| Records |
Author  |
Martínez Alanis, G.T. |
| Title |
Quantitative model-based high angle annular dark field scanning transmission electron microscopy |
Type |
Doctoral thesis |
| Year |
2015 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
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| Keywords |
Doctoral thesis; Electron microscopy for materials research (EMAT); Engineering Management (ENM) |
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Thesis |
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| Publisher |
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Place of Publication |
Antwerpen |
Editor |
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Wos |
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Publication Date |
0000-00-00 |
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Open Access |
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| Notes |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:122528 |
Serial |
2759 |
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| Author |
Martin, J.M.L.; François, J.P.; Gijbels, R.; Almlöf, J. |
| Title |
Structure and infrared spectroscopy of the C11 molecule |
Type |
MA3 Book as author |
| Year |
1991 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
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| Keywords |
MA3 Book as author; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
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| Publisher |
University of Minnesota |
Place of Publication |
Minneapolis, Minn. |
Editor |
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Publication Date |
0000-00-00 |
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Approved |
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| Call Number |
UA @ lucian @ c:irua:717 |
Serial |
3280 |
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| Author |
Martens, T.; Brok, W.J.M.; van Dijk, J.; Bogaerts, A. |
| Title |
Improving dielectric barrier discharge efficiency by optimizing voltage profiles |
Type |
P1 Proceeding |
| Year |
2009 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
95-98 |
| Keywords |
P1 Proceeding; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
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Place of Publication |
S.l. |
Editor |
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Wos |
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Publication Date |
0000-00-00 |
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Series Title |
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Edition |
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Additional Links |
UA library record; WoS full record; |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:85693 |
Serial |
1570 |
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| Author |
Marmorkos, I.K.; Schweigert, V.A.; Peeters, F.M.; Lok, J.G.S. |
| Title |
Binding of remote and spatial separated D- centers in double barrier resonant tunneling semiconductor devices |
Type |
P3 Proceeding |
| Year |
1996 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
2769-2772 |
| Keywords |
P3 Proceeding; Condensed Matter Theory (CMT) |
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Thesis |
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| Publisher |
World Scientific |
Place of Publication |
Singapore |
Editor |
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Wos |
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Publication Date |
0000-00-00 |
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Approved |
MATERIALS SCIENCE, MULTIDISCIPLINARY 135/271 Q2 # PHYSICS, APPLIED 70/145 Q2 # PHYSICS, CONDENSED MATTER 40/67 Q3 # |
| Call Number |
UA @ lucian @ c:irua:15809 |
Serial |
241 |
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| Author |
Markowicz, A.M.; Van Grieken, R.E. |
| Title |
Quantification in XRF analysis of intermediate-thickness samples |
Type |
H3 Book chapter |
| Year |
1992 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
339-358
T2 - Handbook of X-ray spectroscopy / Grie |
| Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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| Notes |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:2855 |
Serial |
8434 |
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| Author |
Markowicz, A.A.; Van Grieken, R.E. |
| Title |
Quantification in XRF analysis of intermediate-thickness samples |
Type |
H3 Book chapter |
| Year |
2002 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
407-431
T2 - Handbook of X-ray spectrometry / Grie |
| Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:36389 |
Serial |
8433 |
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| Author |
Markowicz, A.; Raeymaekers, B.; Van Grieken, R.; Adams, F. |
| Title |
Analytical electron microscopy of single particles |
Type |
H3 Book chapter |
| Year |
1986 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
173-197
T2 - Physical and chemical characterizatio |
| Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:117504 |
Serial |
7455 |
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| Author |
Marguí, E.; Van Grieken, R. |
| Title |
X-ray fluorescence spectrometry and related techniques : an introduction |
Type |
MA3 Book as author |
| Year |
2013 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
148 p. |
| Keywords |
MA3 Book as author; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISBN |
978-1-60650-391-1 |
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UA library record |
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Open Access |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:106179 |
