Records |
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vleugels, G.; Dewolfs, R.; Van Grieken, R. |
Title |
On the memory effect of limestone for air pollution |
Type |
A1 Journal article |
Year |
1993 |
Publication |
Atmospheric environment: part A : general topics |
Abbreviated Journal |
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Volume |
27 |
Issue |
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Pages |
1931-1934 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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A1993LX59700015 |
Publication Date |
2003-08-06 |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0960-1686; 1878-2124 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:6125 |
Serial |
8331 |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vleugels, G.; Fobe, B.; Dewolfs, R.; Van Grieken, R. |
Title |
Surface composition alteration of bare and treated limestones after ambient exposure |
Type |
A1 Journal article |
Year |
1994 |
Publication |
The science of the total environment |
Abbreviated Journal |
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Volume |
151 |
Issue |
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Pages |
59-69 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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A1994NW21600007 |
Publication Date |
2003-09-12 |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0048-9697; 1879-1026 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:8943 |
Serial |
8625 |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vleugels, G.; Van Grieken, R. |
Title |
Suspended matter in run-off water from limestone exposure setups |
Type |
A1 Journal article |
Year |
1995 |
Publication |
The science of the total environment |
Abbreviated Journal |
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Volume |
170 |
Issue |
|
Pages |
125-132 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
A1995RX37000012 |
Publication Date |
2002-07-26 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0048-9697; 1879-1026 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:12349 |
Serial |
8627 |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vleugels, G.; Van Grieken, R. |
Title |
Weathering of bare and treated limestones under ambient conditions using runoff water analysis and microanalysis |
Type |
P3 Proceeding |
Year |
1992 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
Impact Factor |
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Times cited |
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Open Access |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:2865 |
Serial |
8752 |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vleugels, G.J.; Van Grieken, R.E. |
Title |
Weathering of treated and untreated limestones in atmospheric exposures |
Type |
A3 Journal article |
Year |
1991 |
Publication |
Journal of preservation technology |
Abbreviated Journal |
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Volume |
23 |
Issue |
|
Pages |
48-51 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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ISBN |
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UA library record |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:4320 |
Serial |
8755 |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Komy, G.; Reggers, G.; Roekens, E.; Van Grieken, R. |
Title |
Determination of trace metals in rain water by differential-pulse stripping voltammetry |
Type |
A1 Journal article |
Year |
1986 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
|
Volume |
184 |
Issue |
|
Pages |
271-280 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Differential-pulse stripping voltammetry is applied to measure zinc, cadmium, lead and copper by anodic stripping and selenium(IV) by cathodic stripping in rain water at pH 2; subsequently, at pH 9,1, manganese is measured by anodic stripping on the same portion, and cobalt and nickel are measured in the adsorptive mode after formation of their dimethylglyoximates. The instrumental parameters are optimized. The linear ranges, mutual interferences and detection limits are studied. Excellent accuracy is demonstrated; the standard deviation is around 15% at 2.550 μg l−1 levels. The method is shown to be applicable for rain water. |
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Wos |
A1986D964700026 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2670; 1873-4324 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116444 |
Serial |
7793 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Robberecht, H.; Van Dyck, P.; Van Grieken, R. |
Title |
Multi-element analysis of urine by energy-dispersive x-ray fluorescence spectrometry |
Type |
A1 Journal article |
Year |
1981 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
|
Volume |
130 |
Issue |
1 |
Pages |
167-175 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
For multi-element analysis of human urine, 25-ml samples doped with yttrium as internal standard are evaporated gently and then ashed up to 460°C overnight. The residue is pelletized and analysed by energy-dispersive x-ray fluorescence. Acid addition to facilitate the digestion is not mandatory. Recoveries are nearly quantitative for traces of Fe, Ni, Cu, Zn and Sr, to a lesser extent for lead, but not for arsenic or selenium. The standard deviation per measurement is typically around 6%. The detection limits are such that some 10 elements can be determined simultaneously in normal urine, and possibly more in cases of importance to toxicology or industrial hygiene. |
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Place of Publication |
