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Author |
Vanmeert, F. |
Title |
Highly specific X-ray powder diffraction imaging at the macroscopic and microscopic scale |
Type |
Doctoral thesis |
Year |
2019 |
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Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
At or below the surface of painted works of art, valuable information is present that provides insights into an object’s past, such as the artist’s technique and the creative process that was followed or its conservation history, but also on its current state of preservation. Typically, a (very) limited set of small paint samples is taken which provide direct access to the individual paint layers. The chemical build-up of these layers can then be investigated in great detail using various microscopic analytical methods. However, in recent years a new trend towards both elemental and chemical imaging techniques has been set which are capable of visualizing the (often) heterogeneous composition of painted objects on a macroscopic scale. In this dissertation, various forms of specificity attainable with X‑ray powder diffraction (XRPD) imaging are explored: at the chemical, material and spatial level. This high specificity is illustrated throughout several applications stemming from the field of cultural heritage, both at the macroscopic (MA) and microscopic (µ) scale. As a first step, XRPD imaging was transformed to a transportable instrument that can be employed for the in situ investigation of artworks, e.g., inside museums and conservation workshops. With this unique instrument large‑scale maps (cm2 – dm2) reflecting the distribution of crystalline phases on/below the surface of flat painted artefacts can be visualized in a noninvasive manner. In this way compound-specific information was attained which can be related to original pigments or materials that have been added in a later stage and even degradation/secondary products that have formed spontaneously inside the paint layers. Additionally, with MA‑XRPD imaging it was possible to link quantitative information of pigment compositions and preferred orientation effects to the 2D compound‑specific distribution images, allowing for a further distinction between very similar artists’ materials. Furthermore, promising results for the limited depth-selectivity of this technique, obtained by exploiting the small shift in the position of the diffraction signals originating from the layered sequence of the pigments, are shown. Finally, a minute paint sample from Wheat stack under a cloudy sky by Van Gogh was investigated at a synchrotron radiation facility with tomographic µ‑XRPD imaging at the microscopic scale. The high chemical and spatial specificity of this imaging method was exploited to further elucidate the degradation pathway of the red lead pigment. |
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UA @ admin @ c:irua:159805 |
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8043 |
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Verbueken, A.; Verpooten, G.; Nouwen, E.; de Broe, M.; Van Grieken, R. |
Title |
Identification of inorganic and organic microliths in kidney sections by laser microprobe mass analysis (LAMMA) |
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P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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UA @ admin @ c:irua:117510 |
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8054 |
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Wegrzynek, D.; Eisma, D.; Van Grieken, R. |
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Individual particle analysis of sediments from the Gulf of Lions, suspensions from the Rhône river and dust of Saharan origin: preliminary results |
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P3 Proceeding |
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1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:2861 |
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8078 |
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Kontozova, V.; Godoi, R.H.M.; Spolnik, Z.; Worobiec, A.; Deutsch, F.; Van Grieken, R. |
Title |
Influence of gaseous and particulate air pollutants on stained glass windows: case study in the Basilica Saint Urbain in Troyes, France |
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P3 Proceeding |
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2005 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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UA @ admin @ c:irua:52359 |
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8092 |
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Otten, P.; Bruynseels; Van Grieken, R. |
Title |
LAMMA analysis of inorganic ammonium compounds in individual marine aerosol particles |
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P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117509 |
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8147 |
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Verbueken, A.; Paulus, G.; Van de Vyver, F.; Verpooten, G.; de Broe, M.; Van Grieken, R. |
Title |
LAMMA : calibration and application to nephrotoxicology studies |
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P3 Proceeding |
Year |
1983 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:117491 |
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8149 |
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Verbueken, A.H.; Paulus, G.J.; Van de Vyver, F.L.; Verpooten, G.A.; Visser, W.J.; de Broe, M.E.; Van Grieken, R.E. |
Title |
LAMMA in nephrotoxicity studies |
Type |
P3 Proceeding |
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1984 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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Call Number |
UA @ admin @ c:irua:117492 |
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8150 |
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Van Grieken, R.; Verbueken, A.; Bruynseels, F.; Vandeputte, D.; Goossenaerts, C.; Leysen, L.; Otten, P.; Wouters, L. |
Title |
Laser microprobe mass analysis : characteristics and applications |
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P3 Proceeding |
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1987 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117534 |
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8155 |
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Vandeputte, D.; Verbueken, A.; Jacob, W.; de Broe, M.; Van Grieken, R. |
Title |
Localisation of lead in tissues of poisoned rats by laser microprobe mass analysis (LAMMA) |
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P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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UA @ admin @ c:irua:117513 |
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8180 |
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Jacobs, W.; Floren, E.; Luyckx, D.; Bueken, P.; van Beeck, J.; Van Grieken, R. |
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Mapping of toxic vapours on board of tankers |
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P3 Proceeding |
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2011 |
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P3 Proceeding; Economics; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-1-905040-85-8 |
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UA @ admin @ c:irua:89790 |
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8202 |
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Saison, J.-Y.; Roekens, E.; Matheeussen, C.; Verlinden, L.; Desmedt, M.; Van Grieken, R.; Stranger, M. |
Title |
Measurement campaigns in the Euro-region |
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Minutes and reports |
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2005 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:56168 |
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8210 |
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Van Grieken, R.; Torfs, K. |
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Micro- and trace analysis of ambient particles, runoff water and crusts to evaluate environmental effects on monument |
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P3 Proceeding |
