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Author |
Marchetti, A. |
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Title |
Novel insights and approaches for the analytical characterization of tangible cultural heritage objects |
Type |
Doctoral thesis |
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Year |
2021 |
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Abbreviated Journal |
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Volume  |
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Pages |
333 p. |
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Keywords |
Doctoral thesis; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Cultural heritage represents the vehicle of our cultural identity, handed over from past to future generations throughout human history. As a repository of fundamental cultural and social values, the preservation of all forms of cultural heritage is a responsibility of every society and of humankind as a whole. When it comes to tangible cultural heritage, preservation of heritage translates into preservation of objects and, therefore, of the materials they are constituted of. This crucial task relies heavily on the application of scientific analytical methods to answer material and conservation-related questions. The fundamental contribution of this analytical approach led, in the past decades, to an ever-deepening understanding of the factors governing the degradation of cultural heritage. However, the extreme complexity of the heritage object-environment system results in a massive research field, which inevitably presents relevant open questions. This is where the present PhD work comes into play, attempting to fill knowledge gaps in literature by starting from specific case studies and un-answered research questions. The multianalytical research conducted during this PhD unraveled fundamental information on the properties governing the reactivity and long-term behavior of different classes of materials, from α-brass in an indoor environment to artists’ pigments in the presence of light, moisture and soluble particulate matter (PM). The paramount importance of the synthesis conditions on the composition, physical properties and reactivity of heritage materials was also demonstrated, in particular for stable lead pyroantimonate and unstable Geranium lake artists’ pigments. Moreover, the study and characterization of specific heritage objects, namely a series of 16th century reliquary altarpieces and the painting L’Arlesienne, by Vincent Van Gogh, allowed to obtain relevant insights into their composition and on potential risks for their conservation. The challenging nature of the samples considered, created the perfect opportunity to test an innovative spectroscopic technique, optical photo-thermal IR (O-PTIR), for the characterization of heritage materials. Striking results were obtained, highlighting a great potential for the application of this non-destructive sub-micron molecular spectroscopy to the analysis of cultural heritage. Finally, in the last section of this work, strategies to implement the continuous monitoring of PM levels in indoor environmental quality studies were also considered, with a particular focus on the identification of environmental hazards for the collections housed in specific conservation environments (War Heritage Institute in Brussels and St. Martin’s church in Aalst, BE). |
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Most recent IF: NA |
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Call Number |
UA @ admin @ c:irua:177849 |
Serial |
8319 |
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Author |
Van Grieken, R. |
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Title |
Ocean-atmosphere interactions and oil pollution |
Type |
P3 Proceeding |
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Year |
1974 |
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Abbreviated Journal |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:117457 |
Serial |
8325 |
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Author |
Misseeuw, L.; Krajewska, A.; Pasternak, I.; Ciuk, T.; Strupinski, W.; Reekmans, G.; Adriaensens, P.; Geldof, D.; Geldof, D.; Van Vlierberghe, S.; Thienpont, H.; Dubruelf, P.; Vermeulen, N. |
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Title |
Optical-quality controllable wet-chemical doping of graphene through a uniform, transparent and low-roughness F4-TCNQ/MEK layer |
Type |
A1 Journal article |
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Year |
2016 |
Publication |
RSC advances |
Abbreviated Journal |
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Volume |
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Issue |
106 |
Pages |
104491-104501 |
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A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Controllable chemical doping of graphene has already proven very useful for electronic applications, but when turning to optical and photonic applications, the additional requirement of having both a high transparency and a low surface roughness has, to our knowledge, not yet been fulfilled by any chemical dopant system reported so far. In this work, a new method that meets for the first time this opticalquality requirement while also providing efficient, controllable doping is presented. The method relies on F4-TCNQ dissolved in methyl ethyl ketone (MEK) yielding a uniform deposition after spin coating because of an extraordinary charge transfer interaction between the F4-TCNQ and MEK molecules. The formed F4-TCNQ/MEK layer exhibits a very high surface quality and optical transparency over the visible-infrared wavelength range between 550 and 1900 nm. By varying the dopant concentration of F4-TCNQ from 2.5 to 40 mg ml1 MEK, the doping effect can be controlled between Dn ¼ +5.73 1012 cm2 and +1.09 1013 cm2 for initially strongly p-type hydrogen-intercalated graphene grown on 6Hsilicon- carbide substrates, and between Dn ¼ +5.56 1012 cm2 and +1.04 1013 cm2 for initially weakly p-type graphene transferred on silicon samples. This is the first time that truly optical-quality chemical doping of graphene is demonstrated, and the obtained doping values exceed those reported before for F4-TCNQ-based graphene doping by as much as 50%. |
