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Author |
de Nolf, W.; Janssens, K.; Rouchon, V.; Falkenberg, G. |
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Title |
Study of the degradation on historical documents induced by iron gall ink by means of scanning μ-XRF/μ-XRD |
Type |
H3 Book chapter |
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Year |
2007 |
Publication |
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H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:64597 |
Serial |
5850 |
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Author |
de Nolf, W.; Jaroszewicz, J.; Janssens, K.; Falkenberg, G. |
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Title |
2θ-resolution obtainable during – XRPD experiments at Beamline L |
Type |
H3 Book chapter |
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Year |
2008 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
1655-1656 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:74477 |
Serial |
5447 |
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Author |
de Nolf, W.; Jaroszewicz, J.; Terzano, R.; Lind, O.C.; Salbu, B.; Vekemans, B.; Janssens, K.; Falkenberg, G. |
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Title |
Possibilities and limitations of synchrotron X-ray powder diffraction with double crystal and double multilayer monochromators for microscopic speciation studies |
Type |
A1 Journal article |
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Year |
2009 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
Spectrochim Acta B |
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Volume |
64 |
Issue |
8 |
Pages |
775-781 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The performance of a combined microbeam X-ray fluorescence/X-ray powder diffraction (XRF/XRPD) measurement station at Hamburger Synchrotronstrahlungslabor (HASYLAB) Beamline L is discussed in comparison to that at European Synchrotron Radiation Facility (ESRF) ID18F/ID22. The angular resolution in the X-ray diffractograms is documented when different combinations of X-ray source, optics and X-ray diffraction detectors are employed. Typical angular resolution values in the range 0.30.5° are obtained at the bending magnet source when a pink beam form of excitation is employed. A similar setup at European Synchrotron Radiation Facility beamlines ID18F and ID22 allows to reach angular resolution values of 0.10.15°. In order to document the possibilities and limitations for speciation of metals in environmental materials by means of Hamburger Synchrotronstrahlungslabor Beamline L X-ray fluorescence/X-ray powder diffraction setup, two case studies are discussed, one involved in the identification of the crystal phases in which heavy metals such as chromium, iron, barium and lead are present in polluted soils of an industrial site (Val Basento, Italy) and another involved in the speciation of uranium in depleted uranium particles (Ceja Mountains, Kosovo). In the former case, the angular resolution is sufficient to allow identification of most crystalline phases present while in the latter case, it is necessary to dispose of an angular resolution of ca. 0.2° to distinguish between different forms of oxidized uranium. |
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Wos |
000269995300010 |
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2009-06-12 |
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Edition |
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ISSN |
0584-8547; 0038-6987 |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.241 |
Times cited |
7 |
Open Access |
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Notes |
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Approved |
Most recent IF: 3.241; 2009 IF: 2.719 |
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Call Number |
UA @ admin @ c:irua:79739 |
Serial |
5778 |
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Author |
de Nolf, W.; Jaroszewicz, J.; van der Snickt, G.; Janssens, K.; Farnell, S.; Klaassen, L. |
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Title |
Combined micro-XRF/XRPD tomography on historical and modern paint multilayer samples at Beamline L |
Type |
H3 Book chapter |
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Year |
2008 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
1633-1634 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:74475 |
Serial |
5522 |
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Permanent link to this record |
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Author |
de Nolf, W.; Vanmeert, F.; Janssens, K. |
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Title |
XRDUA : crystalline phase distribution maps by two-dimensional scanning and tomographic (micro) X-ray powder diffraction |
Type |
A1 Journal article |
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Year |
2014 |
Publication |
Journal of applied crystallography |
Abbreviated Journal |
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Volume |
47 |
Issue |
3 |
Pages |