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Wos |
A1981ME98900017 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0003-2670; 1873-4324 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:116439 |
Serial |
8285 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Influence of ion energy-distributions and matrix effects on spark source-mass spectrometric analysis |
Type |
A1 Journal article |
Year |
1983 |
Publication |
International journal of mass spectrometry and ion processes |
Abbreviated Journal |
|
Volume |
51 |
Issue |
1 |
Pages |
63-76 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
The energy distributions of ions produced in a spark source mass spectrometer were recorded for different trace element ions and for the total ion current. Both electrodes of pure doped graphite, and with 10% potassium salts added, were examined. The results show that the measured energy of an ion is mainly determined by the m/z ratio and that the energy of the total ion current depends on the sample composition. It was also clear that if the accelerating voltage is set to obtain maximum transmission of the total ion current, the fraction of the heavy elements that is discriminated at the β-slit depends on the matrix composition if the pass band of the instrument is narrow. These effects influence considerably the accuracy in the analysis of variable samples. |
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Place of Publication |
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Language |
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Wos |
A1983QV48400008 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
0168-1176; 1873-2801 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
Call Number |
UA @ admin @ c:irua:113624 |
Serial |
8093 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Influence of ion-source geometry in spark source-mass spectrometric analysis |
Type |
A1 Journal article |
Year |
1984 |
Publication |
International journal of mass spectrometry and ion processes |
Abbreviated Journal |
|
Volume |
59 |
Issue |
3 |
Pages |
221-229 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
A1984TK37900001 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0168-1176; 1873-2801 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
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Open Access |
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Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:113618 |
Serial |
8094 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Influence of spark generator parameters in the analysis of graphite-electrodes by spark source-mass spectrometry |
Type |
A1 Journal article |
Year |
1984 |
Publication |
International journal of mass spectrometry and ion processes |
Abbreviated Journal |
|
Volume |
55 |
Issue |
3 |
Pages |
233-247 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Spark source mass spectrometric analyses of doped carbon samples were performed at different pulse lengths, pulse frequencies and breakdown voltages. The pulse length and pulse frequencies had no influence on the analysis. The relation between breakdown voltage, spark gap and sample matrix was determined. With increasing breakdown voltage, the abundance of the multiply charged ions was found to decrease, whereas the abundance of the cluster ions increased. The breakdown voltage was also found to affect the absolute and relative intensities of different elements in different manners. Interpretation of these results led to some new considerations on the phenomena in a spark discharge. |
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Wos |
A1984SA13700002 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0168-1176; 1873-2801 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:113619 |
Serial |
8098 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Matrix effects and analysis of biological material by spark source mass spectrometry |
Type |
A3 Journal article |
Year |
1985 |
Publication |
Fresenius' Zeitschrift für analytische Chemie |
Abbreviated Journal |
|
Volume |
321 |
Issue |
1 |
Pages |
32-36 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Spark-source mass spectrometric analyses of synthetic simulated biological samples were performed to determine the importance of matrix effects. A correlation between the variation of the relative sensitivity coefficients (RSC's) and the spark plasma composition, hence plasma temperature, was found. The determined RSC's were used in the analysis of four biological standard reference materials. An accuracy of 1013% and detection limits between 0.005 and 0.5 ppm were obtained during analysis under normal conditions. |
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Corporate Author |
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Place of Publication |
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Language |
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Wos |
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Publication Date |
2004-11-14 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0016-1152 |
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116641 |
Serial |
8209 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Preparation of conducting electrodes from biological samples for multi-element trace analysis by spark-source mass spectrometry or emission spectrometry |
Type |
A1 Journal article |
Year |
1984 |
Publication |
Analytica chimica acta |
Abbreviated Journal |
|
Volume |
164 |
Issue |
|
Pages |
83-90 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
