date |
2003-08-08 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0304-4203; 1872-7581 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:116699 |
Serial |
7995 |
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Author |
Brügmann, L.; Bernard, P.C.; Van Grieken, R. |
Title |
Geochemistry of suspended matter from the Baltic Sea: 2: results of bulk trace metal analysis by AAS |
Type |
A1 Journal article |
Year |
1992 |
Publication |
Marine chemistry |
Abbreviated Journal |
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Volume |
38 |
Issue |
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Pages |
303-323 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1992JE94400008 |
Publication Date |
2003-08-08 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0304-4203; 1872-7581 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:2836 |
Serial |
7996 |
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Author |
Van Grieken, R.E.; Johansson, T.B.; Akselsson, K.R.; Winchester, J.W.; Nelson, J.W.; Chapman, K.R. |
Title |
Geophysical applicability of aerosol size distribution measurements using cascade impactors and proton-induced X-ray-emission |
Type |
A1 Journal article |
Year |
1976 |
Publication |
Atmospheric environment : an international journal |
Abbreviated Journal |
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Volume |
10 |
Issue |
8 |
Pages |
571-576 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Proton Induced X-ray Emission, (PIXE), is capable of high precision analysis for trace element components of aerosol particle size fractions sampled by cascade impactor. A statistical evaluation of data quality has been carried out in order to distinguish between analytical uncertainties in the PIXE procedure, errors caused by cascade impactor performance and by other factors in the sampling procedure, and geophysical causes of differences in composition and particle size distributions of the elements in aerosols. Replicate analyses and simultaneous samplings taken in north Florida and St. Louis have been used for the data evaluation. In addition to the analytical error the sampling procedure contributes an error of ~ 10% to be added quadratically. The resulting precision is sufficient to evaluate the data in geophysical terms. This is illustrated by means of sample sets taken simultaneously in an urban, forest and coastal environment of the same region. |
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Wos |
A1976BZ75500001 |
Publication Date |
2003-08-06 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1352-2310 |
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UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:113636 |
Serial |
8000 |
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Author |
Bekshaev, A.; de Hoog, J.; Van Grieken, R. |
Title |
Grazing-emission electron probe microanalysis of particles near the substrate edge |
Type |
A1 Journal article |
Year |
2001 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
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Volume |
56 |
Issue |
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Pages |
2385-2395 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000173118900005 |
Publication Date |
2002-07-25 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0584-8547; 1873-3565 |
ISBN |
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UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:36384 |
Serial |
8007 |
Permanent link to this record |
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Author |
Tsuji, K.; Wagatsuma, K.; Nullens, R.; Van Grieken, R.E. |
Title |
Grazing exit electron probe microanalysis for surface and particle analysis |
Type |
A1 Journal article |
Year |
1999 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
71 |
Issue |
13 |
Pages |
2497-2501 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000081265600046 |
Publication Date |
2002-07-26 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:24723 |
Serial |
8008 |
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Author |
Spolnik, Z.; Tsuji, K.; Van Grieken, R. |
Title |
Grazing-exit electron probe x-ray microanalysis of light elements in particles |
Type |
A1 Journal article |
Year |
2004 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
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Volume |
33 |
Issue |
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Pages |
16-20 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000188743100004 |
Publication Date |
2004-01-21 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0049-8246 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:43524 |
Serial |
8009 |
Permanent link to this record |
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Author |
Tsuji, K.; Spolnik, Z.; Wagatsuma, K.; Van Grieken, R.E.; Vis, R.D. |