Serial |
8768 |
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| Author |
Margu'i', E.; Queralt, I.; Van Grieken, R. |
| Title |
X-ray fluorescence analysis, sample preparation for |
Type |
H1 Book chapter |
| Year |
2009 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
1-20
T2 - Sncyclopedia of analytical chemistry / M |
| Keywords |
H1 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
| Abstract |
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Thesis |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
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Series Title |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISBN |
978-0-471-97670-7 |
Additional Links |
UA library record |
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Open Access |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:81641 |
Serial |
8765 |
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| Author |
Marchetti, A. |
| Title |
Novel insights and approaches for the analytical characterization of tangible cultural heritage objects |
Type |
Doctoral thesis |
| Year |
2021 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
333 p. |
| Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
| Abstract |
Cultural heritage represents the vehicle of our cultural identity, handed over from past to future generations throughout human history. As a repository of fundamental cultural and social values, the preservation of all forms of cultural heritage is a responsibility of every society and of humankind as a whole. When it comes to tangible cultural heritage, preservation of heritage translates into preservation of objects and, therefore, of the materials they are constituted of. This crucial task relies heavily on the application of scientific analytical methods to answer material and conservation-related questions. The fundamental contribution of this analytical approach led, in the past decades, to an ever-deepening understanding of the factors governing the degradation of cultural heritage. However, the extreme complexity of the heritage object-environment system results in a massive research field, which inevitably presents relevant open questions. This is where the present PhD work comes into play, attempting to fill knowledge gaps in literature by starting from specific case studies and un-answered research questions. The multianalytical research conducted during this PhD unraveled fundamental information on the properties governing the reactivity and long-term behavior of different classes of materials, from α-brass in an indoor environment to artists’ pigments in the presence of light, moisture and soluble particulate matter (PM). The paramount importance of the synthesis conditions on the composition, physical properties and reactivity of heritage materials was also demonstrated, in particular for stable lead pyroantimonate and unstable Geranium lake artists’ pigments. Moreover, the study and characterization of specific heritage objects, namely a series of 16th century reliquary altarpieces and the painting L’Arlesienne, by Vincent Van Gogh, allowed to obtain relevant insights into their composition and on potential risks for their conservation. The challenging nature of the samples considered, created the perfect opportunity to test an innovative spectroscopic technique, optical photo-thermal IR (O-PTIR), for the characterization of heritage materials. Striking results were obtained, highlighting a great potential for the application of this non-destructive sub-micron molecular spectroscopy to the analysis of cultural heritage. Finally, in the last section of this work, strategies to implement the continuous monitoring of PM levels in indoor environmental quality studies were also considered, with a particular focus on the identification of environmental hazards for the collections housed in specific conservation environments (War Heritage Institute in Brussels and St. Martin’s church in Aalst, BE). |
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Open Access |
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| Notes |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:177849 |
Serial |
8319 |
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| Author |
Manaigo, F. |
| Title |
Study of a gliding arc discharge for sustainable nitrogen fixation into NOx |
Type |
Doctoral thesis |
| Year |
2024 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
xxiv, 114 p. |
| Keywords |
Doctoral thesis; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
| Abstract |
With the growth of the world population, the agricultural sector is required to meet an increasing demand for nutrients and currently relies on industrially produced fertilizers. Among them, nitrogen-based fertilizers are the most common choice and require N2 to be converted into more reactive molecules in a process called “nitrogen fixation”. This is mainly performed through the Haber-Bosch process, which, is not ideal since it requires large-scale facilities to be economical and is associated with a high energy cost and high CO2 emissions, resulting in an environmental impact that is pushing for the study of greener alternatives. Among these, plasma-based nitrogen fixation into NOx is promising, and gliding arc plasma, specifically, proved to be suitable for nitrogen fixation. This thesis aims to study plasma-based nitrogen fixation focusing on an atmospheric pressure gliding arc plasma on three different levels. On a fundamental level, an approach dealing with laser-based excitation of separate rotational lines was successfully developed. This method