1107-1117 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Imaging of crystalline phase distributions in heterogeneous materials, either plane projected or in virtual cross sections of the object under investigation, can be achieved by scanning X-ray powder diffraction employing X-ray micro beams and X-ray-sensitive area detectors. Software exists to convert the two-dimensional powder diffraction patterns that are recorded by these detectors to one-dimensional diffractograms, which may be analysed by the broad variety of powder diffraction software developed by the crystallography community. However, employing these tools for the construction of crystalline phase distribution maps proves to be very difficult, especially when employing micro-focused X-ray beams, as most diffraction software tools have mainly been developed having structure solution in mind and are not suitable for phase imaging purposes. XRDUA has been developed to facilitate the execution of the complete sequence of data reduction and interpretation steps required to convert large sequences of powder diffraction patterns into a limited set of crystalline phase maps in an integrated fashion. |
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000336738500031 |
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2014-05-28 |
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ISSN |
0021-8898 |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
62 |
Open Access |
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Notes |
; The authors would like to thank the synchrotron beamline staff at ID15 (ESRF, Grenoble, France), MicroXAS (SLS, Villigen, Switzerland) and PO6/BL-L (Petra III/Hasylab, Hamburg, Germany) for accommodating the experiments presented in this paper. Support from FWO 'Big Science' project G0C1213N as well as from the BELSPO project 'S2ART' (SD/RI/04A) is acknowledged. ; |
Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:117758 |
Serial |
5920 |
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Permanent link to this record |
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Author |
de Nolf, W.; Vekemans, B.; Janssens, K.; van der Snickt, G.; Falkenberg, G. |
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Title |
Pigment identification by scanning μ-XRF/μ-XRD |
Type |
H3 Book chapter |
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Year |
2007 |
Publication |
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Abbreviated Journal |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:64595 |
Serial |
5773 |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J. |
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Title |
Echt of namaak? Venetiaans glas uit het oude Antwerpen |
Type |
A3 Journal article |
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Year |
1999 |
Publication |
De wetenschappelijke bibliotheek |
Abbreviated Journal |
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Volume |
67 |
Issue |
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Pages |
58-67 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:25300 |
Serial |
5579 |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J. |
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Title |
On the distinction between 16th and 17th century Venetian glass and façon-de-Venise glass |
Type |
H3 Book chapter |
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Year |
2002 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
95-121 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:40354 |
Serial |
5754 |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Adams, F. |
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Title |
Composition of facon-de-venise and Venetian glass from Antwerp and the Southern Netherlands |
Type |
H3 Book chapter |
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Year |
2000 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
346-350 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:27699 |
Serial |
5542 |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Adams, F. |
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Title |
Samenstelling van 15de- tot 17de-eeuwse glazen voorwerpen opgegraven in Antwerpen |
Type |
H3 Book chapter |
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Year |
1998 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
89-110 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:19318 |
Serial |
5823 |
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Permanent link to this record |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Adams, F. |
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Title |
Samenstelling van 15de- tot 17de-eeuwse glazen voorwerpen opgegraven in Antwerpen: deel 1 |
Type |
A3 Journal article |
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Year |
1998 |
Publication |
Journaal van de Belgische Vereniging voor Glastechnieken |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
9-17 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:24908 |
Serial |
5824 |
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Permanent link to this record |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Adams, F. |
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Title |
Samenstelling van 15de- tot 17de-eeuwse glazen voorwerpen opgegraven in Antwerpen: deel 2 |
Type |
A3 Journal article |
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Year |
1998 |
Publication |
Journaal van de Belgische Vereniging voor Glastechnieken |
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Volume |
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Issue |
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Pages |
5-19 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:24910 |
Serial |
5825 |
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Permanent link to this record |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Adriaens, A.; Adams, F. |
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Title |
Glass trade in Antwerp during the 15th through 17th century |
Type |
H3 Book chapter |
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Year |