Title |
Grazing-exit particle-induced X-ray emission analysis with extremely low background |
Type |
A1 Journal article |
Year |
1999 |
Publication |
Analytical chemistry |
Abbreviated Journal |
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Volume |
71 |
Issue |
22 |
Pages |
5033-5036 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Wos |
000083647100004 |
Publication Date |
2002-07-26 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:27588 |
Serial |
8010 |
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Author |
Godoi, R.H.M.; Goncalves, S.J., Jr.; Sayama, C.; Polezer, G.; Reis Neto, J.M.; Alfoldy, B.; Van Grieken, R.; Riedi, C.A.; Yamamoto, C.I.; Godoi, A.F.L.; Bencs, L. |
Title |
Health implications of atmospheric aerosols from asbestos-bearing road pavements traditionally used in Southern Brazil |
Type |
A1 Journal article |
Year |
2016 |
Publication |
Environmental Science and Pollution Research
T2 – 1st International Caparica Conference on Pollutant Toxic Ions and, Molecules (PTIM), 2015, Caparica, PORTUGAL |
Abbreviated Journal |
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Volume |
23 |
Issue |
24 |
Pages |
25180-25190 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Serpentine and amphibole asbestos occur naturally in certain geologic settings worldwide, most commonly in association with ultramafic rocks, along associated faults. Ultramafic rocks have been used in Pin County, Southern Brazil for decades for the purpose of road paving in rural and urban areas, but without the awareness of their adverse environmental and health impact. The aim of this study was the chemical characterization of aerosols re-suspended in two rural roads of Pin, paved with ultramafic rocks and to estimate the pulmonary deposition of asbestos aerosols. Bulk aerosol samples were analyzed by means of X-ray fluorescence spectrometry and X-ray diffraction analysis, in order to characterize elemental composition and crystallinity. Single-particle compositions of aerosols were analyzed by computer-controlled electron-probe microanalysis, indicating the presence of a few percentages of serpentine and amphibole. Given the chemical composition and size distribution of aerosol particles, the deposition efficiency of chrysotile, a sub-group of serpentine, in two principal segments of the human respiratory system was estimated using a lung deposition model. As an important finding, almost half of the inhaled particles were calculated to be deposited in the respiratory system. Asbestos depositions were significant (similar to 25 %) in the lower airways, even though the selected breathing conditions (rest situation, nose breathing) implied the lowest rate of respiratory deposition. Considering the fraction of inhalable suspended chrysotile near local roads, and the long-term exposure of humans to these aerosols, chrysotile may represent a hazard, regarding more frequent development of lung cancer in the population of the exposed region. |
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Wos |
000389301700060 |
Publication Date |
2016-09-28 |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0944-1344; 1614-7499 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:139232 |
Serial |
8018 |
Permanent link to this record |
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Author |
Čevik, U.; Koz, B.; Makarovska, Y. |
Title |
Heavy metal analysis around Iskenderun Bay in Turkey |
Type |
A1 Journal article |
Year |
2010 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
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Volume |
39 |
Issue |
3 |
Pages |
202-207 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The heavy metal analysis around Iskenderun Bay in Turkey was carried out using mosses, soils, mussels, and sediments. This region is one of the most industrial areas of Turkey, including iron-steel plants, beverage, liquefied petroleum gas (LPG) plants, and oil transfer docks. Energy dispersive X-ray fluorescence spectrometry (Epsilon 5, PANalytical, Almelo, The Netherlands) was used to analyze all samples. V, Cr, Mn, Fe, Ni, Cu, Zn, As, and Pb elements were observed in all samples studied. Although Ce was detected in some mosses and soils, Sn was detected only in some moss samples. Pb concentrations in the moss samples are higher than the soil, the mussel, and the sediment samples. This can be attributed to the mosses that absorb heavy metals such as Pb easily from the air. As the aim of this study was to analyze heavy metals, the evaluation of these elements with their potential hazards for ecology and humans is briefly discussed |
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Wos |
000277637400006 |
Publication Date |
2010-03-29 |
Series Editor |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0049-8246 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:82678 |