can be implemented on atmospheric discharges that produce rather high NOx densities and, thus, can impose essential restrictions for the use of “classical” laser-induced fluorescence methods. The approach is then implemented, providing a discussion on the two-dimensional distributions of both the gas temperature and the NO ground state density. A clear correlation between these quantities is found and the effects of both the gas temperature and the plasma power on NO and NO2 concentrations are discussed, revealing how the NO oxidation is already significant in the plasma afterglow region and how the gas flow rate is a crucial parameter affecting the temperature gradients. >From a technological level, the conventional approach of introducing external resistors to stabilize the arc is challenged by studying both its performance and its stability replacing the external resistor with an inductor. We conclude that similar stabilization results can be obtained while significantly lowering the overall energy cost, which decreased from up to a maximum of 7.9 MJ/mol N to 3 MJ/mol N. Finally, we study whether a small-scale fertilizer production facility based on a gliding arc plasma can be a local competitive alternative. This is done by proposing a comparative model to understand how capital, operative expenditures and transport costs affect the production costs. The model highlights how, with the current best available technology, plasma-based nitrogen fixation, while being an interesting alternative for NOx synthesis, still requires a more efficient use of H2 for direct NH3 production. |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:205259 |
Serial |
9175 |
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| Author |
Magnus, W.; Carrillo-Nunez, H.; Sorée, B. |
| Title |
Transport in nanostructures |
Type |
H3 Book chapter |
| Year |
2011 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
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| Keywords |
H3 Book chapter; Condensed Matter Theory (CMT) |
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Thesis |
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| Publisher |
Pan Stanford |
Place of Publication |
S.l. |
Editor |
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Wos |
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Publication Date |
0000-00-00 |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISBN |
9789814364027 |
Additional Links |
UA library record |
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Times cited |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:93075 |
Serial |
3724 |
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| Author |
Magalhães Cunha, S. |
| Title |
Wave-packet dynamics and electronic transport properties in 2D materials |
Type |
Doctoral thesis |
| Year |
2022 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
219 p. |
| Keywords |
Doctoral thesis; Condensed Matter Theory (CMT) |
| Abstract |
This piece of work is twofold. First, the time evolution of wave-packets in 2D systems is analyzed by the Split-Operator technique in three different scenarios: in multilayer phosphorene, the transient oscillations in the time-dependent average of position and momentum were observed due to the zitterbewegung effect, and the wave packet propagates non-uniformly along the space deforming itself into an elliptical shape. These results were corroborated by the Green’s function formalism except for large values of the wave-vector and long times; in 2D semiconductor quantum wires (QWs) with anisotropic effective masses and different angle orientations with respect to the anisotropic axis. We have shown that the greater this angle, the smaller is the energy levels spacing implying in an increase of the accessible electronic states. Additionally, for non-null magnetic field, the quantum Hall edge states are significantly affected by the edge orientation. In the anisotropic case damped oscillations in the average values of velocity in both x and y directions where obtained. Theses oscillations are originated by the QW geometry but also from subwavepackets with different momentum orientations, whereas for isotropic QWs the wavepacket disperses without splitting; in the third scenario the split-operator technique was used to study the Landau levels, the wave packet trajectories and velocities of electrons in graphene at low-energy regime described by a modified Dirac equation where the momentum-operator is written in a generalized form as result of applying the position-dependent translation operator formalism (PDTO). In the second part of this thesis, the electronic and tunneling properties of α − T3 lattices were studied. Electrons in these lattices behave analogous to integer-spin Dirac Fermions. The presence of a third atomic site in the unit cell leads to a flat band in the energy spectrum, providing unique electronic and tunneling properties. The presence of a super-periodic potential and the inclusion of symmetry-breaking terms results in deviations of the atomic equivalence between the atomic sites affecting the Dirac points and the band-gap. Small deviations in the equivalence between the atomic sites and the number of barriers change the transmission properties in these lattices. Additionally, new tunneling regions are possible by adjusting the symmetry between the atomic sites and affect the omnidirectional total transmission called super-Klein tunneling observed in these lattices. We compare those results to the tunneling probabilities through regions where the energy spectrum changes from linear with a middle flat band to a hyperbolic dispersion. |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:189191 |