2000 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
38-44 |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:27860 |
Serial |
5634 |
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Permanent link to this record |
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Author |
de Raedt, I.; Janssens, K.; Veeckman, J.; Vincze, L.; Vekemans, B.; Jeffries, T. |
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Title |
Trace analysis allows to distinguish between Venetian and facon-de-Venise glass vessels of the 16th and 17th century |
Type |
A1 Journal article |
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Year |
2001 |
Publication |
Journal of analytical atomic spectrometry |
Abbreviated Journal |
J Anal Atom Spectrom |
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Volume |
16 |
Issue |
9 |
Pages |
1012-1017 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000171287600020 |
Publication Date |
2002-07-26 |
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Abbreviated Series Title |
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Edition |
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ISSN |
0267-9477 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
3.379 |
Times cited |
49 |
Open Access |
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Notes |
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Approved |
Most recent IF: 3.379; 2001 IF: 3.305 |
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Call Number |
UA @ admin @ c:irua:34090 |
Serial |
5878 |
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Permanent link to this record |
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Author |
de Raedt, I.; Vekemans, B.; Janssens, K.; Adams, F. |
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Title |
Synchrotron light through ancient glass |
Type |
A3 Journal article |
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Year |
2000 |
Publication |
Europhysics news |
Abbreviated Journal |
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Volume |
31 |
Issue |
6 |
Pages |
15 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Edition |
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ISSN |
0531-7479 |
ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
|
Open Access |
|
|
|
Notes |
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Approved |
Most recent IF: NA |
|
|
Call Number |
UA @ admin @ c:irua:31697 |
Serial |
5863 |
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Permanent link to this record |
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Author |
De Vis, K.; Caen, J.; Janssens, K.; Jacobs, P. |
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Title |
The consolidation of cracks and fissures in dalle de verre : assessment of selected adhesives |
Type |
H2 Book chapter |
|
Year |
2013 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
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Pages |
43-52 |
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Keywords |
H2 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Antwerp Cultural Heritage Sciences (ARCHES) |
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|
Abstract |
Dalle de verre windows, created from 19301940 onwards, consist of glass pieces with a thickness of approximately 2 to 5 cm, set in a matrix of (reinforced) concrete. Besides the degradation of the concrete, the windows suffer mainly from a complex three-dimensional form of cracking of the glass elements. The cracks need to be consolidated in order to ensure stability and improve transparency. A selection of possible adhesives was evaluated: Araldite® 2020, Hxtal NYL-1, Fynebond, Paraloid® B-72, LV740, A18 and OR-G®. An attempt has been made to objectively compare these adhesives using a bench-marking system. None of the adhesives appears to be suitable for in situ application; sufficient penetration of the adhesives can only be realised with the help of vacuum techniques. |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
978-90-8932-113-8 |
Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:114606 |
Serial |
5557 |
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Permanent link to this record |
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Author |
De Vis, K.; Cagno, S.; Van Mol, W.; Schalm, O.; Janssens, K.; Caen, J. |
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Title |
The decolourization of manganese-stained glass : the conversion reaction and evaluation of its effectiveness |
Type |
P2 Proceeding |
|
Year |
2012 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
463-468 |
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Keywords |
P2 Proceeding; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Corporate Author |
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Place of Publication |
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Editor |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
978-90-72290-00-7 |
ISBN |
|
Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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|
Call Number |
UA @ admin @ c:irua:115470 |
Serial |
5566 |
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Permanent link to this record |
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Author |
De Vis, K.; Jacobs, P.; Caen, J.; Janssens, K. |
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Title |
The use of glass bricks in architecture in the 19th and 20th centuries : a case study |
Type |
P2 Proceeding |
|
Year |
2010 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
194-201 |