Four decomposition procedures frequently used for biological material (dry ashing, open wet digestion, wet digestion in a teflon bomb and low-temperature ashing) are optimized for the conversion of biological samples to conducting electrodes suitable for multi-element trace determinations by spark-source mass spectrometry or emission spectrometry. The optimized procedures are evaluated with respect to contamination, retention and preconcentration of the trace elements, homogeneity of the electrodes and precision of the final results. Both dry-ashing methods are prone to losses by volatilization; simple dry ashing suffers from contamination problems during electrode preparation. Wet digestion gives better precision; digestion with nitric/sulfuric acids in an open flask is the method of choice for most elements being simpler and giving lower blanks than the bomb method. |
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Language |
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Wos |
A1984ABC2700007 |
Publication Date |
2002-07-25 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0003-2670; 1873-4324 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:116443 |
Serial |
8411 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Vos, L.; Van Grieken, R. |
Title |
Spark source mass spectrometry for trace analysis of diverse biological matrices |
Type |
H3 Book chapter |
Year |
1983 |
Publication |
|
Abbreviated Journal |
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Volume |
|
Issue |
|
Pages |
303-306
T2 - Mass spectrometry advances 1982 / Sch |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
Impact Factor |
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Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:117486 |
Serial |
8564 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wadsak, M.; Constantinides, I.; Vittiglio, G.; Adriaens, A.; Janssens, K.; Schreiner, M.; Adams, F.C.; Brunella, P.; Wuttmann, M. |
Title |
Multianalytical study of patina formed on archaeological metal objects from Bliesbruck-Reinheim |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Microchimica acta |
Abbreviated Journal |
Microchim Acta |
Volume |
133 |
Issue |
|
Pages |
159-164 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Language |
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Wos |
000087797400024 |
Publication Date |
2003-02-12 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
|
ISSN |
0026-3672; 1436-5073 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
4.58 |
Times cited |
|
Open Access |
|
Notes |
|
Approved |
Most recent IF: 4.58; 2000 IF: 1.303 |
Call Number |
UA @ admin @ c:irua:28228 |
Serial |
5740 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wagner, B.; Nowak, A.; Bulska, E.; Kunicki-Goldfinger, J.; Schalm, O.; Janssens, K. |
Title |
Analiza pierwiastkowa zabytkowych obiektów szklanych |
Type |
A3 Journal article |
Year |
2008 |
Publication |
Nauka i Zabytki |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
71-82 |
Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Corporate Author |
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Publisher |
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Place of Publication |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
Most recent IF: NA |
Call Number |
UA @ admin @ c:irua:115027 |
Serial |
5465 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wagner, B.; Nowak, A.; Bulska, E.; Kunicki-Goldfinger, J.; Schalm, O.; Janssens, K.; schalm |
Title |
Complementary analysis of historical glass by scanning electron microscopy with energy dispersive X-ray spectroscopy and laser ablation inductiveley coupled plasma mass spectrometry |
Type |
A1 Journal article |
Year |
2008 |
Publication |
Microchimica acta |
Abbreviated Journal |
|
Volume |
162 |
Issue |
3-4 |
Pages |
415-424 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Publisher |
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Place of Publication |
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Wos |
000258194900014 |
Publication Date |
2007-10-26 |
Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
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Times cited |
28 |
Open Access |
|
Notes |
|
Approved |
Most recent IF: NA |
Call Number |
UA @ admin @ c:irua:70565 |
Serial |
5533 |
Permanent link to this record |
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Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wegrzynek, D.; Eisma, D.; Van Grieken, R. |
Title |
Individual particle analysis of sediments from the Gulf of Lions, suspensions from the Rhône river and dust of Saharan origin: preliminary results |
Type |
P3 Proceeding |
Year |
1992 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
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Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
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Language |
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Wos |
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Publication Date |
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Series Editor |
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Series Title |
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Abbreviated Series Title |
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Series Volume |
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Series Issue |
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Edition |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
Impact Factor |
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Times cited |
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Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:2861 |
Serial |
8078 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wegrzynek, D.; Jambers, W.; Van Grieken, R.; Eisma, D. |