Serial |
7227 |
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| Author |
Maenhaut, W.; Selen, A.; van Espen, P.; Van Grieken, R.; Winchester, J.W. |
| Title |
Sulfur and heavy metals over the Atlantic Ocean : comparison with other marine data |
Type |
P3 Proceeding |
| Year |
1980 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:117480 |
Serial |
8618 |
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| Author |
Madani, M.; Bogaerts, A.; Vangeneugden, D. |
| Title |
Numerical modelling for a dielectric barrier discharge at atmospheric pressure in nitrogen |
Type |
P1 Proceeding |
| Year |
2005 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
53-56 |
| Keywords |
P1 Proceeding; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
| Abstract |
In this paper we used a one dimensional fluid model, for the simulations of a Dielectric Barrier Discharge at atmospheric pressure. From the current and voltage profiles and the density profiles, we notice that two different regimes can be obtained in a uniform DBD. Furthermore a two dimensional flud model was developed and we describe how the gasflow can be included in such a model. |
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S.l. |
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0000-00-00 |
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Series Issue |
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Edition |
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978-90-808669-2-8 |
ISBN |
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Additional Links |
UA library record; WoS full record; |
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Times cited |
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Open Access |
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| Notes |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:88728 |
Serial |
2399 |
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| Author |
Madani, M.; Bogaerts, A.; Gijbels, R.; Vangeneugden, D. |
| Title |
Modelling of a dielectric barrier glow discharge at atmospheric pressure in nitrogen |
Type |
P3 Proceeding |
| Year |
2002 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
130-133 |
| Keywords |
P3 Proceeding; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
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S.l. |
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0000-00-00 |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:82299 |
Serial |
2150 |
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| Author |
Madani, M.; Bogaerts, A.; Gijbels, R.; Vangeneugden, D. |
| Title |
Parametric study by means of numerical modelling for a dielectric barrier discharge at atmospheric pressure in nitrogen |
Type |
P3 Proceeding |
| Year |
2004 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
49-52 |
| Keywords |
P3 Proceeding; Plasma Lab for Applications in Sustainability and Medicine – Antwerp (PLASMANT) |
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S.l. |
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Wos |
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0000-00-00 |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:82304 |
Serial |
2554 |
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| Author |
Maciel de Menezes, R. |
| Title |
Skyrmionics and magnonics in chiral ferromagnets : from micromagnetic to atomistic control |
Type |
Doctoral thesis |
| Year |
2021 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
222 p. |
| Keywords |
Doctoral thesis; Condensed Matter Theory (CMT) |
| Abstract |
The precise control of skyrmionics and magnonics in magnetic materials is key to the development of novel spin-based technology and information transport applications. Essentially, the inherent stability of magnetic skyrmions (provided by their topological charge) together with their extremely small size (down to a few nanometers) and the ultralow threshold current necessary to move them in nanostructures are the main advantages of skyrmionics. Not least, magnonics offers lower power consumption compared to electronics and the excitation of high frequency (sub-100~nm wavelength) magnons makes it possible for the creation of nanometric devices for ultrafast information transport. Even though extensive research has been carried out in recent years, the precise manipulation of skyrmions and spin waves (magnons) in nanostructures is not fully mastered and needs to be addressed before making functional skyrmionic and magnonic devices. In this thesis, we reveal multiple alternatives for the manipulation of skyrmions and spin-waves in different materials, such as bulk chiral magnets, heterochiral structures, magnet-supperconductor hybrids and two-dimentional magnetic materials. We make use of a multiscale model to numerically simulate the magnetic states at each considered material, from micromagnetic to atomistic control. We first explore the different nucleation mechanisms, activation energy, and the time evolution of the skyrmion formation in chiral magnetic films, crucial for the realization of skyrmion-based devices. We show that the skyrmion lattice is formed from the conical phase progressively, most probably by the formation of chiral bobbres, followed by the cylindrical growth of individual skyrmions from the film surface. That reflects a rod-like (one-dimensional) nucleation of the skyrmion phase, with an activation barrier of several electronvolts per skyrmion for the case of MnSi (Manganese monosilicide). In addition, we reveal the interesting blinking (creation-annihilation) behavior