Serial |
8020 |
Permanent link to this record |
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Author |
Araújo, M.F.D.; Bernard, P.C.; Van Grieken, R.E. |
Title |
Heavy metal contamination in sediments from the Belgian coast and Scheldt estuary |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Marine pollution bulletin |
Abbreviated Journal |
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Volume |
19 |
Issue |
2 |
Pages |
269-273 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Sixty-two samples of total sediments and the separated clay/silt size fractions were analysed by energy-dispersive X-ray fluorescence spectrometry to evaluate the pollution level and the trends in samples collected along the Belgian coast over a period of 6 yr and at four stations located in the Scheldt estuary where two of these were sampled periodically for 4 yr. Three correction methods for grain size effects were applied, either to the bulk sediment samples or to the clay/silt size fractions, and the results were compared. Local variations on the concentrations in some of the elements determined were used to establish whether they result from an anthropogenic or natural origin. The level of pollution was assessed as a function of the location, sampling date, and depth. |
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Wos |
A1988P559400005 |
Publication Date |
2003-08-07 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0025-326x; 1879-3363 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
Call Number |
UA @ admin @ c:irua:116801 |
Serial |
8021 |
Permanent link to this record |
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Author |
Ramesh, R.; Subramanian, V.; Van Grieken, R. |
Title |
Heavy metal distribution in sediments of Krishna River basin, India |
Type |
A1 Journal article |
Year |
1990 |
Publication |
Environmental geology and water sciences |
Abbreviated Journal |
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Volume |
15 |
Issue |
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Pages |
207-216 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Place of Publication |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0177-5146 |
ISBN |
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Additional Links |
UA library record |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116933 |
Serial |
8022 |
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Author |
Biksham, G.; Subramanian, V.; Ramanathan, A.; Van Grieken, R. |
Title |
Heavy metal distribution in the Godavari river basin |
Type |
A1 Journal article |
Year |
1991 |
Publication |
Environmental geology and water sciences |
Abbreviated Journal |
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Volume |
17 |
Issue |
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Pages |
117-126 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Place of Publication |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0177-5146 |
ISBN |
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Additional Links |
UA library record |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:55571 |
Serial |
8023 |
Permanent link to this record |
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Author |
Subramanian, V.; Van Grieken, R.; Van 't dack, L. |
Title |
Heavy metals distribution in the sediments of Ganges and Brahmaputra rivers |
Type |
A1 Journal article |
Year |
1987 |
Publication |
Environmental geology |
Abbreviated Journal |
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Volume |
9 |
Issue |
2 |
Pages |
93-103 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Bed sediments were collected from the entire region of the Ganges basin and some parts of the Brahmaputra. In addition, selected stations were sampled for suspended sediments as well. The samples were analysed for a number of heavy metals (Fe, Mn, Ni, Cr, Cu, and Zn) by the thin-film energy dispersive X-ray fluorescence technique. There are pronounced temporal and spatial variations in the heavy metals distributions. Suspended sediments are 510 times richer than the bed sediments. None of the tributaries contribute significant heavy metal load, but around urban areas in Yamuna (tributary of Ganges), very high levels due to the distribution from the drainage network are observed. Compared to the Brahmaputra, the distribution and fractionation of heavy metals in the Ganges sediments are more erratic and highly variable. All the metals considered show high correlation among themselves. Given the high flux of suspended sediments from the Himalayan rivers (nearly 20% of the global flux), the worldwide budget for heavy metal transport may need to be suitably revised. |
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Wos |
A1987F245600004 |