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Keywords |
P2 Proceeding; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Place of Publication |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
978-0-87290-182-7 |
ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
|
Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:124194 |
Serial |
5892 |
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Permanent link to this record |
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Author |
De Vis, K.; Jacobs, P.; Janssens, K.; Caen, J. |
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Title |
The consolidation of cracks in architectural glass and dalle de verre : first assessment of possible adhesives |
Type |
P3 Proceeding |
|
Year |
2011 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
|
Abbreviated Series Title |
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Series Volume |
|
Series Issue |
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Edition |
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|
|
ISSN |
|
ISBN |
9783839602553 |
Additional Links |
UA library record |
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Impact Factor |
|
Times cited |
|
Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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|
Call Number |
UA @ admin @ c:irua:115170 |
Serial |
5558 |
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Permanent link to this record |
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Author |
De Vis, K.; Janssens, K.; Jacobs, P.; Caen, J. |
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Title |
Dealing with architectural glasses : maintenance, monitoring and emergency treatment |
Type |
P3 Proceeding |
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Year |
2015 |
Publication |
|
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Antwerp Cultural Heritage Sciences (ARCHES) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
|
ISBN |
978-2-9543731-1-9 |
Additional Links |
UA library record |
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Impact Factor |
|
Times cited |
|
Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:126833 |
Serial |
5565 |
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Permanent link to this record |
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Author |
De Vis, K.; Jembrih-Simbürger, D.; Schalm, O.; Schreiner, M.; Caen, J. |
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Title |
Einfluss verschiedener Silbersalze auf die Farbintensität von Silbergelb : analytische Untersuchungen |
Type |
A2 Journal article |
|
Year |
2002 |
Publication |
Zeitschrift für Kunsttechnologie und Konservierung |
Abbreviated Journal |
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Volume |
16 |
Issue |
1 |
Pages |
147-157 |
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Keywords |
A2 Journal article; Art; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Place of Publication |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0931-7198 |
ISBN |
|
Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:107748 |
Serial |
7855 |
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Permanent link to this record |
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Author |
De Wael, K.; Bashir, Q.; van Vlierberghe, S.; Dubruel, P.; Heering, H.A.; Adriaens, A. |
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Title |
Electrochemical determination of hydrogen peroxide with cytochrome c peroxidase and horse heart cytochrome c entrapped in a gelatin hydrogel |
Type |
A1 Journal article |
|
Year |
2012 |
Publication |
Bioelectrochemistry: an international journal devoted to electrochemical aspects of biology and biological aspects of electrochemistry |
Abbreviated Journal |
Bioelectrochemistry |
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Volume |
83 |
Issue |
|
Pages |
15-18 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
A novel and versatile method, based on a membrane-free enzyme electrode in which both the enzyme and a mediator protein are entrapped in a gelatine hydrogel was developed for the fabrication of biosensors. As a proof of principle, we prepared a hydrogen peroxide biosensor by successfully entrapping both horse heart cytochrome c (HHC) and Saccharomyces cerevisae cytochrome c peroxidase (CCP) in a gelatin matrix which is immobilized on a gold electrode. This electrode was first pretreated with 6-mercaptohexanol. The biosensor displayed a rapid response and an expanded linear response range from 0 to 0.3 mM (R = 0.987) with a detection limit of 1 × 10− 5 M in a HEPES buffer solution (pH 7.0). This method of encapsulation is now further investigated for industrial biosensor applications. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Wos |
000297962500003 |
Publication Date |
2011-08-03 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1567-5394 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
|
|
Impact Factor |
3.346 |
Times cited |
31 |
Open Access |
|
|
|
Notes |
; Karolien De Wael is grateful to the Research Foundation-Flanders (FWO, Belgium) for her postdoctoral fellowship. ; |
Approved |
Most recent IF: 3.346; 2012 IF: 3.947 |
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|
Call Number |
UA @ admin @ c:irua:92067 |
Serial |
5589 |
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Permanent link to this record |
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Author |
De Wael, K.; Daems, D.; Van Camp, G.; Nagels, L.J. |
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Title |