of skyrmions close to the phase boundary between the conical and skyrmion phases, where we recall that such switching between topologically distinct states has been proposed as a bit operation for information storage. Next, we discuss the motion of ferromagnetic and antiferromagnetic skyrmions in heterochiral magnets. We report the characteristic deflection of ferromagnetic skyrmions when moving across a heterochiral interface, where the extent of such deflection is tuned by the applied spin-polarized current and the magnitude of Dzyaloshinskii-Moriya interaction. Following, we show that the antiferromagnetic skyrmion achieves much higher velocities than its ferromagnetic counterpart, yet experiences far stronger confinement in nanoengineered heterochiral tracks, which reinforces antiferromagnetic skyrmions as a favorable choice for skyrmion-based devices. After that, we study the interesting coupling of magnetic skyrmions and superconducting vortices in magnet-superconductor heterostructures. We perform numerical simulations, based on experimental observations, to demonstrate that the stray field of magnetic skyrmions can nucleate antivortices in an adjacent superconducting film, giving rise to a hybrid topological object, the skyrmion-vortex pair, which harbor promising features for skyrmionics and quantum computing applications. We then explore the manipulation of a single skyrmion-vortex pair when currents are applied into both superconducting and magnetic parts of the heterostructure, which is of importance for the facilitated skyrmion guidance in racetrack applications. Afterwards, we make use of the high tunability of magnetic parameters in two-dimensional magnetic materials to reveal the rich phase diagram of exotic magnetic configurations in magnetic monolayers with suppressed nearest-neighbour exchange, where we show that several unique cycloidal, checkerboard, row-wise and spin-ice states are stabilized by the competition between the second-nearest-neighbor exchange, Dzyaloshinskii-Moriya, and dipolar interactions. Additionally, we show the coexistence of ferromagnetic and antiferromagnetic spin-cycloids, as well as novel types of skyrmions and chiral domain walls. Finally, in the last part of the thesis, we present the spin wave properties in the two-dimensional magnetic materials CrBr$3$ and CrI$3$. Using spin-dynamics simulations parametrized from first principles, we reveal that the spin wave dispersion in such materials can be tuned in a broad range of frequencies by strain-engineering, and that a designed pattern of strain, as well as structural defects (halide vacancies) can be turned useful in the design of spin-wave guides. Lastly, we discuss the realization of magnonic crystals by moiré-periodic modulation of magnetic parameters in van der Waals heterostructures, where we show that the several nanometer small periodicities in such samples are ideal for the interference of terahertz spin waves. Recalling the wide range of possibilities for manipulating spin waves in such two-dimensional materials, we therefore suggest these systems as a front-runner for prospective terahertz magnonic applications. |
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Open Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:184244 |
Serial |
7019 |
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| Author |
Mabesoone, J.M.; Duarte, P.J.; Van Grieken, R.; Delgao, A.; Freire, E.M.P. |
| Title |
Geoquimica dos microclasticos da Bacio do Parnaiba |
Type |
H3 Book chapter |
| Year |
1985 |
Publication |
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Abbreviated Journal |
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| Volume |
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Issue |
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Pages |
30-31
T2 - Fanerozoico Nordestino : serie D |
| Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:117502 |
Serial |
8001 |
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| Author |
Lumbeeck, G. |
| Title |
Mechanisms of nano-plasticity in as-deposited and hydrided nanocrystalline Pd and Ni thin films |
Type |
Doctoral thesis |
| Year |
2019 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
130 p. |
| Keywords |
Doctoral thesis; Electron microscopy for materials research (EMAT) |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:164918 |
Serial |
6309 |
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| Author |
Lu, Y. |
| Title |
Electron energy-loss spectroscopy (EELS) characterization of diamond and related materials |
Type |
Doctoral thesis |
| Year |
2013 |
Publication |
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Abbreviated Journal |
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Pages |
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Doctoral thesis; Electron microscopy for materials research (EMAT) |
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Place of Publication |
Antwerpen |
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Wos |
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Publication Date |
0000-00-00 |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:111231 |
Serial |
932 |
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| Author |
Lu, Q. |
| Title |
Precipitation behavior and heat resistance properties of Al-Cu-Mg-Ag-(Si) alloy |
Type |
Doctoral thesis |
| Year |
2024 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
VIII, 212 p. |
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Doctoral thesis; Engineering sciences. Technology; Electron microscopy for materials research (EMAT) |
| Abstract |