Publication Date |
2006-07-30 |
Series Editor |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0943-0105 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:111507 |
Serial |
8024 |
Permanent link to this record |
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Author |
Facetti, J.; Dekov, V.M.; Van Grieken, R. |
Title |
Heavy metals in sediments from the Paraguay river: a preliminary study |
Type |
A1 Journal article |
Year |
1998 |
Publication |
The science of the total environment |
Abbreviated Journal |
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Volume |
209 |
Issue |
|
Pages |
79-86 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000072368900008 |
Publication Date |
2002-07-26 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0048-9697; 1879-1026 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:20961 |
Serial |
8025 |
Permanent link to this record |
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|
Author |
Jha, P.K.; Subramanian, V.; Sitasawad, R.; Van Grieken, R. |
Title |
Heavy metals in sediments of the Yamura River (a tributary of the Ganges), India |
Type |
A1 Journal article |
Year |
1990 |
Publication |
The science of the total environment |
Abbreviated Journal |
|
Volume |
95 |
Issue |
|
Pages |
7-27 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Yamuna River sediments are more enriched in metals than those of the Ganges and average Indian river sediments. Variation of metals in suspended, bed and core sediment are due to the varying proportions of grain size and mineral content. Iron, Mn and Pb show a preference for the oxide fraction, whereas Cu and Zn are predominant in organic and carbonate fractions of sediments. Of the total elemental content, 80% Mn, 78% Fe, 69% Pb, 67% Cu and 55% Zn are available in chemically mobile phases of the sediments. The high partition coefficient of metals with respect to Mn suggests similar chemical mobility and preferences for solid phases. River sediments in the vicinity of Delhi show an increase in sorption of metals downstream, consequently metals are retained in sediments. The high correlation coefficient and significant regression relation among the metals indicate their similar behaviour during transport. At Allahabad, the contribution of the Yamuna to the Ganges is 3200 t Pb year−1, 12 100 t Zn year−1 and 8500 t Cu year−1 in particulate form. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
A1990DP94300002 |
Publication Date |
2003-09-12 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0048-9697; 1879-1026 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116655 |
Serial |
8026 |
Permanent link to this record |
|
|
|
Author |
Subramanian, V.; Jha, P.K.; Van Grieken, R. |
Title |
Heavy metals in the Ganges estuary |
Type |
A1 Journal article |
Year |
1988 |
Publication |
Marine pollution bulletin |
Abbreviated Journal |
|
Volume |
19 |
Issue |
2 |
Pages |
290-293 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
A1988P559400010 |
Publication Date |
2003-08-07 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0025-326x; 1879-3363 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116803 |
Serial |
8027 |
Permanent link to this record |
|
|
|
Author |
Török, S.; Van Dyck, P.; Van Grieken, R. |
Title |
Heterogeneity effects in direct X-ray fluorescence analysis of hair |
Type |
A1 Journal article |
Year |
1984 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
13 |
Issue |
1 |
Pages |
27-32 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The methodology of direct hair analysis by energy-dispersive x-ray fluorescence was studied. The effect on the XRF result of having a non-homogeneous radial distribution of the analyte in a single hair strand and the macroscopic effects in a bundle of hairs were calculated to evaluate possible systematic errors. The detection limits were mapped as a function of the target thickness and surface fraction. It appeared that a 10 mg cm−2 sample thickness, i. e. a target with about four layers of hair strands, is recommended. The standard deviation of this simple direct analytical method is 619% for some important elements. Discrepancies with neutron activation analysis had a mean value of around 15%. About twelve elements can be determined simultaneously on a routine basis. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
A1984SB70200004 |
Publication Date |
2005-05-28 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0049-8246 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116485 |
Serial |
8029 |
Permanent link to this record |
|
|
|
Author |
Török, S.; Braun, T.; Van Dyck, P.; Van Grieken, R. |
Title |
Heterogeneity effects in direct XRF analysis of traces of heavy metals preconcentrated on polyurethane foam sorbents |
Type |
A1 Journal article |
Year |
1986 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