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000388111900075 |
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2016-10-27 |
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ISSN |
2046-2069 |
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UA library record; WoS full record; WoS citing articles |
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no |
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Call Number |
UA @ admin @ c:irua:136405 |
Serial |
8335 |
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Author |
Robberecht, H.; Van Grieken, R.; Van der Sloot, H.A. |
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Title |
OPtimized selenite determination in environmental waters by X-ray fluorescence |
Type |
H3 Book chapter |
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Year |
1980 |
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Abbreviated Journal |
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Pages |
463-468
T2 - Analytical techniques in environmenta |
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Keywords |
H3 Book chapter; Pharmacology. Therapy; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:117482 |
Serial |
8343 |
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Author |
Kontozova, V.; Godoi, R.; Krata, A.; Van Grieken, R. |
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Title |
Oszklenie ochronne i jego wpływ na średniowieczne okna witrazowe: z perspektywy chemii atmosfery: studium przypadku kaplica Sainte Chapelle w Paryzu |
Type |
A3 Journal article |
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Year |
2007 |
Publication |
Analityka |
Abbreviated Journal |
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3 |
Pages |
20-25 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:65079 |
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8349 |
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Author |
Margui, E.; Van Grieken, R. |
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Title |
Overview of most commonly used analytical techniques for elemental analysis |
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A3 Journal article |
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Year |
2014 |
Publication |
Petro Industry News |
Abbreviated Journal |
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8-10 |
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Keywords |
A3 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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1472-0590 |
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no |
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Call Number |
UA @ admin @ c:irua:114599 |
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8352 |
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Author |
Wegrzynek, D.; Van Grieken, R.; Eisma, D. |
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Title |
Particle analysis of sediments from the Gulf of Lions, suspended matter from the Rhone river, and Sahara dust |
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H3 Book chapter |
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1994 |
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51-60
T2 - Particles and particle-water interactio |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:9525 |
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8358 |
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Author |
Peeters, B.; Safdar, S.; Carlier, B.; Spasic, D.; Daems, D.; Lammertyn, J. |
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Title |
PCR amplified DNAzyme-amplicons for generic solid-phase antimicrobial resistance screening |
Type |
P1 Proceeding |
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Year |
2019 |
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Abbreviated Journal |
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Pages |
971-974
T2 - Transducers 2019 : Eurosensors XXXIII |
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Keywords |
P1 Proceeding; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
Fiber optic surface plasmon resonance (FO-SPR) has shown its potential for the detection of nucleic acids and more recently the technology has been combined with catalytic active strands such as DNAzymes. In this work, an innovative, generic solid-phase DNA sensor concept is presented, based on FO-SPR and PCR amplified DNAzyme activity. Improved levels of specificity and sensitivity were obtained down to picomolar concentrations. Moreover, the FO-SPR sensor concept enables AuNP amplified DNA target detection, independent of the target sequence length. The FO-SPR sensor was demonstrated for the screening of the mobile colistin resistance (MCR-2) gene, a gene important for the antimicrobial resistance in Gram-negative species such as E. Coli. |
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000539487000245 |
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UA @ admin @ c:irua:166108 |
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8367 |
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Author |
Brunekreef, B.; Janssen, N., A.H.; de Hartog, J., J.; Oldenwening, M.; Meliefste, K.; Hoek, G.; Lanki, T.; Timonen, K., L.; Vallius, M.; Pekkanen, J.; Van Grieken, R. |
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Title |
Personal, indoor, and outdoor exposures to PM2.5 and its components for groups of cardiovascular patients in Amsterdam and Helsinki |
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Minutes and reports |
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2005 |
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Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:51816 |
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8374 |
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Bencs, L.; Ravindra, K.; Van Grieken, R. |
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Title |
Platinum : environmental pollution and health effects |
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H2 Book chapter |
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2011 |
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Abbreviated Journal |