With the rapid increase in the speed of new-generation aerospace vehicles, conventional heat-resistant aluminum alloys cannot meet the long-term service of the equipment. Therefore, the development of new high-strength heat-resistant aluminum alloys is of great strategic for the sustainable and high-quality development of industries. Al-Cu-Mg-Ag alloy is an age-hardenable heat-resistant aluminum alloy and has high strength and heat resistance. The addition of alloying elements such as Si and Sc to Al-Cu-Mg-Ag alloy introduces a competitive relationship among the σ-Al5Cu6Mg2, θ′-Al2Cu, and Ω phases. Therefore, a systematic investigation of precipitation behavior and heat resistance of Al-Cu-Mg-Ag-(Si) is essential for guiding the design of high-strength heat-resistant aluminum alloys. Combined characterization testing methods such as scanning electron microscopy, transmission electron microscopy, atom probe tomography, microhardness testing, and tensile testing with simulation calculation methods such as calculation of phase diagram, first-principles calculations, and Ab initio molecular dynamics, the effects of heat treatment processes and element content on the precipitation behavior, mechanical properties, and heat resistance of Al-Cu-Mg-Ag-(Si) alloys were systematically investigated. Furthermore, a multiple interface segregation structure was constructed at the θ′/Al interface, and a new Al-Cu-Mg-Ag-Si-Sc alloy with synergistically improved strength and heat resistance was developed. The main conclusions are as follows: (1) Based on the Kampmann-Wagner-Numerical theory, the relationship between the coarsening rate of the Ω phase and the aging process was analyzed, revealing for the first time that the critical size of Ω phase ( ) under thermal exposure temperature was the key factor determining the coarsening rate of Ω phase during long time thermal exposure heat treatment. After artificial ageing, when the size of Ω phase was smaller than the critical size , the dissolution of smaller Ω phase leaded to a rapid decrease in the number density of Ω phases, thereby reducing the heat resistance of the alloy. When the size of Ω phase was greater than or equal to the critical size , the coarsening rate of Ω phase was consistent, but a larger initial size would result in a larger final size after long-term thermal exposure. Therefore, the closer the size of Ω phase in the alloy is to the critical size under heat exposure temperature, the better the heat resistance of the alloy. (2) A concept of constructing a multiple interface segregation structure at the precipitate/matrix interface was proposed, and based on this concept, a multiple interface segregation structure containing the C/L-AlMgSiCu interfacial phase, newly discovered χ-AgMg interfacial phase, and Sc segregation layer was successfully constructed at the θ′/Al interface. The existence of the multiple interface segregation structure ensured that the designed Al-Cu-Mg-Ag-Si-Sc alloy maintains a yield strength of 400 MPa after thermal exposure at 200 C for 100 h, with a strength retention rate of 97%, creating a new record for the synergistic improvement of strength and heat resistance in aluminum alloys. In addition, combining transmission electron microscopy ex-situ/in-situ characterization with first-principles calculations, it is shown that the χ-AgMg interface phase will be destroyed due to the diffusion of the outer Ag layer during thermal exposure, and gradually dissolve into the matrix, but it can still delay the coarsening behavior of θ′-Al2Cu phase. (3) The criteria for determining whether Ω phase can precipitate are updated in Al-Cu-Mg-Ag-Si alloys with low Mg/Si ratio based on phase diagram thermodynamic calculations and multi-scale structural characterization. When W(Mg)/W(Si) > 1.4 and X(Ag)/X(Mgexcess) > 1, Ω phase can precipitate in Al-Cu-Mg-Ag-Si alloys, where X(Mgexcess) represents the atomic percentage of residual Mg elements after the formation of the AlMgSiCu quaternary precipitate phase C/L phase in the supersaturated solid solution, and the W(Mg) is the mass fraction of Mg in the supersaturated solid solution before artificial ageing. (4) The effects of alloy element content on precipitation behavior and heat resistance of Al-Cu-Mg-Ag-Si alloys were systematically analyzed. Critical conditions for the precipitation of σ-Al5Cu6Mg2 and Ω phase in Al-Cu-Mg-Ag-Si alloys are revealed. Based on calculation of phase diagram results, the conditions for precipitating σ-Al5Cu6Mg2 phase in the alloy are: ① W(Mg)/W(Si) > 1.8; ② W(Cu) > 2.7W(Mg) – 5W(Si). When W(Mg)/W(Si) < 1.8, the alloy is mainly precipitated with C/L/Q′-AlMgSiCu. When W(Cu) < 2.7W(Mg) – 5W(Si), the alloy will generate GPB zone. In addition, W(Ag)/W(Si) > 4 is the critical condition which the Ω phase can the main precipitates in Al-Cu-Mg-Ag-Si alloys. Furthermore, the correlation between precipitate types and heat resistance was summarized, showing that Al-Cu-Mg-Ag-(Si) alloys with Ω phase as the main strengthening phase are more suitable for the preparation of structures with short service time but high temperature, while Al-Cu-Mg-Ag-(Si) alloys with low Mg content and multiple segregation structures are more suitable for structures requiring long-term service at medium to high temperatures. This study, for the first time, combines calculation of phase diagram with multi-scale microstructure characterization, systematically unraveling the effects of element content on precipitation behavior, strength, and heat resistance of Al-Cu-Mg-Ag-(Si) alloys. In addition, a concept of constructing a multiple interface segregation structure at the precipitate/matrix interface was proposed to synergistically improve alloy strength and heat resistance. This work provides theoretical guidance for optimizing the composition and processing of Al-Cu-Mg-Ag-(Si) alloy and regulating the microstructure. Furthermore, it also offers new ideas and theoretical guidance for the development of novel high-strength heat-resistant alloys in other systems. |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:206180 |