15 |
Issue |
1 |
Pages |
7-11 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Trace amounts of heavy metals were preconcentrated on discs of polyurethane (PU) foam loaded with ammonium diethyldithiocarbamate (DDTC), to increase the sensitivity of XRF. Since the diameter of the cavities in the open-cell PU foams reaches 30300 μm, considerable heterogeneity effects might occur, which could reduce the accuracy of the method. The possible systematic error introduced by considering the sample to be homogeneous is calculated using the Berry et al. model. The calculations show that the underestimation of the absorption correction factor when considering the sample as being homogeneous is less than 2% for high-Z elements when the sample thickness is at least 2 mm. The detection limits are also around the minima for this thickness. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
A1986AYN6000002 |
Publication Date |
2005-05-28 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0049-8246 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116488 |
Serial |
8030 |
Permanent link to this record |
|
|
|
Author |
Marguí, E.; Padilla, R.; Hidalgo, M.; Queralt, I.; Van Grieken, R. |
Title |
High-energy polarized-beam EDXRF for trace metal analysis of vegetation samples in environmental studies |
Type |
A1 Journal article |
Year |
2006 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
35 |
Issue |
3 |
Pages |
169-177 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000237818300005 |
Publication Date |
2006-03-23 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0049-8246 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:57751 |
Serial |
8031 |
Permanent link to this record |
|
|
|
Author |
Marguí, E.; Fontàs, C.; van Meel, K.; Van Grieken, R.; Queralt, I.; Hidalgo, M. |
Title |
High-energy polarized-beam energy-dispersive X-ray fluorescence analysis combined with activated thin layers for cadmium determination at trace levels in complex environmental liquid samples |
Type |
A1 Journal article |
Year |
2008 |
Publication |
Analytical chemistry |
Abbreviated Journal |
|
Volume |
80 |
Issue |
7 |
Pages |
2357-2364 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000254593500015 |
Publication Date |
2008-03-08 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0003-2700; 5206-882x |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:68425 |
Serial |
8032 |
Permanent link to this record |
|
|
|
Author |
Jain, R.; Rather, J.A.; Dwivedi, A.; Vikas |
Title |
Highly sensitive and selective voltammetric sensor fullerene modified glassy carbon electrode for determination of cefitizoxime in solubilized system |
Type |
A1 Journal article |
Year |
2010 |
Publication |
Electroanalysis |
Abbreviated Journal |
|
Volume |
22 |
Issue |
21 |
Pages |
2600-2606 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The usefulness of fullerene modified glassy carbon electrode in mediating the reduction of cefitizoxime in solubilized system has been demonstrated. Due to the unique structure and extraordinary properties, fullerene shows higher catalytic efficiency towards cefitizoxime reduction. The kinetic parameters, electron transfer coefficient (α) and rate constant (K0) across the modified electrode are 0.37 and 0.1081/s respectively. The proposed square-wave voltammetric method is linear over the concentration range 1.210.3 µg/mL. The limit of detection (LOD) is found 0.27 ng/mL. High sensitivity and selectivity together with low detection limit of the electrode response make it suitable for the determination of cefitizoxime. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000284052900015 |
Publication Date |
2010-10-04 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1040-0397 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:98690 |
Serial |
8042 |
Permanent link to this record |
|
|
|
Author |
Akbulut, S.; Van Grieken, R.; Kilic, M.A.; Čevik, U.; Rotondo, G.G. |
Title |
Identification of heavy metal origins related to chemical and morphological soil properties using several non-destructive X-ray analytical methods |
Type |
A1 Journal article |
Year |
2013 |
Publication |
Environmental monitoring and assessment |
Abbreviated Journal |
|
Volume |
185 |
Issue |
3 |
Pages |
2377-2394 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Soils are complex mixtures of organic, inorganic materials, and metal compounds from anthropogenic sources. In order to identify the pollution sources, their magnitude and development, several X-ray analytical methods were applied in this study. The concentrations of 16 elements were determined in all the soil samples using energy dispersive X-ray fluorescence spectrometry. Soils of unknown origin were observed by scanning electron microscopy equipped with a Si(Li) X-ray detector using Monte Carlo simulation approach. The mineralogical analyses were carried out using X-ray diffraction spectrometry. Due to the correlations between heavy metals and oxide compounds, the samples were analyzed also by electron probe microanalyzer (EPMA) in order to have information about their oxide contents. On the other hand, soil pH and salinity levels were identified owing to their influence between heavy metal and soil-surface chemistry. Moreover, the geoaccumulation index (I geo) enables the assessment of contamination by comparing current and pre-industrial concentrations. |