Title |
Individual particle analysis of Western Mediterranean sediment cores, Rhône suspended matter and Sahara aerosols: investigation of inputs to the sediments |
Type |
A1 Journal article |
Year |
1997 |
Publication |
Marine chemistry |
Abbreviated Journal |
|
Volume |
57 |
Issue |
|
Pages |
25-40 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
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Corporate Author |
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Thesis |
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Publisher |
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Place of Publication |
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Editor |
|
Language |
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Wos |
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Publication Date |
|
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0304-4203; 1872-7581 |
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:18778 |
Serial |
8079 |
Permanent link to this record |
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|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wegrzynek, D.; Van Grieken, R.; Eisma, D. |
Title |
Particle analysis of sediments from the Gulf of Lions, suspended matter from the Rhone river, and Sahara dust |
Type |
H3 Book chapter |
Year |
1994 |
Publication |
|
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
51-60
T2 - Particles and particle-water interactio |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
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Corporate Author |
|
Thesis |
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Publisher |
|
Place of Publication |
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Editor |
|
Language |
|
Wos |
|
Publication Date |
|
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
|
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:9525 |
Serial |
8358 |
Permanent link to this record |
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|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Winchester, J.W.; Meinert, D.L.; Nelson, J.W.; Johansson, T.B.; Van Grieken, R.E.; Orsini, C.; Kaufmann, H.C.; Akselsson, R. |
Title |
Trace metals in the St-Louis aerosol |
Type |
H3 Book chapter |
Year |
1975 |
Publication |
|
Abbreviated Journal |
|
Volume |
|
Issue |
|
Pages |
385-394
T2 - Nuclear techniques in environmental r |
Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
|
Publication Date |
|
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
|
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:117459 |
Serial |
8694 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wiorek, A.; Parrilla, M.; Cuartero, M.; Crespo, G.A. |
Title |
Epidermal patch with glucose biosensor : pH and temperature correction toward more accurate sweat analysis during sport practice |
Type |
A1 Journal article |
Year |
2020 |
Publication |
Analytical Chemistry |
Abbreviated Journal |
Anal Chem |
Volume |
92 |
Issue |
14 |
Pages |
10153-10161 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
We present an epidermal patch for glucose analysis in sweat incorporating for the first time pH and temperature correction according to local dynamic fluctuations in sweat during on-body tests. This sort of correction is indeed the main novelty of the paper, being crucial toward reliable measurements in every sensor based on an enzymatic element whose activity strongly depends on pH and temperature. The results herein reported for corrected glucose detection during on-body measurements are supported by a two-step validation protocol: with the biosensor operating off- and on-bodily, correlating the results with UV-vis spectrometry and/or ion chromatography. Importantly, the wearable device is a flexible skin patch that comprises a microfluidic cell designed with a sweat collection zone coupled to a fluidic channel in where the needed electrodes are placed: glucose biosensor, pH potentiometric electrode and a temperature sensor. The glucose biosensor presents a linear range of response within the expected physiological levels of glucose in sweat (10-200 mu M), and the calibration parameters are dynamically adjusted to any change in pH and temperature during the sport practice by means of a new “correction approach”. In addition, the sensor displays a fast response time, appropriate selectivity, and excellent reversibility. A total of 9 validated on-body tests are presented: the outcomes revealed a great potential of the wearable glucose sensor toward the provision of reliable physiological data linked to individuals during sport activity. In particular, the developed “correction approach” is expected to impact into the next generation of wearable devices that digitalize physiological activities through chemical information in a trustable manner for both sport and healthcare applications. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000554986200089 |
Publication Date |
2020-06-26 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0003-2700; 5206-882x |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
7.4 |
Times cited |
|
Open Access |
|
Notes |
|
Approved |
Most recent IF: 7.4; 2020 IF: 6.32 |
Call Number |
UA @ admin @ c:irua:175265 |
Serial |
7931 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Wonders, J.H.A.M.; Houweling, S.; de Bont, F.A.J.; van Leeuwen, H.P.; Eeckhaoudt, S.M.; Van Grieken, R. |
Title |
Characterization of aerosol-associated lead by DPASV and LAMMA |
Type |
A1 Journal article |
Year |
1994 |
Publication |
International journal of environmental analytical chemistry |
Abbreviated Journal |
|
Volume |
56 |
Issue |
|
Pages |