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580-595
T2 - Encyclopedia of environmental health |
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Keywords |
H2 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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978-0-444-52273-3 |
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UA @ admin @ c:irua:93109 |
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8390 |
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Trincavelli, J.; Montoro, S.; Van Grieken, R.; van Espen, P. |
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Prediction of Mα/Lα intensity ratios and the use in the spectra evaluation |
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P3 Proceeding |
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1992 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation); Chemometrics (Mitac 3) |
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UA @ admin @ c:irua:2863 |
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8405 |
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Tsuji, K.; Spolnik, Z.; Wagatsuma, K.; Nullens, R.; Van Grieken, R.E. |
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Preliminary experiments on grazing-exit electron probe microanalysis (GE-EPMA) |
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P1 Proceeding |
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1999 |
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119-122
T2 - Electron Microscopy and Analysis 1999 |
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P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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000088782800027 |
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UA @ admin @ c:irua:27602 |
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8408 |
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Goossenaerts, C.; Verbueken, A.; Van Grieken, R. |
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Preliminary LAMMA investigations on healthy and acid rain affected spruce needles |
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P3 Proceeding |
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1986 |
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P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Call Number |
UA @ admin @ c:irua:117511 |
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8409 |
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Author |
Van Grieken, R.; Wollast, R. |
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Progress in Belgian oceanographic research : proceedings of symposium, Brussels, 3-5 March 1985 |
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1985 |
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479 p. |
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ME3 Book as editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA @ admin @ c:irua:117474 |
Serial |
8422 |
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| Permanent link to this record |
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Author |
Markowicz, A.A.; Van Grieken, R.E. |
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Title |
Quantification in XRF analysis of intermediate-thickness samples |
Type |
H3 Book chapter |
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Year |
2002 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
407-431
T2 - Handbook of X-ray spectrometry / Grie |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:36389 |
Serial |
8433 |
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| Permanent link to this record |
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Author |
Markowicz, A.M.; Van Grieken, R.E. |
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Title |
Quantification in XRF analysis of intermediate-thickness samples |
Type |
H3 Book chapter |
| |
Year |
1992 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
339-358
T2 - Handbook of X-ray spectroscopy / Grie |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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no |
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Call Number |
UA @ admin @ c:irua:2855 |
Serial |
8434 |
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Author |
Piñera, I.; Abreu, Y.; van Espen, P.; Diaz, A.; Leyva, A.; Cruz, C.M. |
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| |
Title |
Radiation damage evaluation on LYSO and LuYAP materials through Dpa calculation assisted by Monte Carlo method |
Type |
P1 Proceeding |
| |
Year |
2011 |
Publication |
IEEE conference record
T2 – IEEE Nuclear Science Symposium/Medical Imaging Conference (NSS/MIC)/18th, International Workshop on Room-Temperature Semiconductor X-Ray and, Gamma-Ray Detectors, OCT 23-29, 2011, Valencia, SPAIN |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
1609-1611 |
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Keywords |
P1 Proceeding; Engineering sciences. Technology; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The aim of the present work is to study the radiation damage induced in LYSO and LuYAP crystals by the gamma radiation and the secondary electrons/positrons generated. The displacements per atom (dpa) distributions inside each material were calculated following the Monte Carlo assisted Classical Method (MCCM) introduced by the authors. As gamma sources were used Sc-44, Na-22 and V-48. Also the energy of gammas from the annihilation processes (511 keV) was included in the study. This procedure allowed studying the in-depth dpa distributions inside each crystal for all four sources. It was also possible to obtain the separate contribution from each atom to the total dpa. The LYSO crystals were found to receive more damage, mainly provoked by the displacements of silicon and oxygen atoms. |
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000304755601169 |
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ISSN |
978-1-4673-0120-6 |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
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Call Number |
UA @ admin @ c:irua:113072 |
Serial |
8447 |
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| Permanent link to this record |
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Author |