Address |
|
Corporate Author |
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Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000314033300029 |
Publication Date |
2012-06-21 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1420-2026; 1573-2967 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:106755 |
Serial |
8052 |
Permanent link to this record |
|
|
|
Author |
Bottari, F.; Moretto, L.M.; Ugo, P. |
Title |
Impedimetric sensing of the immuno-enzymatic reaction of gliadin with a collagen-modified electrode |
Type |
A1 Journal article |
Year |
2018 |
Publication |
Electrochemistry communications |
Abbreviated Journal |
|
Volume |
97 |
Issue |
|
Pages |
51-55 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
This paper presents a previously unexplored biosensing strategy for detecting gliadin which exploits the crosslinking of gliadin with collagen, catalyzed by transglutaminase at the interfacial electron transfer rate, on a modified electrode. The process is monitored by electrochemical impedance spectroscopy using a glassy carbon electrode coated with a collagen layer. To validate the specificity of the response as well as to eliminate possible interferences from other proteins, such as soy protein or casein, the captured gliadin is further reacted with a specific anti-gliadin antibody. Changes in charge transfer resistance, measured from the Nyquist plots, scale linearly with the gliadin concentration in the range 5-20 mg/L, a range suitable for testing the gliadin concentration in gluten-free food commodities. |
Address |
|
Corporate Author |
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Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000451326800011 |
Publication Date |
2018-10-10 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1388-2481; 1873-1902 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:156285 |
Serial |
8067 |
Permanent link to this record |
|
|
|
Author |
Schalm, O.; Cabal, A.; van Espen, P.; Laquière, N.; Storme, P. |
Title |
Improved radiographic methods for the investigation of paintings using laboratory and synchrotron X-ray sources |
Type |
A1 Journal article |
Year |
2011 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
|
Volume |
26 |
Issue |
5 |
Pages |
1068-1077 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
It is generally known that radiographic inspection of 1517th century paintings can easily be done with a polychromatic X-ray source using a voltage between 20 kV and 40 kV in combination with classic X-ray films. Unfortunately, the spatial structure of numerous 19th and early 20th century paintings cannot be visualized with conventional radiography due to several reasons such as the use of lead white grounds or low absorbing pigments. Radiographic images are blurred or worse, they do not contain the picture of the painting. During the last decades, many technological innovations have been introduced in the field of radiography but their possibilities in cultural heritage have not been explored in full detail. In our investigation we used phosphor imaging plates, energy dispersive detectors and CCD-cameras in combination with synchrotron radiation and conventional X-ray tubes in order to improve the quality of radiographic images. Several promising techniques that could improve the quality of radiographs of paintings were identified. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000289731900023 |
Publication Date |
2011-04-11 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0267-9477 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:89928 |
Serial |
8070 |
Permanent link to this record |
|
|
|
Author |
Wegrzynek, D.; Jambers, W.; Van Grieken, R.; Eisma, D. |
Title |
Individual particle analysis of Western Mediterranean sediment cores, Rhône suspended matter and Sahara aerosols: investigation of inputs to the sediments |
Type |
A1 Journal article |
Year |
1997 |
Publication |
Marine chemistry |
Abbreviated Journal |
|
Volume |
57 |
Issue |
|
Pages |
25-40 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
|
Publication Date |
|
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0304-4203; 1872-7581 |
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:18778 |
Serial |
8079 |
Permanent link to this record |