193-205 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
A1994PF99800002 |
Publication Date |
2007-07-07 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0306-7319 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:9514 |
Serial |
7611 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Darchuk, L.; Brooker, A.; Potgieter, H.; Van Grieken, R. |
Title |
Damage and molecular changes under a laser beam in SEM-EDX/MRS interface : a case study on iron-rich particles |
Type |
A1 Journal article |
Year |
2011 |
Publication |
Journal of Raman spectroscopy |
Abbreviated Journal |
|
Volume |
42 |
Issue |
4 |
Pages |
808-814 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
The control of damage to individual environmental particles by a laser beam during Raman spectroscopy carried out in ambient air is generally well understood. The nature and control of damage under vacuum conditions (e.g. in the scanning electron microscopy with energy X-ray detection combined with micro-Raman spectroscopyinterfaced SEM-EDX/MRS) are more complex and less well comprehended. The physical and chemical processes that affect the damage caused to small particles by lasers still remain somewhat unclear, but certainly the atmosphere (vacuum/air) and the beam intensity have very significant influences. Furthermore, it has been determined that some particles (e.g. haematite), although stable under an electron beam, are damaged by the laser beam, hampering their analysis. Additionally, when simultaneous analyses by SEM/EDX and MRS are considered, the correct choice of the collection surface plays a crucial role. As a result, the following collection substrates were tested to determine their influence on the laser beam damage process to the particle: silver and aluminium foils and silicon wafers. A test study was performed using artificial examples of haematite (Fe2O3) particles. Exposure of Fe2O3 particles in vacuum to 514- and 785-nm laser radiation often leads to their melting, transformation and evaporation. The dependence of the damage caused by the laser beam on the particle structure is reported here. Molecular and crystallographic changes have also been revealed. Formation of magnetite (as an effect of re-crystallisation) and Raman inactive structures was detected. |
Address |
|
Corporate Author |
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Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000290484700033 |
Publication Date |
2010-09-27 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0377-0486 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:89518 |
Serial |
7751 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; de Hoog, J.; Osán, J.; Szalóki, I.; Joos, P.; Van Grieken, R. |
Title |
Unconventional microanalysis for low-Z, volatile and organic aerosol compounds |
Type |
A1 Journal article |
Year |
2000 |
Publication |
Journal of aerosol science |
Abbreviated Journal |
|
Volume |
31 |
Issue |
S1 |
Pages |
384-385 |
Keywords |
A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
|
Publication Date |
|
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0021-8502; 1879-1964 |
ISBN |
|
Additional Links |
UA library record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:31639 |
Serial |
8704 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; de Hoog, J.; Osán, J.; Szalóki, I.; Ro, C.-U.; Van Grieken, R. |
Title |
Thermal stability of beam sensitive atmospheric aerosol particles in electron probe microanalysis at liquid nitrogen temperature |
Type |
A1 Journal article |
Year |
2003 |
Publication |
Spectrochimica acta: part B : atomic spectroscopy |
Abbreviated Journal |
|
Volume |
58 |
Issue |
|
Pages |
479-496 |
Keywords |
A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000182680400008 |
Publication Date |
2003-04-23 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0584-8547; 1873-3565 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:41220 |
Serial |
8663 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Kaplinski, A.; Van Grieken, R. |
Title |
Ruthenium staining as an alternative preparation method for automated EPMA of individual biogenic and organic particles |
Type |
A1 Journal article |
Year |
2005 |
Publication |
X-ray spectrometry |
Abbreviated Journal |
|
Volume |
34 |
Issue |
3 |
Pages |
245-252 |
Keywords |
A1 Journal article; Laboratory Experimental Medicine and Pediatrics (LEMP); AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000229093000014 |
Publication Date |
2005-01-31 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0049-8246 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:52229 |
Serial |
8488 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Potgieter-Vermaak, S.; Brooker, A.; Darchuk, L.; Stefaniak, E.; Van Grieken, R. |
Title |
Interfaced SEM/EDX and micro-Raman spectrometry for characterisation of heterogeneous environmental particles: fundamental and practical challenges |
Type |
A1 Journal article |
Year |
2010 |
Publication |
Microchemical journal |
Abbreviated Journal |
|
Volume |
94 |
Issue |
1 |
Pages |
65-72 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