Otten, P.; Bruynseels, F.; Van Grieken, R. |
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Title |
Reaction of marine aerosols with HNO3 vapour studied by single particle analysis |
Type |
P3 Proceeding |
| |
Year |
1986 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:117508 |
Serial |
8455 |
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Author |
Claes, M.; de Bokx, P.; Van Grieken, R. |
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Title |
Recent developments of laboratory grazing emission X-ray fluorescence spectrometry |
Type |
P1 Proceeding |
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Year |
1999 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
103-107
T2 - Proceedings of the European Conferenc |
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Keywords |
P1 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
000081658400015 |
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UA library record; WoS full record |
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Notes |
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no |
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Call Number |
UA @ admin @ c:irua:24718 |
Serial |
8459 |
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Author |
Bruynseels, F.; Van Grieken, R. |
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Title |
Recombination reactions and geometry effects in laser microprobe mass analysis studied with 12C/13C bilayers |
Type |
P3 Proceeding |
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Year |
1986 |
Publication |
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Abbreviated Journal |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:117512 |
Serial |
8462 |
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| Permanent link to this record |
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Author |
Injuk, J.; Van Grieken, R. |
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Title |
Reference matarials for microanalytical nuclear techniques |
Type |
P3 Proceeding |
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Year |
1995 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:55574 |
Serial |
8467 |
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Author |
Kontozova, V.; Krupińska, B.; Van Grieken, R.; Janssen, E.; Moris, H.; Aerts, D.; Watteeuw, L.; van Bos, M.; Peckstadt, A. |
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Title |
Research for preventive conservation and optimal presentation of world heritage in Museum Plantin-Moretus, Antwerp |
Type |
P3 Proceeding |
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Year |
2011 |
Publication |
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Issue |
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Pages |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISBN |
978-989-97522-0-7 |
Additional Links |
UA library record |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:92095 |
Serial |
8473 |
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Author |
Swerling, G.; Travaglini, B.; Van Grieken, R.; Spolnik, Z.; Bencs, L.; [et al.]; European Project Freindly-Heating |
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Title |
Il riscaldamento nelle chiese e la conservazione dei beni culturali = Church heating and the preservation of the cultural heritage |
Type |
ME2 Book as editor or co-editor |
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Year |
2006 |
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Volume |
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Issue |
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Pages |
240 p. |
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Keywords |
ME2 Book as editor or co-editor; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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ISBN |
88-370-5034-8 |
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UA library record |
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no |
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Call Number |
UA @ admin @ c:irua:61684 |
Serial |
8480 |
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Author |
Moropoulou, A.; Bisbikou, K.; Torfs, K.; Van Grieken, R. |
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Title |
Risk analysis for the protection of cultural heritage from industrial pollution |
Type |
H3 Book chapter |
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Year |
1999 |
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Volume |
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Pages |
475-484
T2 - Structural studies, repairs and maint |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:27598 |
Serial |
8483 |
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| Permanent link to this record |
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Author |
Godoi, R.H.M.; Godoi, A.F.L.; de Quadros, L.C.; Polezer, G.; Silva, T.O.B.; Yamamoto, C.I.; Van Grieken, R.; Potgieter-Vermaak, S. |
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Title |
Risk assessment and spatial chemical variability of PM collected at selected bus stations |
Type |
A1 Journal article |
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Year |
2013 |
Publication |
Air quality, atmosphere & health |
Abbreviated Journal |
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Volume |
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Issue |
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Pages |
1-11 |
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Keywords |
A1 Journal article; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Abstract |