|
|
|
Author |
van Malderen, H.; Hoornaert, S.; Injuk, J.; Przybylowicz, W.J.; Pineda, C.A.; Prozesky, V.M.; Van Grieken, R. |
Title |
Individual particle characterization of Siberian aerosols by micro-PIXE and backscattering spectrometry |
Type |
A1 Journal article |
Year |
2001 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
30 |
Issue |
|
Pages |
320-329 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000171234700008 |
Publication Date |
2002-08-25 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0049-8246 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:36084 |
Serial |
8080 |
Permanent link to this record |
|
|
|
Author |
Camuffo, D.; Brimblecombe, P.; Van Grieken, R.; Busse, H.-J.; Sturaro, G.; Valentino, A.; Bernardi, A.; Blades, N.; Shooter, D.; de Bock, L.; Gysels, K.; Wieser, M.; Kim, O. |
Title |
Indoor air quality at the Correr Museum, Venice, Italy |
Type |
A1 Journal article |
Year |
1999 |
Publication |
The science of the total environment |
Abbreviated Journal |
|
Volume |
236 |
Issue |
|
Pages |
135-152 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000082983600010 |
Publication Date |
2002-07-25 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0048-9697; 1879-1026 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:27591 |
Serial |
8082 |
Permanent link to this record |
|
|
|
Author |
Godoi, R.H.M.; Carneiro, B.H.B.; Paralovo, S.L.; Campos, V.P.; Tavares, T.M.; Evangelista, H.; Van Grieken, R.; Godoi, A.F.L. |
Title |
Indoor air quality of a museum in a subtropical climate : the Oscar Niemeyer museum in Curitiba, Brazil |
Type |
A1 Journal article |
Year |
2013 |
Publication |
The science of the total environment |
Abbreviated Journal |
|
Volume |
452 |
Issue |
|
Pages |
314-320 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The assessment of damage to indoor cultural heritage, in particular by pollutants, is nowadays a major and growing concern for curators and conservators. Nevertheless, although many museums have been widely investigated in Europe, the effects of particulate matter and gaseous pollutants in museums under tropical and subtropical climates and with different economic realities are still unclear. An important portion of the world's cultural heritage is currently in tropical countries where both human and financial resources for preserving museum collections are limited. Hence, our aim is to assess the damage that can be caused to the artwork by pollution in hot and humid environments, where air quality and microclimatic condition differences can cause deterioration. As a case study, particulate matter as well as gases were collected at the Oscar Niemeyer Museum (MON) in Curitiba, Brazil, where large modern and contemporary works of art are displayed. NO2, SO2, O3, Acetic Acid, Formic Acids and BTEX, in the ambient air, were sampled by means of passive diffusive sampling and their concentrations were determined by IC or GCMS. The particulate matter was collected in bulk form and analyzed with the use of energy dispersive X-ray fluorescence and aethalometer. The chemical compositions of individual particles were quantitatively elucidated, including low-Z components like C, N and O, as well as higher-Z elements, using automated electron probe microanalysis. The gaseous and particulate matter levels were then compared with the concentrations obtained for the same pollutants in other museums, located in places with different climates, and with some reference values provided by international cultural heritage conservation centers. Results are interpreted separately and as a whole with the specific aim of identifying compounds that could contribute to the chemical reactions taking place on the surfaces of artifacts and which could potentially cause irreversible damage to the artworks. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000318530600034 |
Publication Date |
2013-03-23 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0048-9697; 1879-1026 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:106766 |
Serial |
8083 |
Permanent link to this record |
|
|
|
Author |
Gysels, K.; Delalieux, F.; Deutsch, F.; Van Grieken, R.; Camuffo, D.; Bernardi, A.; Sturaro, G.; Busse, H.-J.; Wieser, M. |
Title |
Indoor environment and conservation in the Royal Museum of Fine Arts, Antwerp, Belgium |
Type |
A1 Journal article |
Year |
2004 |
Publication |
Journal of cultural heritage |
Abbreviated Journal |
|
Volume |
5 |
Issue |
|
Pages |
221-230 |
Keywords ![sorted by Keywords field, descending order (down)](img/sort_desc.gif) |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000222196400010 |
Publication Date |
2004-05-29 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1296-2074 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:44970 |
Serial |
8084 |
Permanent link to this record |