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Author | Özen, M.; Mertens, M.; Snijkers, F.; Van Tendeloo, G.; Cool, P. | ||||
Title | Texturing of hydrothermally synthesized BaTiO3 in a strong magnetic field by slip casting | Type | A1 Journal article | ||
Year | 2016 | Publication | Ceramics international | Abbreviated Journal | Ceram Int |
Volume | 42 | Issue | 42 | Pages | 5382-5390 |
Keywords | A1 Journal article; Electron microscopy for materials research (EMAT); Laboratory of adsorption and catalysis (LADCA) | ||||
Abstract | Barium titanate powder was processed by slip casting in a rotating strong magnetic field of 9.4 T. The orientation factor of the sintered compact was analyzed by the X-ray diffraction technique and the microstructure (grain-size) was analyzed by scanning electron microscope. The hydrothermally prepared barium titanate was used as matrix material and the molten-salt synthesized barium titanate, with a larger particle-size, was used as template for the templated grain-growth process. Addition of large template particles was observed to increase the orientation factor of the sintered cast (5 vol% loading). Template particles acted as starting grains for the abnormal grain-growth process and the average grain-size was increased after sintering. Increasing the solid loading (15 vol%) resulted in a similar orientation factor with a decrease of the average grain size by more than half. However, addition of templates to the 15 vol% cast had a negative effect on the orientation factor. The impingement of growing particles was stated as the primary cause of particle misorientation resulting in a low orientation factor after sintering. Different heating conditions were tested and it was determined that a slow heating rate gave the highest orientation factor, the smallest average grain-size and the highest relative density. (C) 2015 Elsevier Ltd and Techna Group S.r.l. All rights reserved. | ||||
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Corporate Author | Thesis | ||||
Publisher | Place of Publication | Barking | Editor | ||
Language | Wos | 000369460500098 | Publication Date | 2015-12-23 | |
Series Editor | Series Title | Abbreviated Series Title | |||
Series Volume | Series Issue | Edition | |||
ISSN | 0272-8842 | ISBN | Additional Links | UA library record; WoS full record; WoS citing articles | |
Impact Factor | 2.986 | Times cited | 11 | Open Access | |
Notes | Approved | Most recent IF: 2.986 | |||
Call Number | UA @ lucian @ c:irua:132228 | Serial | 4260 | ||
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