Serial |
9167 |
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| Author |
Lou, W.-K. |
| Title |
The electrical properties of low low dimensional topological insulators |
Type |
Doctoral thesis |
| Year |
2012 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
186 p. |
| Keywords |
Doctoral thesis; Condensed Matter Theory (CMT) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:158894 |
Serial |
7858 |
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| Author |
Loomba, V.; Pourfallah, H.; Olsen, J.E.; Einarsrud, K.E. |
| Title |
Lab-scale physical model experiments to understand the effect of particle bed on tapping flow rates |
Type |
P1 Proceeding |
| Year |
2022 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
159-170 |
| Keywords |
P1 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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Publication Date |
2022-02-03 |
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978-3-030-92543-7; 2367-1181; 2367-1696; 978-3-030-92546-8; 978-3-030-92544-4 |
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UA library record |
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Open Access |
Not_Open_Access |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:186090 |
Serial |
7177 |
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| Author |
Lobato, I. |
| Title |
Accurate modeling of high angle electron scattering |
Type |
Doctoral thesis |
| Year |
2014 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
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Doctoral thesis; Electron microscopy for materials research (EMAT) |
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Place of Publication |
Antwerpen |
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0000-00-00 |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:120593 |
Serial |
50 |
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Liu, X.; Van Winckel, T.; Kjellerup, B.V.; Takacs, I.; Sturm, B.; Vlaeminck, S.E.; Al-Omari, A.; Murthy, S.; De Clippeleir, H. |
| Title |
Pinpointing bioflocculation limitations for enhanced carbon management in high-rate activated sludge |
Type |
P3 Proceeding |
| Year |
2017 |
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Pages |
6 p.
T2 - WEF Nutrient Symposium 2017, 12 - 14 Jun |
| Keywords |
P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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Approved |
no |
| Call Number |
UA @ admin @ c:irua:151118 |
Serial |
8384 |
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Lisiecki, I.; Turner, S.; Bals, S.; Pileni, M.P.; Van Tendeloo, G. |
| Title |
Enhanced stability against oxidation due to 2D self-organisation of hcp cobalt nanocrystals |
Type |
H1 Book chapter |
| Year |
2008 |
Publication |
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Issue |
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Pages |
273-274 |
| Keywords |
H1 Book chapter; Electron microscopy for materials research (EMAT) |
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Springer |
Place of Publication |
Berlin |
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0000-00-00 |
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ISBN |
978-3-540-85226-1 |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ lucian @ c:irua:87610 |
Serial |
1055 |
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Lindeboom, R.E.F.; Clauwaert, P.; Alloul, A.; Coessens, W.; Christiaens, M.; Vanoppen, M.; Rabaey, K.; Verliefde, A.R.D.; Vlaeminck, S.E. |
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Water and nutrient recovery from combined urine and grey water treatment in Space |
Type |
P3 Proceeding |
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2015 |
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Pages |
3 p.
T2 - IWA Resource Recovery Conference, 30 Aug |
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P3 Proceeding; Engineering sciences. Technology; Sustainable Energy, Air and Water Technology (DuEL) |
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no |
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UA @ admin @ c:irua:151143 |
Serial |
8747 |
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| Author |
Lind, O.C.; Salbu, B.; Janssens, K.; Simionovici, A.S. |
| Title |
Radioactive particle characterisation by means of synchrotron radiation-based X-ray micro beam techniques |
Type |
P3 Proceeding |
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2002 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:39941 |
Serial |
5797 |
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| Author |
Lind, O.C.; Claussen-Kjerre, L.; de Nolf, W.; Falkenberg, G.; Jaroszewicz, J.; Janssens, K.; Salbu, B. |
| Title |
Characterization of Yenisey River U-particles using a combination of μ-XRF, μ-XRD and U-LIII μ-XANES |
Type |
H3 Book chapter |
| Year |
2008 |
Publication |
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Issue |
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Pages |
1279-1280 |
| Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
| Call Number |
UA @ admin @ c:irua:74471 |
Serial |
5508 |
| Permanent link to this record |