The molecular character of atmospheric particulate matter is of prime importance when interpreting air pollution trends and its subsequent influence on environmental monitoring and preventative conservation. The known methods of estimating the molecular composition normally involve elemental analysis of particles (both as bulk and computer controlled analyses of single particles) with subsequent multivariate analyses to clusterise the elements in groups of elements that are closely related to each other. With this approach one can at best suggest associations. Evidently the application of molecular spectroscopy in addition to elemental concentration profiles would provide intimate information regarding the nature of the particles and consequently their fate. This paper gives an overview of research performed in our laboratory and describes the optimisation of experimental parameters to use scanning electron microscopy with energy-dispersive X-ray detection (SEM/EDX) or electron probe X-ray microanalysis (EPXMA) in parallel with micro-Raman Spectrometry (MRS) to investigate single environmental particles. The challenges associated with the two stand-alone techniques are revealed and consequently those posed with an interfaced approach are discussed. Preliminary results, of an initial investigation of the SEM/EDX interfaced with MRS to ultra-fine heterogeneous environmental particles, are given. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000273238800011 |
Publication Date |
2009-09-10 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0026-265x; 0026-265x |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:79801 |
Serial |
8114 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Potgieter-Vermaak, S.; Darchuk, L.; Vishnyakov, V.; Potgieter, H.; Van Grieken, R. |
Title |
Behavior of semi-volatile particles under a laser and electron beam: influence on the quality of analytical results |
Type |
A1 Journal article |
Year |
2010 |
Publication |
AIP conference proceedings |
Abbreviated Journal |
|
Volume |
1267 |
Issue |
|
Pages |
523-524 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
|
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000281210900279 |
Publication Date |
2010-08-05 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0094-243x |
ISBN |
|
Additional Links |
UA library record; WoS full record |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:84573 |
Serial |
7553 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Potgieter-Vermaak, S.S.; Berghmans, P.; Winkler, H.; Burger, R.; Van Grieken, R. |
Title |
Air particulate emissions in developing countries : a case study in South Africa |
Type |
A1 Journal article |
Year |
2011 |
Publication |
Analytical letters |
Abbreviated Journal |
|
Volume |
44 |
Issue |
11 |
Pages |
1907-1924 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
Atmospheric aerosols were collected during the winter in Bethlehem, South Africa. The particulate mass concentrations, ambient carbon mass concentrations, and chemical composition of various particulate fractions showed that the area is highly polluted. The fine particle mass concentrations peaked at 1000 µg/m3 for PM2.5. Ambient carbon mass concentrations ranged from 20 to 40 µg/m3. Single particle analysis confirmed that the fine particle fraction was dominated by organic particles. The topographical conditions, causing a low inversion, together with the high amounts of emissions from biomass burning, result in unacceptable levels of air pollution and pose a considerable health threat to the population. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000294602300006 |
Publication Date |
2011-08-12 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
0003-2719 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:91079 |
Serial |
7429 |
Permanent link to this record |
|
|
|
Author ![sorted by Author field, ascending order (up)](img/sort_asc.gif) |
Worobiec, A.; Samek, J.; Krata, A.; van Meel, K.; Krupińska, B.; Stefaniak, E.A.; Karaszkiewicz, P.; Van Grieken, R. |
Title |
Transport and deposition of airborne pollutants in exhibition areas located in historical buildings: study in Wawel Castle Museum in Cracow, Poland |
Type |
A1 Journal article |
Year |
2010 |
Publication |
Journal of cultural heritage |
Abbreviated Journal |
|
Volume |
11 |
Issue |
3 |
Pages |
354-359 |
Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Laboratory Experimental Medicine and Pediatrics (LEMP) |
Abstract |
Historical buildings and castles that have been turned nowadays into museums, as an exhibition area for precious cultural heritage (CH) items, need more attention since they are CH objects by themselves. Moreover, the preservation techniques require often, significant interventions; however such changes are not always possible or are very limited. The aim of the present study was to investigate the influence of outdoor air pollution on the composition of particulate matter and gases inside the museum of Wawel Castle in Cracow, Poland. During this study a combination of micro and trace analysis techniques were applied, including energy dispersive X-ray fluorescence (EDXRF) and electron probe microanalysis (EPMA). An intensive transport of air pollutants coupled with accumulation of the particles inside the museum was noticed (considerably higher in winter than summer). A high content of carbon and organic matter agglomerated with inorganic particles was determined. Those particles are of special concern because of their adhesive properties and reactivity. It was also noted that the conditions inside the museum favour the reaction of the particles with gaseous pollutants. It was especially the case for nitrate particles. |
Address |
|
Corporate Author |
|
Thesis |
|
Publisher |
|
Place of Publication |
|
Editor |
|
Language |
|
Wos |
000279867800017 |
Publication Date |
2010-03-25 |
Series Editor |
|
Series Title |
|
Abbreviated Series Title |
|
Series Volume |
|
Series Issue |
|
Edition |
|
ISSN |
1296-2074 |
ISBN |
|
Additional Links |
UA library record; WoS full record; WoS citing articles |
Impact Factor |
|
Times cited |
|
Open Access |
|
Notes |
|
Approved |
no |
Call Number |
UA @ admin @ c:irua:83277 |
Serial |
8698 |
Permanent link to this record |