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1996 |
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Proceedings of the EC Workshop on Non-Destructive Testing to Evaluate Damage due to Environmental Effects on Historic Monuments |
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UA @ admin @ c:irua:14660 |
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8230 |
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Artaxo, P.; Van Grieken, R.; Watt, F.; Jaksic, M. |
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The microanalysis of individual atmospheric aerosol particles by electron, proton and laser microprobe |
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P3 Proceeding |
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1990 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117515 |
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8235 |
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Gysels, K.; Van Grieken, R. |
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Microanalysis of museum aerosols related to the conservation of works of art |
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P3 Proceeding |
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1999 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:24719 |
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8236 |
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Moropoulou, A.; Koui, M.; Theoulakis, P.; Bakolas, A.; Roumpopoulos, K.; Michailidis, P.; Van Grieken, R.; Cardell-Fernandez, C. |
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Microstructural criteria for the evaluation of stone susceptibility to sea-salt decay |
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P3 Proceeding |
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2002 |
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UA @ admin @ c:irua:36681 |
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8249 |
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Van Grieken, R.; Dewolfs, R. |
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Modern micro-analytical techniques for the elucidation of causes and mechanisms of material deterioration |
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1992 |
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UA @ admin @ c:irua:2858 |
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8269 |
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Smekens, A.; Vervoort, M.; Pauwels, J.; Berghmans, P.; van Espen, P.; Van Grieken, R. |
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Morphology and fractal dimension of soot and carbon black aggregates determined by image analysis |
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P3 Proceeding |
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1998 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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UA @ admin @ c:irua:22779 |
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8283 |
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Van Grieken, R. |
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Ocean-atmosphere interactions and oil pollution |
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P3 Proceeding |
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1974 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117457 |
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8325 |
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Brunekreef, B.; Janssen, N., A.H.; de Hartog, J., J.; Oldenwening, M.; Meliefste, K.; Hoek, G.; Lanki, T.; Timonen, K., L.; Vallius, M.; Pekkanen, J.; Van Grieken, R. |
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Personal, indoor, and outdoor exposures to PM2.5 and its components for groups of cardiovascular patients in Amsterdam and Helsinki |
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Minutes and reports |
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2005 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:51816 |
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8374 |
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Trincavelli, J.; Montoro, S.; Van Grieken, R.; van Espen, P. |
Title |
Prediction of Mα/Lα intensity ratios and the use in the spectra evaluation |
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P3 Proceeding |
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1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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no |
Call Number |
UA @ admin @ c:irua:2863 |
Serial |
8405 |
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Author |
Goossenaerts, C.; Verbueken, A.; Van Grieken, R. |
Title |
Preliminary LAMMA investigations on healthy and acid rain affected spruce needles |
Type |
P3 Proceeding |
Year |
1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117511 |
Serial |
8409 |
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Author |
Otten, P.; Bruynseels, F.; Van Grieken, R. |
Title |
Reaction of marine aerosols with HNO3 vapour studied by single particle analysis |
Type |
P3 Proceeding |
Year |
1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117508 |
Serial |
8455 |
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Author |
Bruynseels, F.; Van Grieken, R. |
Title |
Recombination reactions and geometry effects in laser microprobe mass analysis studied with 12C/13C bilayers |
Type |
P3 Proceeding |
Year |
1986 |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:117512 |
Serial |
8462 |
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Author |
Injuk, J.; Van Grieken, R. |
Title |
Reference matarials for microanalytical nuclear techniques |
Type |
P3 Proceeding |
Year |
1995 |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:55574 |
Serial |
8467 |
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Author |
Kontozova, V.; Krupińska, B.; Van Grieken, R.; Janssen, E.; Moris, H.; Aerts, D.; Watteeuw, L.; van Bos, M.; Peckstadt, A. |
Title |
Research for preventive conservation and optimal presentation of world heritage in Museum Plantin-Moretus, Antwerp |
Type |
P3 Proceeding |
Year |
2011 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-989-97522-0-7 |
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no |
Call Number |
UA @ admin @ c:irua:92095 |
Serial |
8473 |
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Author |
Chou, L.; Harlay, J.; Roevros, N.; Lannuzel, D.; Rebreanu, L.; van der Zee, C.; Lapernat, P.-E.; Daro, M.-H.; Aerts, K.; Godoi, R.; Van Grieken, R. |
Title |
Role of oceanic production and dissolution of calcium carbonate in climate change (CCCC): final report |
Type |
Minutes and reports |
Year |
2009 |
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Keywords |
Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:80696 |
Serial |
8486 |
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Author |
Delalieux, F.; Van Grieken, R.; Moropoulou, A. |
Title |
Salt weathering research: present state and future directions |
Type |
P3 Proceeding |
Year |
2003 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:42732 |
Serial |
8490 |
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Author |
van Malderen, H.; Van Grieken, R.; Khodzher, T.V.; Grachev, M.; Bufetov, N.S.; Koutsenogii, K.P. |
Title |
Single particle analysis of aerosols from Siberia |
Type |
P3 Proceeding |
Year |
1994 |
Publication |
Proceedings of the Russian-Ukrainian-Austrian-German Analytical Symposium |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
Call Number |
UA @ admin @ c:irua:9527 |
Serial |
8530 |
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Author |
Jambers, W.; Van Grieken, R. |
Title |
Single particle characterisation of inorganic North Sea suspensions |
Type |
P3 Proceeding |
Year |
1996 |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:14670 |
Serial |
8537 |
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Author |
Van Grieken, R.; Kontozova, V.; Godoi, R.H.M.; Spolnik, Z.; Worobiec, A.; Deutsch, F.; Bencs, L. |
Title |
Some studies of the effect of indoor and outdoor pollutants on cultural heritage items |
Type |
P3 Proceeding |
Year |
2005 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
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no |
Call Number |
UA @ admin @ c:irua:57632 |
Serial |
8556 |
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