The use of potentiometric sensors to study (bio)molecular interactions |
Type |
A1 Journal article |
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Year |
2012 |
Publication |
Analytical chemistry |
Abbreviated Journal |
Anal Chem |
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Volume |
84 |
Issue |
11 |
Pages |
4921-4927 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Potentiometric sensors were used to study molecular interactions in liquid environments, with sensorgram methodology. This is demonstrated with a lipophilic rubber-, and with a collagen based hydrogel sensor coating. The investigated molecules were promazine and tartaric acid respectively. The sensors were placed in a hydrodynamic wall jet system for the recording of sensorgrams. mV sensor responses were first converted to a signal, expressing the concentration of adsorbed organic ions. Using a linearization method, a pseudo first order kinetic model of adsorption was shown to fit the experimental results perfectly. Kass, kon and koff values were calculated.. The technique can be used over 4 decades of concentration, and it is very sensitive to low MW compounds as well as to multiply charged large biomolecules. This study is the first to demonstrate the application of potentiometric sensors as an alternative and complement to SPR methods. |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000304783100041 |
Publication Date |
2012-04-28 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2700; 5206-882x |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
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|
Impact Factor |
6.32 |
Times cited |
10 |
Open Access |
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|
|
Notes |
; Financial support for this work was provided by the University of Antwerp by granting D.D. a BOF interdisciplinary research project. We thank J. Everaert for his help in interpreting the results. K.D.W. and D.D. contributed equally to this work. ; |
Approved |
Most recent IF: 6.32; 2012 IF: 5.695 |
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Call Number |
UA @ admin @ c:irua:97520 |
Serial |
5898 |
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Permanent link to this record |
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Author |
De Wael, K.; De Belder, S.; Pilehar, S.; Van Steenberge, G.; Herrebout, W.; Heering, H.A. |
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Title |
Enzyme-gelatin electrochemical biosensors : scaling down |
Type |
A1 Journal article |
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Year |
2012 |
Publication |
Biosensors |
Abbreviated Journal |
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Volume |
2 |
Issue |
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Pages |
101-113 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Molecular Spectroscopy (MolSpec) |
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|
Abstract |
In this article we investigate the possibility of scaling down enzyme-gelatin modified electrodes by spin coating the enzyme-gelatin layer. Special attention is given to the electrochemical behavior of the selected enzymes inside the gelatin matrix. A glassy carbon electrode was used as a substrate to immobilize, in the first instance, horse heart cytochrome c (HHC) in a gelatin matrix. Both a drop dried and a spin coated layer was prepared. On scaling down, a transition from diffusion controlled reactions towards adsorption controlled reactions is observed. Compared to a drop dried electrode, a spin coated electrode showed a more stable electrochemical behavior. Next to HHC, we also incorporated catalase in a spin coated gelatin matrix immobilized on a glassy carbon electrode. By spincoating, highly uniform sub micrometer layers of biocompatible matrices can be constructed. A full electrochemical study and characterization of the modified surfaces has been carried out. It was clear that in the case of catalase, gluteraldehyde addition was needed to prevent leaking of the catalase from the gelatin matrix. |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Wos |
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Publication Date |
2012-03-15 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
2079-6374 |
ISBN |
|
Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
|
Approved |
Most recent IF: NA |
|
|
Call Number |
UA @ admin @ c:irua:96507 |
Serial |
5606 |
|
Permanent link to this record |
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Author |
De Wael, K.; Nagels, L.; Van Camp, G. |
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Title |
Potentiometric sensors and method for measuring intermolecular interactions |
Type |
Patent |
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Year |
2013 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
Patent; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:111264 |
Serial |
5779 |
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Permanent link to this record |
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Author |
De Wael, K.; Verstraete, A.; van Vlierberghe, S.; Dejonghe, W.; Dubruel, P.; Adriaens, A. |
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Title |
The electrochemistry of a gelatin modified gold electrode |
Type |
A1 Journal article |
|
Year |
2011 |
Publication |
International journal of electrochemical science |
Abbreviated Journal |
Int J Electrochem Sc |
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Volume |
6 |
Issue |
6 |
Pages |
1810-1819 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