The chemical characterization of particulate matter inside and outside of confined bus shelters has been discerned for the first time. Transit patrons are at risk due to the close vicinity of densely trafficked areas resulting in elevated pollution footprints. Incomplete combustion processes, as well as exhaust and wear and tear emissions from public and personal transportation vehicles, are key contributors to degraded urban air quality and are often implicated as causal to various diseases in humans. Urban planning, therefore, includes efficient public transport systems to mitigate the effect. The bus rapid transit system was inaugurated in Curitiba to ensure dedicated traffic lanes, major bus interchanges and semi-confined bus stops called tube stations. To assess the chemical risk that the passengers are exposed to, an investigation of the aerosol inside and outside five of these tube stations was launched. Electron probe X-ray micro-analysis and X-ray fluorescence were used to determine the elemental composition of individual and of bulk particle samples. An aethalometer quantified the black carbon. Elemental concentrations inside the shelters were in general higher than outside, especially for traffic-related elements. The lead concentration exceeded the NAAS standard at times, although the average was below the guideline. The biogenic, organic and soot clusters showed the highest abundance for the city centre sites. The overall carcinogenic risk could be classed as moderate, and the risk was significant at two sites during one of the sampling campaigns. The non-carcinogenic risk is well below the significant value. |
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000328332500006 |
Publication Date |
2013-11-01 |
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Series Issue |
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Edition |
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ISSN |
1873-9318 |
ISBN |
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Additional Links |
UA library record; WoS full record; WoS citing articles |
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no |
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Call Number |
UA @ admin @ c:irua:111086 |
Serial |
8484 |
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Author |
Chou, L.; Harlay, J.; Roevros, N.; Lannuzel, D.; Rebreanu, L.; van der Zee, C.; Lapernat, P.-E.; Daro, M.-H.; Aerts, K.; Godoi, R.; Van Grieken, R. |
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Title |
Role of oceanic production and dissolution of calcium carbonate in climate change (CCCC): final report |
Type |
Minutes and reports |
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Year |
2009 |
Publication |
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Keywords |
Minutes and reports; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:80696 |
Serial |
8486 |
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Author |
Delalieux, F.; Van Grieken, R.; Moropoulou, A. |
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Title |
Salt weathering research: present state and future directions |
Type |
P3 Proceeding |
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Year |
2003 |
Publication |
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Volume |
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Issue |
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Keywords |
P3 Proceeding; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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no |
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Call Number |
UA @ admin @ c:irua:42732 |
Serial |
8490 |
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Author |
Schmeling, M.; Van Grieken, R.E. |
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Title |
Sample preparation for X-ray fluorescence |
Type |
H3 Book chapter |
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Year |
2002 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
933-976
T2 - Handbook of X-ray spectrometry / Grie |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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UA library record |
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Notes |
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Approved |
no |
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| |
Call Number |
UA @ admin @ c:irua:36388 |
Serial |
8494 |
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| Permanent link to this record |
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Author |
Injuk, J.; Van Grieken, R.E. |
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Title |
Sample preparation for XRF |
Type |
H3 Book chapter |
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Year |
1992 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
657-692
T2 - Handbook of X-ray spectroscopy / Grie |
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Keywords |
H3 Book chapter; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Additional Links |
UA library record |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:2857 |
Serial |
8496 |
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| Permanent link to this record |
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Author |
Robberecht, H.; Van Grieken, R. |
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Title |
Selenium content and speciation in environmental waters determied by X-ray fluorescence spectroscopy |
Type |
H3 Book chapter |
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Year |
1980 |
Publication |
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Abbreviated Journal |
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Volume |
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Issue |
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Pages |
362-366
T2 - Trace substances in environmental hea |
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Keywords |
H3 Book chapter; Pharmacology. Therapy; AXES (Antwerp X-ray Analysis, Electrochemistry and Speciation) |
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Wos |
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ISSN |
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ISBN |
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Additional Links |
UA library record |
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Impact Factor |
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Times cited |
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Open Access |
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Notes |
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Approved |
no |
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Call Number |
UA @ admin @ c:irua:117481 |
Serial |
8505 |
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| Permanent link to this record |