This paper discusses the electrochemical behaviour of gelatin coated gold electrodes in physiological pH conditions in a potential window −1.5 till 1.0 V vs SCE by performing cyclic voltammetry. A comparison is made between gelatin A and gelatin B, which have respectively a positive and a negative net charge at physiological pH. The deposition of gelatin onto the gold surface is confirmed by means of attenuated total reflection-infrared (ATR-IR) spectroscopic analyses. |
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Place of Publication |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1452-3981 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles; WoS full record; WoS citing articles |
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|
Impact Factor |
1.469 |
Times cited |
|
Open Access |
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|
Notes |
; The authors would like to acknowledge the Flemish Institute for Technological Research (VITO, Belgium) and the Research Foundation-Flanders (FWO, Belgium) for the Ph.D. funding granted to Annelies Verstraete. Karolien De Wael and Sandra Van Vlierberghe are also grateful to the Research Foundation-Flanders (FWO, Belgium) for their postdoctoral fellowship. ; |
Approved |
Most recent IF: 1.469; 2011 IF: 3.729 |
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Call Number |
UA @ admin @ c:irua:89617 |
Serial |
5598 |
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Permanent link to this record |
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Author |
Decleir, W.; Vlaeminck, A.; Geladi, P.; Van Grieken, R. |
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Title |
Determination of protein-bound copper and zinc in some organs of the cuttlefish Sepia officinalis L |
Type |
A1 Journal article |
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Year |
1978 |
Publication |
Comparative biochemistry and physiology : B : biochemistry and molecular biology |
Abbreviated Journal |
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Volume |
60 |
Issue |
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Pages |
347-350 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Thesis |
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Wos |
A1978FN59800001 |
Publication Date |
2003-02-11 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
1096-4959 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:116555 |
Serial |
7785 |
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Permanent link to this record |
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Author |
Dekov, V.; Subramanian, V.; Van Grieken, R. |
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Title |
Chemical composition of riverine suspended matter and sediments from the Indian sub-continent |
Type |
A3 Journal article |
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Year |
1999 |
Publication |
Mitteilungen aus dem Geologisch-Paläontologischen Institut der Universität Hamburg |
Abbreviated Journal |
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Volume |
82 |
Issue |
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Pages |
99-109 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0072-1115 |
ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:24722 |
Serial |
7655 |
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Permanent link to this record |
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Author |
Dekov, V.; van Alsenoy, V.; Onar, N.; van Put, A.; Van Grieken, R. |
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Title |
Partitioning of heavy metals between estuarine sediments and dissolved phase as a function of salinity, pH and time (Scheldt estuary) |
Type |
A1 Journal article |
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Year |
2001 |
Publication |
Geologica Balcanica |
Abbreviated Journal |
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Volume |
30 |
Issue |
3/4 |
Pages |
65-76 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Abbreviated Series Title |
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Series Issue |
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Edition |
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ISSN |
0324-0894 |
ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:36086 |
Serial |
8362 |
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Permanent link to this record |
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Author |
Dekov, V.M.; Araujo, F.; Van Grieken, R.; Subramanian, V. |
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Title |
Chemical composition of sediments and suspended matter from the Cauvery and Brahmaputra rivers (India) |
Type |
A1 Journal article |
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Year |
1998 |
Publication |
The science of the total environment |
Abbreviated Journal |
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|
|
Volume |
212 |
Issue |
|
Pages |
89-105 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
000073203500001 |
Publication Date |
2002-07-26 |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
|
Series Issue |
|
Edition |
|
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ISSN |
0048-9697; 1879-1026 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Impact Factor |
|
Times cited |
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Open Access |
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Notes |
|
Approved |
no |
|
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Call Number |
UA @ admin @ c:irua:20962 |
Serial |
7656 |
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Permanent link to this record |